叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.972484212478772477982484002480372481070.12
29.992479752479472479610.01
单位质量响应值RSD%判断
24885.3624820.920.19数据可信
供试品溶液-24111901批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min167299-6729944.45243.332.3644.4543.332.36
267049-6704944.28744.29
366126-6612643.67843.68
465491-6549143.25843.26
564285-6428542.46242.46
663380-6338041.86441.86
10min185469-8546956.45455.582.0656.9556.062.07
285777-8577756.65857.15
384786-8478656.00356.49
484655-8465555.91656.40
582884-8288454.74755.22
681267-8126753.67954.14
15min192577-9257761.14961.361.5962.2762.461.60
295370-9537062.99464.12
393037-9303761.45362.56
492917-9291761.37462.48
592701-9270161.23162.31
690751-9075159.94361.00
20min196486-9648663.73163.981.4865.5365.761.49
299083-9908365.44667.27
397100-9710064.13765.93
497191-9719164.19765.98
596665-9666563.84965.61
694646-9464662.51664.24
30min199066-9906665.43567.192.2667.9469.682.20
2101608-10160867.11469.66
3104747-10474769.18871.69
4103454-10345468.33470.83
5102309-10230967.57770.05
699119-9911965.47067.89
45min1101733-10173367.19768.782.4570.4372.012.40
2105279-10527969.53972.83
3107237-10723770.83274.10
4105842-10584269.91173.17
5104096-10409668.75871.98
6100548-10054866.41469.56
60min1102228-10222867.52469.181.8671.5173.181.82
2105592-10559269.74673.81
3105738-10573869.84273.90
4107096-10709670.73974.77
5105249-10524969.51973.50
6102503-10250367.70571.59
90min1102055-10205567.41069.772.9772.1474.542.87
2106295-10629570.21075.05
3109116-10911672.07376.91
4107995-10799571.33376.15
5106785-10678570.53475.29
6101544-10154467.07271.71
极限1104528-10452869.04370.591.7074.5276.141.64
2105418-10541869.63175.25
3109558-10955872.36578.00
4107500-10750071.00676.62
5107874-10787471.25376.79
6106387-10638770.27175.66
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.972498012505132502862504382503552502790.12
29.992490492493372491930.09
单位质量响应值RSD%判断
25103.2124944.240.45数据可信
供试品溶液-24111902批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min163501-6350141.65840.072.6841.6640.072.68
262430-6243040.95640.96
360956-6095639.98939.99
460338-6033839.58339.58
560339-6033939.58439.58
658950-5895038.67338.67
10min180973-8097353.12052.501.2853.5852.941.29
280761-8076152.98153.44
379989-7998952.47552.92
479687-7968752.27752.72
580550-8055052.84353.28
678179-7817951.28751.72
15min190945-9094559.66259.261.4060.7260.291.40
291939-9193960.31461.36
390484-9048459.36060.39
489158-8915858.49059.51
590919-9091959.64560.67
688549-8854958.09059.09
20min195736-9573662.80562.971.4064.5264.651.40
297897-9789764.22365.94
396575-9657563.35665.04
495516-9551662.66164.33
596311-9631163.18264.87
693844-9384461.56463.21
30min1100171-10017165.71566.522.1168.1368.912.07
2102769-10276967.41969.85
3103762-10376268.07070.46
4101566-10156666.63069.00
5102320-10232067.12469.52
697813-9781364.16866.50
45min1104787-10478768.74368.531.7471.8971.661.71
2105259-10525969.05272.23
3106357-10635769.77372.92
4101908-10190866.85469.96
5105891-10589169.46772.60
6102604-10260467.31170.35
60min1104765-10476568.72868.962.3372.6472.842.27
2109270-10927071.68475.63
3106531-10653169.88773.81
4103356-10335667.80471.65
5104218-10421868.37072.28
6102549-10254967.27571.06
90min1105991-10599169.53371.051.6374.2075.701.58
2110134-11013472.25176.99
3110635-11063572.57977.28
4107997-10799770.84975.45
5107578-10757870.57475.24
6107451-10745170.49075.03
极限1108609-10860971.25071.081.2876.6976.521.29
2110155-11015572.26477.81
3109089-10908971.56577.07
4108271-10827171.02876.42
5107977-10797770.83676.29
6106000-10600069.53974.86
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