厄贝沙坦氨氯地平片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100374-202105对照品来源中检院对照品使用方法左氨氯地平需分装，厄贝沙坦105℃烘干2小时
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数8000
标示量(mg)5供试品稀释倍数2系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.683273832810330613288132745328470.41
213.613303333109330710.17
单位质量响应值RSD%判断
2401.102429.900.85数据可信
供试品溶液-8145761批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min165665-6566585.82385.101.6485.8285.101.64
265555-6555585.67985.68
363077-6307782.44082.44
464870-6487084.78484.78
566033-6603386.30486.30
665482-6548285.58485.58
10min172908-7290895.28994.842.0895.7795.312.07
271725-7172593.74394.22
370838-7083892.58493.04
472272-7227294.45894.93
572350-7235094.56095.04
675280-7528098.38998.86
15min173108-7310895.55196.621.8296.5697.621.82
273318-7331895.82596.82
373196-7319695.66696.64
473720-7372096.35197.35
573586-7358696.17597.18
676632-76632100.156101.18
20min173508-7350896.07397.052.0897.6198.582.07
272736-7273695.06496.59
373633-7363396.23797.74
474339-7433997.16098.69
574127-7412796.88398.42
677178-77178100.870102.45
30min173904-7390496.59197.501.7898.6699.571.77
273429-7342995.97098.03
374053-7405396.78698.82
473925-7392596.61898.69
575273-7527398.380100.46
676991-76991100.626102.76
45min173670-7367096.28595.941.3498.8998.551.34
272566-7256694.84297.43
372586-7258694.86897.44
473033-7303395.45398.06
573375-7337595.90098.52
675192-7519298.274100.97
60min172809-7280995.16095.161.3098.3098.321.29
271164-7116493.01096.13
372759-7275995.09598.20
472687-7268795.00098.14
573885-7388596.56699.72
673571-7357196.15699.40
极限171715-7171593.73095.102.3097.4098.782.26
270711-7071192.41896.05
372670-7267094.97898.61
472378-7237894.59798.26
573548-7354896.12699.82
675564-7556498.761102.54
厄贝沙坦氨氯地平片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100374-202105对照品来源中检院对照品使用方法左氨氯地平需分装，厄贝沙坦105℃烘干2小时
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数8000
标示量(mg)5供试品稀释倍数2系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.683316733072332393310833150331470.20
213.613315333182331680.07
单位质量响应值RSD%判断
2423.032437.030.41数据可信
供试品溶液-8145761批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min157054-5705474.12175.002.8074.1275.012.80
255758-5575872.43772.44
360168-6016878.16678.17
459146-5914676.83876.84
557182-5718274.28774.29
657097-5709774.17674.18
10min171963-7196393.48993.382.7693.9093.802.76
269111-6911189.78490.19
375049-7504997.49897.93
472584-7258494.29694.72
570676-7067691.81792.23
671895-7189593.40193.81
15min177411-77411100.56798.033.26101.5098.973.25
272358-7235894.00294.90
377272-77272100.386101.36
478006-78006101.340102.29
572895-7289594.70095.62
674825-7482597.20798.14
20min177740-77740100.99499.243.23102.48100.723.21
273928-7392896.04297.47
377784-77784101.052102.59
479399-79399103.150104.66
573014-7301494.85596.30
676468-7646899.342100.81
30min176318-7631899.14798.462.36101.20100.502.37
273969-7396996.09598.05
376435-7643599.299101.39
478251-78251101.658103.75
573426-7342695.39097.37
676351-7635199.190101.21
45min177636-77636100.85998.352.68103.46100.932.66
274076-7407696.23498.73
375858-7585898.549101.20
478030-78030101.371104.02
572770-7277094.53897.04
675853-7585398.543101.12
60min177677-77677100.91398.262.21104.07101.392.21
274399-7439996.65499.68
375254-7525497.765100.96
477584-77584100.792104.01
573581-7358195.59198.62
675338-7533897.874101.00
极限175526-7552698.11897.241.96101.84100.901.97
273603-7360395.62099.18
375440-7544098.006101.74
476831-7683199.813103.59
572759-7275994.52398.09
674919-7491997.330100.99
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