类型试验信息(多次测定用,隔开)图谱读取备注
项目代号:已存用户保存
项目名称:已存用户保存
试验名称可缺:待存默认值
时间点可缺:待存默认值
图谱类型:已存HPLC用户保存
样品类型:已存参比制剂,参比制剂,参比制剂,参比制剂用户保存
批号:已存505806批,506993批,506993批,GJ031批用户保存
规格可缺:待存默认值
介质名称:已存用户保存
方法名称可缺:已存桨法,桨法,桨法,桨法用户保存
转速可缺:已存50转,50转,50转,50转用户保存
组成图标坎地沙坦酯氢氯噻嗪片溶出曲线测定HPLC图谱
参比制剂-505806批批()-含0.35%吐温20的pH6.8磷酸盐溶液-桨法-50转
注1:成分名称多个峰按出峰顺序【,】(半角逗号)隔开;
注2:试验批号和介质名称都一样的填一个;有任何不一致的需要【,】(半角逗号)隔开填写波数个;
注3:特别注意:批号和规格必须存在;
编号351
项目名称坎地沙坦酯氢氯噻嗪片
选择方法
峰的筛选AUTO
根据对照品保留时间的0.95~1.05进行筛选;
对照品图谱务必只出主成分峰;
测定类型溶出
成分(个数)与图不符:3
成分名称
进样针数1针　2针
双波长
溶出度
图谱类型
制剂单位
王丹2024-03-11 15:37:13进行了保存!
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既往测定情况概览
编号 试验名称 介质体积 取样体积 补液体积 R批号 R来源 R使用方法 R含量(%) R水分(%) R稀释 R标示量(mg) T稀释 操作
6831 900,900 1.5,1.5 1.5,1.5 100309-202205,100685-201903 中检院,中检院 直接使用,直接使用 99.70,99.80 0,0 1000,1000 12.5,16 1,1 使用
6830 900,900 1.5,1.5 1.5,1.5 100309-202205,100685-201903 中检院,中检院 直接使用,直接使用 99.70,99.80 0,0 1000,1000 12.5,16 1,1 使用
6829 900,900 1.5,1.5 1.5,1.5 100309-202205,100685-201903 中检院,中检院 直接使用,直接使用 99.70,99.80 0,0 1000,1000 12.5,16 1,1 使用
6828 900,900 1.5,1.5 1.5,1.5 100309-202205,100685-201903 中检院,中检院 直接使用,直接使用 99.70,99.80 0,0 1000,1000 12.5,16 1,1 使用
5753 900,900 1.5,1.5 1.5,1.5 100309-202205,100685-201903 中检院,中检院 直接使用,直接使用 99.70,99.80 0,0 1000,1000 12.5,16 1,1 使用
5752 900,900 1.5,1.5 1.5,1.5 100309-202205,100685-201903 中检院,中检院 直接使用,直接使用 99.70,99.80 0,0 1000,1000 12.5,16 1,1 使用
5749 900,900 1.5,1.5 1.5,1.5 100309-202205,100685-201903 中检院,中检院 直接使用,直接使用 99.70,99.80 0,0 1000,1000 12.5,16 1,1 使用
5748 900,900 1.5,1.5 1.5,1.5 100309-202205,100685-201903 中检院,中检院 直接使用,直接使用 99.70,99.80 0,0 1000,1000 12.5,16 1,1 使用
5094 900,900 1.5,1.5 1.5,1.5 100309-202205,100685-201903 中检院,中检院 直接使用,直接使用 99.70,99.80 0,0 1000,1000 12.5,16 1,1 使用
5093 900,900 1.5,1.5 1.5,1.5 100309-202205,100685-201903 中检院,中检院 直接使用,直接使用 99.70,99.80 0,0 1000,1000 12.5,16 1,1 使用
5090 900,900 1.5,1.5 1.5,1.5 100309-202205,100685-201903 中检院,中检院 直接使用,直接使用 99.70,99.80 0,0 1000,1000 12.5,16 1,1 使用
5070 900,900 1.5,1.5 1.5,1.5 100309-202205,100685-201903 中检院,中检院 直接使用,直接使用 99.70,99.80 0,0 1000,1000 12.5,16 1,1 使用
5069 900,900 1.5,1.5 1.5,1.5 100309-202205,100685-201903 中检院,中检院 直接使用,直接使用 99.70,99.80 0,0 1000,1000 12.5,16 1,1 使用
5067 900,900 1.5,1.5 1.5,1.5 100309-202205,100685-201903 中检院,中检院 直接使用,直接使用 99.70,99.80 0,0 1000,1000 12.5,16 1,1 使用
5021 900,900 1.5,1.5 1.5,1.5 100309-202205,100685-201903 中检院,中检院 直接使用,直接使用 99.70,99.80 0,0 1000,1000 12.5,16 1,1 使用
5020 900,900 1.5,1.5 1.5,1.5 100309-202205,100685-201903 中检院,中检院 直接使用,直接使用 99.70,99.80 0,0 1000,1000 12.5,16 1,1 使用
5019 900,900 1.5,1.5 1.5,1.5 100309-202205,100685-201903 中检院,中检院 直接使用,直接使用 99.70,99.80 0,0 1000,1000 12.5,16 1,1 使用
5008 900,900 1.5,1.5 1.5,1.5 100309-202205,100685-201903 中检院,中检院 直接使用,直接使用 99.70,99.80 0,0 1000,1000 12.5,16 1,1 使用
5007 900,900 1.5,1.5 1.5,1.5 100309-202205,100685-201903 中检院,中检院 直接使用,直接使用 99.70,99.80 0,0 1000,1000 12.5,16 1,1 使用
5006 900,900 1.5,1.5 1.5,1.5 100309-202205,100685-201903 中检院,中检院 直接使用,直接使用 99.70,99.80 0,0 1000,1000 12.5,16 1,1 使用
注意:::正在使用与其他方法的参数!恢复
【 坎地沙坦 】信息
介质体积(ml)取样体积(ml)补液体积(ml)
对照品批号对照品来源对照品使用方法
对照品含量(%)对照品水分(%)对照品稀释倍数
标示量(mg)供试品稀释倍数系数
称样量1(mg)称样量2(mg)
注意:::正在使用与其他方法的参数!恢复
【 】信息
介质体积(ml)取样体积(ml)补液体积(ml)
对照品批号对照品来源对照品使用方法
对照品含量(%)对照品水分(%)对照品稀释倍数
标示量(mg)供试品稀释倍数系数
称样量1(mg)称样量2(mg)
注意:::正在使用与其他方法的参数!恢复
【 酯氢氯噻嗪 】信息
介质体积(ml)取样体积(ml)补液体积(ml)
对照品批号对照品来源对照品使用方法
对照品含量(%)对照品水分(%)对照品稀释倍数
标示量(mg)供试品稀释倍数系数
称样量1(mg)称样量2(mg)
谢202进行了保存!
供试品测定波数:::4次
供试品测定片数:::6片
供试品取样点数:::5min,10min,15min,20min,30min,45min,60min,极限;
对照品的峰个数:::3个峰
图谱最多峰个数:::2个峰
对照品保留时间:::1.223,3.607,0
对照品　峰面积:::412919,273641,0
待处理PDF文件:::查阅
筛选规则为:::自动
图谱张数为:::224
序号文件名溶液名称保留时间峰面积 保留时间峰面积
1cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-rj无峰无面积1NA1
2cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-dz1-11.2194728341MA13.6253129602MA2
3cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-dz1-21.2194721781MA13.6033130432MA2
4cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-dz1-31.2194730721MA13.6013127792MA2
5cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-dz1-41.2194730681MA13.6013127122MA2
6cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-dz1-51.2204726081MA13.6033128752MA2
7cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p1-5min1.2293348611MA13.6061049792MA2
8cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p2-5min1.2272534031MA13.599761622MA2
9cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p3-5min1.2302372141MA13.600755742MA2
10cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p4-5min1.2302787171MA13.603870682MA2
11cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p5-5min1.2272123601MA13.602680352MA2
12cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p6-5min1.2282011321MA13.606622372MA2
13cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p1-10min1.2295143831MA13.6032342612MA2
14cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p2-10min1.2293942301MA13.6001790812MA2
15cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p3-10min1.2273774691MA13.6001687272MA2
16cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p4-10min1.2303931711MA13.6051818862MA2
17cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p5-10min1.2293657921MA13.5981613002MA2
18cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p6-10min1.2293803881MA13.6001649602MA2
19cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p1-15min1.2305230391MA13.6072917672MA2
20cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p2-15min1.2304475261MA13.6032398792MA2
21cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p3-15min1.2304533661MA13.6032354912MA2
22cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p4-15min1.2295010251MA13.6032678262MA2
23cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p5-15min1.2304277551MA13.6032251852MA2
24cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p6-15min1.2294599891MA13.6072387352MA2
25cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p1-20min1.2295252891MA13.6033180842MA2
26cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p2-20min1.2294777401MA13.6002763842MA2
27cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p3-20min1.2274826911MA13.6002758242MA2
28cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p4-20min1.2295157501MA13.6003043742MA2
29cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p5-20min1.2304568161MA13.6002624722MA2
30cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p6-20min1.2304901321MA13.6072810722MA2
31cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p1-30min1.2305245491MA13.6033324612MA2
32cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p2-30min1.2335029931MA13.6003113202MA2
33cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p3-30min1.2285142371MA13.5993149332MA2
34cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p4-30min1.2285228021MA13.6043279872MA2
35cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p5-30min1.2304962821MA13.6033027982MA2
36cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p6-30min1.2295082891MA13.6063150642MA2
37cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p1-45min1.2305265961MA13.6033374012MA2
38cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p2-45min1.2305251221MA13.5993300412MA2
39cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p3-45min1.2305412391MA13.5993414572MA2
40cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p4-45min1.2275252171MA13.6003347662MA2
41cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p5-45min1.2315151411MA13.6063241772MA2
42cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p6-45min1.2315233101MA13.5993295782MA2
43cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p1-60min1.2295257641MA13.6073349082MA2
44cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p2-60min1.2305297761MA13.6033348052MA2
45cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p3-60min1.2285445531MA13.6033445072MA2
46cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p4-60min1.2305289641MA13.6033346622MA2
47cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p5-60min1.2305175761MA13.6023269932MA2
48cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p6-60min1.2295312561MA13.6063346562MA2
49cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p1-JX1.2315384801MA13.6013395702MA2
50cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p2-JX1.2305436961MA13.6083431152MA2
51cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p3-JX1.2285474301MA13.6063458582MA2
52cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p4-JX1.2305434621MA13.6063432692MA2
53cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p5-JX1.2315325301MA13.6053357112MA2
54cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p6-JX1.2285398651MA13.6063381512MA2
55cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-dz2-11.2234723101MA13.6023120992MA2
56cbzj-505806p-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-dz2-21.2234728241MA13.6063127222MA2
57cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-rj无峰无面积1NA1
58cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-dz1-11.2224715671MA13.6103115482MA2
59cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-dz1-21.2234717141MA13.6063121022MA2
60cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-dz1-31.2234719371MA13.6033122292MA2
61cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-dz1-41.2224725151MA13.6093122032MA2
62cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-dz1-51.2244726901MA13.6033123042MA2
63cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p1-5min1.2302436741MA13.603813762MA2
64cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p2-5min1.2292636141MA13.609844952MA2
65cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p3-5min1.2302721711MA13.603889852MA2
66cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p4-5min1.2291963171MA13.607682102MA2
67cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p5-5min1.2302708131MA13.602867972MA2
68cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p6-5min1.2292600981MA13.606840742MA2
69cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p1-10min1.2313764261MA13.6051726372MA2
70cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p2-10min1.2314027231MA13.6041852862MA2
71cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p3-10min1.2324228691MA13.6011935482MA2
72cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p4-10min1.2303813191MA13.6041679142MA2
73cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p5-10min1.2314167291MA13.6071937452MA2
74cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p6-10min1.2314499521MA13.5992030642MA2
75cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p1-15min1.2294361941MA13.6082319352MA2
76cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p2-15min1.2304662701MA13.6092493052MA2
77cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p3-15min1.2314718021MA13.6022567762MA2
78cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p4-15min1.2294469501MA13.6032367382MA2
79cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p5-15min1.2304726791MA13.6032570762MA2
80cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p6-15min1.2335222871MA13.6072773182MA2
81cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p1-20min1.2294739911MA13.6102713812MA2
82cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p2-20min1.2284904701MA13.6032856842MA2
83cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p3-20min1.2304992011MA13.6112925942MA2
84cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p4-20min1.2304963641MA13.6072820342MA2
85cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p5-20min1.2304942311MA13.6052915052MA2
86cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p6-20min1.2325339141MA13.6063154742MA2
87cbzj-506993p-1-rcqx-pH6.8+0.35tw20-16mg12.5mg-jf50z-p1-30min1.2305088661MA13.6073124152MA2
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169cbzj-GJ031p-rcqx-pH6.8+0.35tw20-8mg6.25mg-jf50z-rj无峰无面积1NA1
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221cbzj-GJ031p-rcqx-pH6.8+0.35tw20-8mg6.25mg-jf50z-p5-JX1.2292689061MA13.6021661172MA2
222cbzj-GJ031p-rcqx-pH6.8+0.35tw20-8mg6.25mg-jf50z-p6-JX1.2302716981MA13.6011680782MA2
223cbzj-GJ031p-rcqx-pH6.8+0.35tw20-8mg6.25mg-jf50z-dz2-11.2272375011MA13.5991566652MA2
224cbzj-GJ031p-rcqx-pH6.8+0.35tw20-8mg6.25mg-jf50z-dz2-21.2272377831MA13.6051566452MA2
Current page cost:154 ms