替米沙坦左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100629-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)100.0对照品水分(%)0对照品稀释倍数1250
标示量(mg)80供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.137533547506587569707533827530457534820.30
211.167495537461737478630.32
单位质量响应值RSD%判断
67698.2967012.810.72数据可信
供试品溶液-F73103批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1115325-11532515.41014.993.6715.4114.993.68
2104136-10413613.91513.91
3114273-11427315.26915.27
4112145-11214514.98514.99
5112666-11266615.05515.05
6114453-11445315.29415.29
10min1220935-22093529.52228.025.0129.6128.115.00
2190565-19056525.46425.54
3214085-21408528.60728.69
4209972-20997228.05728.14
5215431-21543128.78628.87
6207318-20731827.70227.79
15min1311952-31195241.68439.826.3341.9340.056.32
2261290-26129034.91435.13
3310703-31070341.51741.76
4303349-30334940.53440.77
5304286-30428640.66040.90
6296283-29628339.59039.83
20min1372500-37250049.77447.644.8250.2648.104.82
2324243-32424343.32643.74
3360330-36033048.14848.62
4352746-35274647.13547.60
5367144-36714449.05949.53
6362348-36234848.41848.88
30min1468871-46887162.65264.802.5963.4165.532.55
2492796-49279665.84966.50
3504909-50490967.46768.21
4482341-48234164.45265.18
5483725-48372564.63765.38
6477091-47709163.75064.48
45min1581959-58195977.76377.982.2678.8779.072.28
2558693-55869374.65475.67
3597050-59705079.77980.90
4586512-58651278.37179.46
5587241-58724178.46979.57
6590204-59020478.86579.95
60min1641976-64197685.78390.113.0887.3291.623.02
2674029-67402990.06691.50
3675139-67513990.21491.77
4707329-70732994.51596.03
5671799-67179989.76891.30
6675720-67572090.29291.81
90min1682699-68269991.22495.972.4793.2497.992.42
2727597-72759797.22399.16
3720436-72043696.26798.33
4725635-72563596.96199.01
5723113-72311396.62498.66
6729924-72992497.53499.56
120min1640222-64022285.54897.347.4788.0799.907.30
2717651-71765195.89498.37
3762564-762564101.896104.49
4720515-72051596.27798.86
5803635-803635107.384109.96
6726361-72636197.05899.62
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
极限1705723-70572394.30198.454.1697.30101.544.07
2732428-73242897.869100.88
3795337-795337106.275109.44
4721617-72161796.42499.54
5731092-73109297.691100.86
6734360-73436098.127101.23
替米沙坦左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100629-202204对照品来源中检院对照品使用方法直接使用
对照品含量(%)100.0对照品水分(%)0对照品稀释倍数1250
标示量(mg)80供试品稀释倍数10系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.137470807451347447897455127439597452950.16
211.167400017429217414610.28
单位质量响应值RSD%判断
66962.7166439.160.56数据可信
供试品溶液-E21595批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1109303-10930314.74914.924.3314.7514.924.34
2115629-11562915.60215.60
3115894-11589415.63815.64
4110602-11060214.92414.92
5108823-10882314.68414.68
6103102-10310213.91213.91
10min1206379-20637927.84728.314.1927.9328.404.18
2224083-22408330.23630.32
3209094-20909428.21428.30
4214340-21434028.92129.00
5207209-20720927.95928.04
6197913-19791326.70526.78
15min1293124-29312439.55239.272.8239.7939.522.81
2294838-29483839.78340.04
3279964-27996437.77638.02
4298279-29827940.24840.49
5298464-29846440.27340.51
6281703-28170338.01138.24
20min1354436-35443647.82548.402.4448.2848.862.43
2361043-36104348.71749.19
3353823-35382347.74248.20
4368578-36857849.73350.20
5367805-36780549.62950.09
6346355-34635546.73547.17
30min1470496-47049663.48563.712.2964.2164.442.29
2485774-48577465.54766.29
3464771-46477162.71363.43
4484308-48430865.34966.09
5469032-46903263.28864.02
6458623-45862361.88362.58
45min1629719-62971984.97081.993.1686.0483.073.12
2591459-59145979.80780.92
3590663-59066379.70080.77
4610023-61002382.31283.42
5631400-63140085.19786.28
6592426-59242679.93880.98
60min1647413-64741387.35791.053.0688.9092.583.01
2679801-67980191.72793.28
3650968-65096887.83789.35
4684338-68433892.34093.90
5689272-68927293.00594.57
6696824-69682494.02495.51
90min1709514-70951495.73798.094.3797.77100.134.29
2703539-70353994.93096.99
3762563-762563102.895104.89
4718597-71859796.96299.04
5770814-770814104.008106.09
6696507-69650793.98295.99
120min1705798-70579895.23599.093.0797.80101.683.01
2761347-761347102.731105.32
3755486-755486101.940104.51
4736539-73653999.383102.00
5735827-73582799.287101.94
6711346-71134695.98498.51
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
极限1715153-71515396.498100.774.7999.59103.914.70
2746973-746973100.791103.95
3732699-73269998.865102.00
4763759-763759103.056106.22
5808554-808554109.100112.31
6713776-71377696.31299.37
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