洛索洛芬钠细粒剂项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100638-202104对照品来源中检所对照品使用方法直接使用
对照品含量(%)87.5对照品水分(%)0对照品稀释倍数200
标示量(mg)60供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.831668785167094916685091669502167073516696960.07
214.791667508166633116669200.05
单位质量响应值RSD%判断
112589.08112705.880.08数据可信
供试品溶液-24110502批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11647015-164701595.95094.361.5095.9594.361.50
21587577-158757792.48792.49
31626544-162654494.75894.76
41620424-162042494.40194.40
51594916-159491692.91592.91
61641629-164162995.63695.64
15min11723102-1723102100.38399.541.29100.5499.691.29
21686131-168613198.22998.38
31708471-170847199.53099.69
41683547-168354798.07898.24
51709105-170910599.56799.72
61741061-1741061101.429101.59
30min11738301-1738301101.26899.891.30101.60100.211.31
21689840-168984098.44598.76
31712562-171256299.769100.09
41690272-169027298.47098.79
51715377-171537799.933100.25
61741277-1741277101.442101.77
极限11730233-1730233100.79899.581.04101.29100.071.04
21690377-169037798.47698.96
31708729-170872999.545100.04
41687210-168721098.29298.78
51712936-171293699.790100.28
61725993-1725993100.551101.05
洛索洛芬钠细粒剂项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100638-202104对照品来源中检所对照品使用方法直接使用
对照品含量(%)87.5对照品水分(%)0对照品稀释倍数200
标示量(mg)60供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.831667518166966416707331668353166867016689880.08
214.791667564166798916677760.02
单位质量响应值RSD%判断
112541.34112763.760.14数据可信
供试品溶液-24110502批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11705760-170576099.36897.542.0399.3797.542.03
21663786-166378696.92396.92
31700292-170029299.04999.05
41669833-166983397.27597.28
51691960-169196098.56498.56
61614168-161416894.03294.03
15min11738997-1738997101.304100.121.51101.47100.281.51
21710948-171094899.67099.83
31729283-1729283100.738100.90
41737078-1737078101.192101.35
51725839-1725839100.538100.70
61669860-166986097.27797.43
30min11737083-1737083101.19399.821.68101.53100.151.68
21695378-169537898.76399.09
31716338-171633899.984100.32
41732401-1732401100.920101.25
51735668-1735668101.110101.44
61664587-166458796.97097.29
极限11736154-1736154101.139100.001.61101.64100.501.61
21693932-169393298.67999.17
31729678-1729678100.761101.26
41731632-1731632100.875101.37
51737410-1737410101.212101.71
61670870-167087097.33697.82
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