培哚普利氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号DJ468-220103对照品来源中检院对照品使用方法直接使用
对照品含量(%)94.8对照品水分(%)0对照品稀释倍数2000
标示量(mg)10供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.764195641776418684201441816418860.24
210.834181941850418340.06
单位质量响应值RSD%判断
3892.753862.790.55数据可信
供试品溶液-687573批-培哚普利-醋酸盐缓冲液（pH4.5)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min142615-4261593.76496.052.7193.7696.052.71
243060-4306094.74394.74
344703-4470398.35998.36
444527-4452797.97197.97
542163-4216392.77092.77
644867-4486798.71998.72
10min145462-45462100.029100.500.86101.07101.570.87
245641-45641100.422101.48
345280-4528099.628100.72
446139-46139101.518102.61
545366-4536699.817100.85
646176-46176101.600102.70
15min145139-4513999.31899.931.16101.47102.111.15
245346-4534699.773101.94
344605-4460598.143100.34
446032-46032101.283103.50
545449-45449100.000102.14
645922-45922101.041103.27
20min144750-4475098.46299.001.16101.72102.301.12
245114-4511499.263102.54
344170-4417097.186100.48
445251-4525199.564102.91
545719-45719100.594103.84
644965-4496598.935102.28
30min144672-4467298.29098.620.93102.64103.010.92
244673-4467398.293102.67
344186-4418697.221101.59
445325-4532599.727104.18
544860-4486098.704103.07
645216-4521699.487103.93
45min144064-4406496.95398.311.29102.40103.801.25
245004-4500499.021104.49
343886-4388696.561102.01
444932-4493298.862104.42
545349-4534999.780105.25
644849-4484998.680104.23
极限143673-4367396.09297.771.86102.61104.351.79
244519-4451997.954104.53
343222-4322295.100101.62
445071-4507199.168105.82
545328-4532899.734106.31
644797-4479798.565105.21
培哚普利氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100374-202106对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数2000
标示量(mg)10供试品稀释倍数2系数0.721
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.981594351588161593081593351593991592590.16
213.981590801586631588720.19
单位质量响应值RSD%判断
11391.9211364.230.18数据可信
供试品溶液-687573批-氨氯地平-醋酸盐缓冲液（pH4.5)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1151388-15138886.25186.723.5286.2586.723.52
2146784-14678483.62883.63
3160143-16014391.24091.24
4154698-15469888.13788.14
5145952-14595283.15483.15
6154328-15432887.92787.93
10min1163981-16398193.42694.301.3694.3895.271.37
2162443-16244392.55093.48
3167942-16794295.68396.70
4167788-16778895.59596.57
5164445-16444593.69194.61
6166540-16654094.88495.86
15min1168326-16832695.90294.501.0797.9096.521.07
2163553-16355393.18295.14
3165589-16558994.34296.42
4167519-16751995.44297.48
5164663-16466393.81595.78
6165589-16558994.34296.37
20min1167216-16721695.26993.551.0098.3396.620.98
2163181-16318192.97095.96
3164366-16436693.64696.77
4164115-16411593.50396.60
5163900-16390093.38096.39
6162458-16245892.55895.64
30min1166635-16663594.93893.171.4699.0697.271.43
2161318-16131891.90995.93
3162430-16243092.54396.71
4165742-16574294.42998.57
5160859-16085991.64795.69
6164232-16423293.56997.68
45min1165891-16589194.51493.630.7299.6998.770.69
2163647-16364793.23698.28
3163011-16301192.87498.07
4164997-16499794.00599.20
5165232-16523294.13999.20
6163303-16330393.04098.19
极限1165719-16571994.41693.951.04100.64100.120.97
2163040-16304092.89098.97
3163164-16316492.96199.19
4164775-16477593.879100.11
5167612-16761295.495101.60
6165091-16509194.059100.24
点击查看处理图标(自动生成)
　
原始图谱下载图谱(姜进硙 于 2024-03-11 19:06:30 完成)
生成报告数据部分(等待生成报告)
Current page cost:40 ms