枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数125
标示量(mg)100供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.429530079526519516879516919522039522480.07
217.479496129493629494870.02
单位质量响应值RSD%判断
54664.0654349.570.41数据可信
供试品溶液-2022072301批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1520571-52057148.35946.212.6548.3646.212.65
2481118-48111844.69444.69
3491081-49108145.62045.62
4493663-49366345.86045.86
5500682-50068246.51246.51
6497416-49741646.20846.21
10min1515200-51520047.86045.523.3847.9445.603.38
2483081-48308144.87744.95
3464985-46498543.19643.27
4490454-49045445.56245.64
5497682-49768246.23346.31
6488535-48853545.38345.46
15min1506150-50615047.02045.402.0047.1845.552.00
2484996-48499645.05545.20
3476855-47685544.29844.45
4485096-48509645.06445.22
5489558-48955845.47845.63
6489430-48943045.46645.62
20min1500734-50073446.51744.702.3246.7644.932.33
2474147-47414744.04744.27
3469273-46927343.59443.82
4475374-47537444.16144.39
5484377-48437744.99745.23
6483322-48332244.89945.13
30min1490100-49010045.52943.772.4345.8444.072.42
2456186-45618642.37842.68
3463765-46376543.08243.38
4469960-46996043.65843.96
5474281-47428144.05944.36
6472513-47251343.89544.20
45min1479397-47939744.53442.593.3344.9342.963.32
2434507-43450740.36440.73
3451117-45111741.90742.27
4455563-45556342.32042.69
5465328-46532843.22743.61
6464605-46460543.16043.54
极限1454380-45438042.21040.284.2942.6840.734.27
2399661-39966137.12737.56
3429369-42936939.88740.32
4435898-43589840.49340.94
5442013-44201341.06241.51
6440342-44034240.90641.35
枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数125
标示量(mg)100供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.429511379505069504589518759513289510610.07
217.479505849512919509380.06
单位质量响应值RSD%判断
54595.9254432.630.22数据可信
供试品溶液-2022072401批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1452067-45206741.99044.443.4341.9944.443.44
2499020-49902046.35146.35
3486156-48615645.15645.16
4476622-47662244.27044.27
5469454-46945443.60443.60
6487571-48757145.28745.29
10min1455456-45545642.30444.683.0442.3744.763.04
2494525-49452545.93346.01
3492897-49289745.78245.86
4480749-48074944.65444.73
5474863-47486344.10744.18
6487900-48790045.31845.39
15min1454738-45473842.23844.332.8142.3844.482.81
2490407-49040745.55145.70
3486637-48663745.20145.35
4473103-47310343.94344.09
5472179-47217943.85844.00
6486473-48647345.18545.34
20min1451706-45170641.95643.922.6842.1744.142.68
2486220-48622045.16245.39
3481651-48165144.73744.96
4468964-46896443.55943.78
5467834-46783443.45443.67
6480441-48044144.62544.85
30min1446428-44642841.46643.162.3741.7543.462.37
2474322-47432244.05744.36
3473494-47349443.98044.28
4460315-46031542.75643.05
5460646-46064642.78643.08
6472775-47277543.91344.21
45min1440004-44000440.86942.372.1241.2242.742.12
2464952-46495243.18643.56
3464013-46401343.09943.47
4453739-45373942.14542.51
5451775-45177541.96242.33
6462413-46241342.95043.32
极限1421142-42114239.11740.291.8039.5440.731.81
2441829-44182941.03941.49
3440469-44046940.91241.36
4431179-43117940.04940.48
5430169-43016939.95640.39
6437716-43771640.65741.10
枸橼酸西地那非片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号420012-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)98.8对照品水分(%)0对照品稀释倍数125
标示量(mg)100供试品稀释倍数1系数0.7118
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
117.429490209488049491139472819484519485340.08
217.479507469498259502860.07
单位质量响应值RSD%判断
54450.8654395.310.08数据可信
供试品溶液-2022072401批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1515912-51591248.00043.897.4548.0043.897.45
2466780-46678043.42943.43
3433099-43309940.29540.30
4449706-44970641.84041.84
5513972-51397247.81947.82
6451086-45108641.96941.97
10min1517793-51779348.17544.018.1948.2544.088.19
2481491-48149144.79744.87
3417689-41768938.86138.93
4453472-45347242.19142.26
5513395-51339547.76647.85
6454270-45427042.26542.33
15min1524706-52470648.81844.257.6148.9844.397.62
2480007-48000744.65944.81
3436501-43650140.61240.74
4451229-45122941.98242.12
5511694-51169447.60747.77
6449272-44927241.80041.94
20min1508018-50801847.26543.746.7447.5143.966.75
2473638-47363844.06744.29
3432723-43272340.26040.46
4446730-44673041.56341.77
5506680-50668047.14147.38
6453173-45317342.16342.37
30min1509680-50968047.42043.247.3247.7443.537.31
2467012-46701243.45043.75
3428773-42877339.89340.16
4435158-43515840.48740.77
5500510-50051046.56746.88
6447355-44735541.62141.90
45min1499959-49995946.51642.447.4946.9242.817.49
2460073-46007342.80543.17
3417525-41752538.84639.18
4432414-43241440.23140.58
5492975-49297545.86646.26
6434085-43408540.38740.74
极限1465082-46508243.27140.156.1943.7540.586.20
2434503-43450340.42640.86
3400286-40028637.24237.64
4416646-41664638.76439.18
5460690-46069042.86243.33
6412038-41203838.33638.75
点击查看处理图标(人工保存)
　
原始图谱下载图谱(谢超君 于 2024-11-12 15:32:57 完成)
生成报告数据部分下载报告(谢超君 于 2024-11-12 15:33:18 完成)
Current page cost:93 ms