洛索洛芬钠细粒剂项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100638对照品来源中检所对照品使用方法直接使用
对照品含量(%)87.5对照品水分(%)0对照品稀释倍数200
标示量(mg)60供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
115.041686849168797816897711693108169243516900280.17
215.011673023167664816748360.16
单位质量响应值RSD%判断
112368.88111581.350.50数据可信
供试品溶液-24102801批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11580339-158033992.62091.312.1392.6291.312.13
21591404-159140493.26893.27
31570575-157057592.04792.05
41569713-156971391.99792.00
51504896-150489688.19888.20
61531077-153107789.73389.73
15min11697733-169773399.500100.552.9299.65100.702.92
21770941-1770941103.790103.95
31744456-1744456102.238102.39
41761035-1761035103.210103.36
51655253-165525397.01097.16
61664411-166441197.54797.70
30min11697642-169764299.495100.692.3599.81101.012.35
21767380-1767380103.582103.91
31743992-1743992102.211102.53
41746842-1746842102.378102.70
51664109-166410997.52997.84
61688412-168841298.95499.27
极限11712267-1712267100.352100.572.64100.84101.062.64
21766452-1766452103.527104.03
31754395-1754395102.821103.31
41737495-1737495101.830102.33
51656576-165657697.08897.56
61669008-166900897.81698.29
洛索洛芬钠细粒剂项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100638对照品来源中检所对照品使用方法直接使用
对照品含量(%)87.5对照品水分(%)0对照品稀释倍数200
标示量(mg)60供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
115.041674253167527116755261674595168911516777520.38
215.011671410167016216707860.06
单位质量响应值RSD%判断
111552.66111311.530.16数据可信
供试品溶液-24102801批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11641826-164182696.69198.831.9696.6998.821.96
21687529-168752999.38399.38
31682780-168278099.10399.10
41635290-163529096.30696.31
51705668-1705668100.451100.45
61715371-1715371101.022101.02
15min11664344-166434498.01799.621.8498.1899.791.84
21698941-1698941100.055100.22
31686897-168689799.34599.51
41649365-164936597.13597.30
51722283-1722283101.429101.60
61727647-1727647101.745101.91
30min11663708-166370897.98099.501.7198.3099.831.71
21702776-1702776100.281100.61
31683665-168366599.15599.49
41649859-164985997.16497.49
51715937-1715937101.056101.39
61721001-1721001101.354101.69
极限11659538-165953897.73499.311.7798.2299.811.77
21694686-169468699.804100.30
31680100-168010098.94599.44
41647051-164705196.99997.48
51714119-1714119100.949101.45
61722469-1722469101.440101.95
洛索洛芬钠细粒剂项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100638对照品来源中检所对照品使用方法直接使用
对照品含量(%)87.5对照品水分(%)0对照品稀释倍数200
标示量(mg)60供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
115.041676444167616916777071676116167404316760960.08
215.011673599167391216737560.02
单位质量响应值RSD%判断
111442.55111509.390.05数据可信
供试品溶液-24102801批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11755855-1755855103.36699.064.25103.3799.064.25
21676341-167634198.68598.68
31755848-1755848103.365103.37
41568528-156852892.33892.34
51643227-164322796.73596.74
61696152-169615299.85199.85
15min11761535-1761535103.70099.494.26103.8799.664.26
21683352-168335299.09899.26
31767200-1767200104.034104.21
41574709-157470992.70292.86
51653537-165353797.34297.50
61699930-1699930100.074100.24
30min11758215-1758215103.50599.294.18103.8599.624.18
21678336-167833698.80299.13
31761522-1761522103.699104.05
41574460-157446092.68793.00
51650273-165027397.15097.47
61696986-169698699.900100.23
极限11754985-1754985103.31599.064.19103.8399.564.19
21673222-167322298.50199.00
31757412-1757412103.457103.98
41571309-157130992.50292.96
51646284-164628496.91597.40
61693004-169300499.666100.17
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