叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.062498312502282499722501552505642501500.12
210.102497482503312500400.17
单位质量响应值RSD%判断
24865.8124756.440.32数据可信
供试品溶液-24120602批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min186877-8687757.48157.112.1557.4857.102.15
289051-8905158.92058.92
386937-8693757.52157.52
486488-8648857.22457.22
584679-8467956.02756.03
683820-8382055.45955.46
10min1111433-11143373.72972.781.0574.3773.421.05
2111073-11107373.49174.15
3110412-11041273.05373.69
4108898-10889872.05172.69
5109487-10948772.44173.06
6108687-10868771.91272.53
15min1121475-12147580.37377.781.8281.8379.221.80
2117619-11761977.82279.29
3117754-11775477.91179.36
4115987-11598776.74278.18
5117101-11710177.47978.91
6115390-11539076.34777.76
20min1126196-12619683.49779.782.5285.8582.092.48
2119507-11950779.07181.41
3121112-12111280.13382.45
4118750-11875078.57080.86
5120390-12039079.65581.94
6117507-11750777.74880.01
30min1125718-12571883.18079.832.2586.4683.022.23
2120409-12040979.66882.88
3120240-12024079.55682.76
4119060-11906078.77581.94
5120759-12075979.89983.07
6117752-11775277.91081.04
45min1127513-12751384.36880.822.4088.5784.902.36
2121511-12151180.39784.50
3121847-12184780.61984.71
4120512-12051279.73683.77
5122630-12263081.13785.20
6118909-11890978.67582.67
60min1129726-12972685.83279.873.8090.9784.853.67
2119160-11916078.84183.83
3119911-11991179.33884.32
4117221-11722177.55882.48
5120441-12044179.68984.65
6117857-11785777.97982.85
90min1128718-12871885.16579.114.0791.2684.973.94
2119195-11919578.86484.73
3118694-11869478.53384.40
4116073-11607376.79982.58
5119731-11973179.21985.07
6114958-11495876.06181.79
极限1130689-13068986.46979.364.5593.5186.114.37
2117564-11756477.78584.53
3117709-11770977.88184.62
4116161-11616176.85783.50
5120433-12043379.68486.41
6117120-11712077.49284.07
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数2000
标示量(mg)5供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.062492642491162493812497322495112494010.10
210.102495122507892501500.37
单位质量响应值RSD%判断
24791.3524767.330.07数据可信
供试品溶液-24120701批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min184487-8448755.97256.731.8655.9756.731.86
285945-8594556.93756.94
388465-8846558.60758.61
485128-8512856.39656.40
585803-8580356.84356.84
683946-8394655.61355.61
10min1109363-10936372.45272.311.3773.0772.941.37
2107945-10794571.51272.14
3111924-11192474.14874.80
4108966-10896672.18972.82
5108921-10892172.15972.79
6107792-10779271.41172.03
15min1115980-11598076.83576.751.5278.2678.181.52
2115738-11573876.67578.10
3119183-11918378.95780.43
4115121-11512176.26677.69
5114833-11483376.07577.51
6114216-11421675.66777.08
20min1116108-11610876.92077.901.6379.2080.181.62
2117483-11748377.83180.11
3121153-12115380.26282.61
4117756-11775678.01280.29
5117189-11718977.63679.91
6115810-11581076.72378.97
30min1114320-11432075.73677.581.9478.8780.721.92
2117464-11746477.81880.96
3120922-12092280.10983.35
4117208-11720877.64980.79
5117363-11736377.75280.89
6115305-11530576.38879.49
45min1116595-11659577.24378.661.8381.2282.681.81
2118299-11829978.37282.38
3122913-12291381.42885.56
4118601-11860178.57282.58
5118345-11834578.40282.41
6117676-11767677.95981.91
60min1115897-11589776.78079.082.8181.6283.962.74
2120707-12070779.96784.85
3124929-12492982.76487.80
4120051-12005179.53284.41
5118366-11836678.41683.29
6116220-11622076.99481.81
90min1117708-11770877.98078.511.9583.6784.281.94
2118899-11889978.76984.54
3122764-12276481.33087.29
4118192-11819278.30184.06
5117604-11760477.91183.66
6115911-11591176.79082.46
极限1115743-11574376.67877.732.0583.2384.372.03
2117707-11770777.97984.62
3121927-12192780.77587.64
4116388-11638877.10683.74
5116918-11691877.45784.07
6115339-11533976.41182.94
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