叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.011219193121987212199771219110121918012194660.04
210.011217598121699712172980.04
单位质量响应值RSD%判断
121824.78121608.190.13数据可信
供试品溶液-24103102批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min183088-8308811.20610.654.4411.2110.654.44
281095-8109510.93710.94
377951-7795110.51310.51
479066-7906610.66410.66
572787-727879.8179.82
679646-7964610.74210.74
10min1159184-15918421.46920.472.7121.5920.592.69
2151653-15165320.45420.58
3151787-15178720.47220.59
4147681-14768119.91820.04
5151945-15194520.49320.60
6148266-14826619.99720.12
15min1217076-21707629.27727.772.8129.6428.122.81
2206322-20632227.82728.18
3204237-20423727.54627.89
4202444-20244427.30427.64
5200946-20094627.10227.44
6204369-20436927.56327.90
20min1257807-25780734.77132.973.0335.4633.623.02
2240200-24020032.39633.05
3242606-24260632.72033.37
4242743-24274332.73933.38
5236388-23638831.88232.52
6246845-24684533.29233.94
30min1314332-31433242.39440.053.0043.4741.072.99
2292807-29280739.49140.51
3294153-29415339.67340.69
4294525-29452539.72340.73
5289067-28906738.98739.98
6296897-29689740.04341.06
45min1369522-36952249.83847.223.1451.3848.683.12
2343182-34318246.28547.74
3353691-35369147.70349.16
4341733-34173346.09047.54
5340494-34049445.92347.35
6351856-35185647.45548.92
60min1401758-40175854.18551.952.5556.2853.942.55
2378007-37800750.98252.95
3387186-38718652.22054.20
4381440-38144051.44553.41
5374082-37408250.45352.39
6388657-38865752.41954.41
90min1443485-44348559.81358.052.1462.5160.622.16
2424253-42425357.21959.76
3436790-43679058.91061.48
4421731-42173156.87959.41
5421468-42146856.84459.34
6434791-43479158.64161.21
极限1493702-49370266.58664.062.3569.9567.272.36
2466445-46644562.91066.08
3475724-47572464.16167.38
4470178-47017863.41366.58
5463025-46302562.44965.58
6480573-48057364.81568.04
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.011217967121802412178131217379121683212176030.05
210.011216296121604212161690.02
单位质量响应值RSD%判断
121638.66121495.400.09数据可信
供试品溶液-24103102批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min198146-9814613.25313.243.5213.2513.243.51
297912-9791213.22213.22
392730-9273012.52212.52
4102595-10259513.85413.85
5100653-10065313.59213.59
696192-9619212.98912.99
10min1180615-18061524.39024.571.4324.5424.721.44
2180549-18054924.38124.53
3178830-17883024.14924.29
4186276-18627625.15425.31
5183094-18309424.72424.88
6182310-18231024.61924.76
15min1235483-23548331.79932.432.2632.2232.852.23
2235265-23526531.76932.19
3242311-24231132.72133.13
4247790-24779033.46133.89
5235719-23571931.83132.26
6244481-24448133.01433.43
20min1271733-27173336.69437.912.6637.4738.692.62
2274050-27405037.00737.78
3286185-28618538.64539.42
4286892-28689238.74139.55
5276615-27661537.35338.13
6288889-28888939.01139.80
30min1317366-31736642.85645.203.9144.0446.403.85
2322199-32219943.50944.69
3342159-34215946.20447.40
4344123-34412346.46947.70
5332087-33208744.84446.04
6350447-35044747.32348.54
45min1372207-37220750.26252.313.5951.9254.013.53
2375888-37588850.75952.42
3404879-40487954.67456.39
4384162-38416251.87653.63
5383239-38323951.75153.44
6403735-40373554.51956.26
60min1395933-39593353.46556.754.0455.6859.033.98
2409536-40953655.30257.53
3432920-43292058.46060.78
4426400-42640057.58059.91
5414147-41414755.92558.19
6442544-44254459.76062.11
90min1441429-44142959.60962.733.3062.4265.643.27
2453911-45391161.29564.14
3476654-47665464.36667.34
4469473-46947363.39666.36
5462500-46250062.45465.34
6483174-48317465.24668.26
极限1491998-49199866.43869.542.6669.9173.152.60
2520949-52094970.34773.87
3504594-50459468.13971.82
4526148-52614871.04974.72
5525489-52548970.96074.54
6520550-52055070.29374.03
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