他克莫司颗粒项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号D230603对照品来源自制对照品使用方法直接使用
对照品含量(%)97.04对照品水分(%)0对照品稀释倍数17500
标示量(mg)1供试品稀释倍数1.4系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 14.261580421576311578691569441574221575820.28
2 14.001514041518181516110.20
单位质量响应值RSD%判断
11050.6310829.361.44数据可信
供试品溶液-023431批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min144302-4430228.29729.663.5128.3029.663.51
245393-4539328.99328.99
346199-4619929.50829.51
447729-4772930.48530.49
548854-4885431.20431.20
646182-4618229.49729.50
10min169616-6961644.46547.153.2444.7847.483.24
274082-7408247.31847.64
372912-7291246.57046.90
474683-7468347.70248.04
576634-7663448.94849.29
674988-7498847.89648.22
15min183510-8351053.34058.164.5854.1559.014.54
292927-9292759.35460.20
393130-9313059.48460.33
495661-9566161.10161.97
590150-9015057.58158.47
690927-9092758.07758.94
20min196133-9613361.40265.763.6462.8067.263.61
2105871-10587167.62269.13
3105269-10526967.23768.74
4103054-10305465.82367.37
5101669-10166964.93866.47
6105763-10576367.55369.06
30min1110722-11072270.72077.124.3172.8079.364.28
2122647-12264778.33780.60
3125168-12516879.94782.20
4121895-12189577.85780.14
5120165-12016576.75279.00
6123896-12389679.13581.39
45min1136905-13690587.44487.161.5290.3190.251.46
2136598-13659887.24890.38
3137480-13748087.81190.95
4138254-13825488.30691.45
5137139-13713987.59390.70
6132397-13239784.56587.70
60min1139894-13989489.35390.061.0693.1994.111.07
2139575-13957589.14993.25
3143004-14300491.34095.46
4141305-14130590.25494.38
5139730-13973089.24893.33
6142464-14246490.99595.07
90min1145153-14515392.71293.001.9597.5598.051.87
2144337-14433792.19197.28
3144508-14450892.30097.43
4151062-15106296.486101.61
5145635-14563593.02098.09
6142909-14290991.27996.36
极限1145036-14503692.63792.151.1698.5098.241.10
2142219-14221990.83896.95
3144758-14475892.46098.62
4146512-14651293.58099.78
5144740-14474092.44898.55
6142383-14238390.94397.04
他克莫司颗粒项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号D230603对照品来源自制对照品使用方法直接使用
对照品含量(%)97.04对照品水分(%)0对照品稀释倍数17500
标示量(mg)1供试品稀释倍数1.4系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
1 14.261561341565631572081564381563511565390.26
2 14.001505861504331505100.08
单位质量响应值RSD%判断
10977.4910750.711.48数据可信
供试品溶液-023431批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min147979-4797930.85930.593.9530.8630.593.95
249389-4938931.76631.77
349006-4900631.52031.52
446530-4653029.92729.93
548132-4813230.95830.96
644311-4431128.50028.50
10min174552-7455247.95147.052.6848.2947.392.66
272229-7222946.45746.81
373966-7396647.57447.92
475748-7574848.72049.05
570357-7035745.25345.60
672077-7207746.35946.68
15min189268-8926857.41658.902.7758.2959.762.72
291378-9137858.77359.64
392499-9249959.49460.37
489181-8918157.36058.23
596031-9603161.76662.61
691058-9105858.56759.40
20min1101342-10134265.18265.472.9166.7066.992.85
2100868-10086864.87766.40
3107266-10726668.99270.53
499167-9916763.78365.29
599493-9949363.99365.53
6102597-10259765.98967.47
30min1121053-12105377.86076.122.3380.1078.362.28
2118927-11892776.49278.74
3120926-12092677.77880.08
4117539-11753975.59977.82
5113571-11357173.04775.29
6118033-11803375.91778.13
45min1136851-13685188.02186.272.0191.1289.361.96
2134382-13438286.43389.53
3135988-13598887.46690.64
4132024-13202484.91687.98
5129857-12985783.52286.58
6135692-13569287.27590.33
60min1139860-13986089.95688.941.5394.0492.991.47
2136341-13634187.69391.75
3137436-13743688.39792.54
4137072-13707288.16392.17
5137161-13716188.22092.20
6141832-14183291.22495.25
90min1144154-14415492.71892.601.2597.8097.641.22
2142043-14204391.36096.39
3145786-14578693.76898.89
4144257-14425792.78497.77
5141713-14171391.14896.11
6145911-14591193.84898.89
极限1144002-14400292.62091.482.3098.7397.542.19
2138571-13857189.12795.17
3142694-14269491.77997.95
4143358-14335892.20698.22
5138163-13816388.86594.84
6146544-14654494.255100.34
点击查看处理图标(人工保存)
　
原始图谱下载图谱(姜进硙 于 2024-11-25 15:56:38 完成)
生成报告数据部分(等待生成报告)
Current page cost:62 ms