佩玛贝特片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号HX240702对照品来源ZZ对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数100000
标示量(mg)0.1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 10.002085120882210612072520949208940.60
2 10.052058020915207481.15
单位质量响应值RSD%判断
2089.402064.480.85数据可信
供试品溶液-24103101批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min117185-1718574.17372.049.0174.1772.049.01
217077-1707773.70673.71
319280-1928083.21583.21
415749-1574967.97567.97
515190-1519065.56265.56
615666-1566667.61667.62
10min121003-2100390.65293.331.6190.7893.451.60
221740-2174093.83393.96
321896-2189694.50694.64
421501-2150192.80192.91
521647-2164793.43193.54
621956-2195694.76594.88
15min122363-2236396.52197.701.6996.8097.981.68
223068-2306899.56499.84
322394-2239496.65596.95
422214-2221495.87896.15
522671-2267197.85198.12
623112-2311299.754100.02
20min122840-2284098.58098.821.3999.0299.261.39
223438-23438101.161101.61
322686-2268697.91698.37
422557-2255797.35997.79
522770-2277098.27898.71
623080-2308099.616100.05
30min122864-2286498.68499.281.4499.2899.881.43
223436-23436101.153101.77
322572-2257297.42498.04
422764-2276498.25298.84
523077-2307799.603100.20
623298-23298100.557101.16
45min122783-2278398.33498.531.2699.1099.301.25
223282-23282100.488101.27
322457-2245796.92797.71
422668-2266897.83898.59
522770-2277098.27899.04
623015-2301599.336100.11
60min122740-2274098.14998.871.4899.0899.801.47
223472-23472101.308102.26
322536-2253697.26898.21
422809-2280998.44699.36
522751-2275198.19699.12
623138-2313899.866100.80
极限122607-2260797.57598.501.7298.6799.601.71
223491-23491101.390102.51
322365-2236596.53097.64
422682-2268297.89898.98
522762-2276298.24499.33
623025-2302599.379100.48
佩玛贝特片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号HX240702对照品来源ZZ对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数100000
标示量(mg)0.1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 10.002095621204210732104121141210830.45
2 10.052115321169211610.06
单位质量响应值RSD%判断
2108.302105.570.10数据可信
供试品溶液-24103102批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min17084-708430.13920.3230.6730.1420.3230.67
24347-434718.49418.49
36013-601325.58225.58
43276-327613.93813.94
54205-420517.89017.89
63725-372515.84815.85
10min118767-1876779.84575.3810.1279.8975.4110.11
218223-1822377.53077.56
318136-1813677.16077.20
414129-1412960.11260.14
518934-1893480.55580.58
618111-1811177.05477.08
15min122923-2292397.52692.349.2197.7192.509.21
221763-2176392.59192.75
322469-2246995.59595.77
417919-1791976.23776.36
523581-23581100.326100.49
621568-2156891.76291.92
20min123201-2320198.70995.709.0099.0596.029.00
222974-2297497.74398.06
324619-24619104.742105.07
418612-1861279.18579.44
522808-2280897.03797.37
622755-2275596.81297.12
30min123091-2309198.24198.183.3398.7598.663.36
223706-23706100.858101.33
324008-24008102.143102.65
421818-2181892.82593.21
523086-2308698.22098.71
622754-2275496.80797.28
45min123215-2321598.76998.721.7999.4499.361.79
223758-23758101.079101.72
323144-2314498.46799.14
422790-2279096.96197.50
522727-2272796.69297.35
623588-23588100.356100.99
60min123207-2320798.73599.631.2799.57100.441.26
222996-2299697.83798.65
323865-23865101.534102.37
423462-2346299.820100.52
523537-23537100.139100.96
623444-2344499.743100.54
极限123083-2308398.207100.551.7099.21101.521.67
223499-2349999.977100.95
324273-24273103.270104.28
423823-23823101.355102.22
523453-2345399.781100.77
623673-23673100.717101.68
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