盐酸司来吉兰片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号101298-201801对照品来源中检院对照品使用方法减压干燥3h
对照品含量(%)99.5对照品水分(%)0对照品稀释倍数1000
标示量(mg)5供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.152502832502772503422502382503512502980.02
210.182498292498002498140.01
单位质量响应值RSD%判断
24659.9024539.690.35数据可信
供试品溶液-24103001批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1170440-17044068.93968.416.6468.9468.416.64
2178033-17803372.01072.01
3177344-17734471.73271.73
4153623-15362362.13762.14
5156792-15679263.41963.42
6178557-17855772.22272.22
10min1220483-22048389.18085.025.0289.3985.225.02
2221152-22115289.45189.67
3214562-21456286.78587.00
4199365-19936580.63980.83
5196291-19629179.39579.59
6209268-20926884.64484.86
15min1229858-22985892.97289.723.3393.4590.183.34
2228501-22850192.42392.91
3225040-22504091.02491.50
4213511-21351186.36086.79
5212734-21273486.04686.47
6221289-22128989.50689.98
20min1230579-23057993.26491.062.7294.0291.792.74
2232456-23245694.02394.78
3226732-22673291.70892.46
4219596-21959688.82289.51
5216723-21672387.66088.35
6224734-22473490.90091.64
30min1234646-23464694.90991.842.1595.9492.842.17
2231577-23157793.66894.71
3225454-22545491.19192.21
4222875-22287590.14891.10
5223066-22306690.22591.17
6224806-22480690.92991.94
45min1231503-23150393.63891.421.7894.9692.701.80
2229993-22999393.02794.35
3224629-22462990.85792.15
4221343-22134389.52890.75
5222696-22269690.07591.30
6225980-22598091.40492.69
60min1232556-23255694.06491.681.8795.6693.241.87
2229255-22925592.72894.33
3223562-22356290.42692.00
4228905-22890592.58794.08
5221323-22132389.52091.01
6224429-22442990.77692.34
极限1231021-23102193.44391.051.7495.3292.881.75
2227735-22773592.11494.00
3222940-22294090.17492.02
4220297-22029789.10590.88
5222658-22265890.06091.82
6225932-22593291.38493.22
点击查看处理图标(自动生成)
　
原始图谱下载图谱(谢超君 于 2024-11-04 15:31:48 完成)
生成报告数据部分下载报告(谢超君 于 2024-11-04 15:31:58 完成)
Current page cost:50 ms