替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.272390124101240402406124162240530.41
213.222404824131240900.25
单位质量响应值RSD%判断
1812.581822.240.38数据可信
加速6月-供试品溶液-2024050921批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min123945-2394592.43094.204.0692.4394.204.06
224631-2463195.07895.08
324541-2454194.73194.73
426188-26188101.088101.09
523538-2353890.85990.86
623580-2358091.02191.02
10min125607-2560798.84598.764.9499.7799.704.93
225334-2533497.79298.74
325557-2555798.65299.60
427891-27891107.662108.67
524065-2406592.89393.80
625057-2505796.72297.63
15min125310-2531097.69998.973.6299.61100.903.63
225701-2570199.208101.14
325820-2582099.668101.60
427146-27146104.786106.87
524265-2426593.66595.50
625590-2559098.780100.66
20min124723-2472395.43397.474.2398.32100.394.22
224865-2486595.98198.90
325760-2576099.436102.37
427059-27059104.450107.59
523935-2393592.39195.17
625159-2515997.11699.98
30min124228-2422893.52296.524.2097.37100.424.18
225123-2512396.977100.86
325803-2580399.602103.53
426476-26476102.200106.38
523574-2357490.99894.70
624824-2482495.82399.66
极限124474-2447494.47296.273.6799.25101.133.68
224871-2487196.004100.85
325143-2514397.054101.98
426484-26484102.231107.43
523704-2370491.50096.11
624966-2496696.371101.17
替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.272389724201239532404324185240560.57
213.222385324094239740.72
单位质量响应值RSD%判断
1812.811813.460.03数据可信
中间条件6月-供试品溶液-2024050921批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min125011-2501196.77296.503.1296.7796.503.12
225728-2572899.54699.55
323974-2397492.75992.76
424769-2476995.83595.84
525917-25917100.277100.28
624247-2424793.81693.82
10min126211-26211101.41599.122.00102.38100.082.00
226120-26120101.063102.06
324796-2479695.94096.87
425513-2551398.71499.67
525535-2553598.79999.80
625527-2552798.76899.71
15min125834-2583499.95698.391.91101.94100.341.91
225923-25923100.300102.31
324560-2456095.02796.91
425489-2548998.621100.57
525379-2537998.196100.19
625387-2538798.227100.15
20min125639-2563999.20297.461.29102.18100.401.28
225057-2505796.95099.96
324693-2469395.54198.38
425382-2538298.207101.14
525088-2508897.070100.04
625277-2527797.801100.71
30min125687-2568799.38797.771.94103.36101.681.93
225913-25913100.262104.24
324514-2451494.84998.64
425117-2511797.182101.10
525229-2522997.615101.56
625152-2515297.317101.20
极限125677-2567799.34998.201.55104.32103.091.54
225946-25946100.389105.37
325046-2504696.907101.65
424882-2488296.273101.16
525399-2539998.273103.19
625323-2532397.979102.84
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