维格列汀片项目信息
介质体积(ml)1000取样体积(ml)1.5补液体积(ml)1.5
对照品批号101002-200701对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.052670132668892668682667732669032668890.04
29.982670122670312670220.01
单位质量响应值RSD%判断
26556.1226755.710.53数据可信
稳定性考察-中间条件36月-供试品溶液-S210101批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1266417-26641799.54882.1614.9099.5582.1614.90
2206046-20604676.99076.99
3240159-24015989.73789.74
4201077-20107775.13475.13
5231655-23165586.55986.56
6174013-17401365.02165.02
10min1268102-268102100.17899.771.41100.3399.891.42
2261896-26189697.85997.97
3272723-272723101.905102.04
4264033-26403398.65798.77
5267080-26708099.79699.93
6268179-268179100.207100.30
15min1268184-268184100.209100.131.29100.51100.401.29
2263797-26379798.56998.83
3273178-273178102.075102.36
4264986-26498699.01499.27
5267435-26743599.929100.21
6270306-270306101.001101.25
20min1267851-267851100.084100.091.32100.53100.511.32
2263766-26376698.55898.97
3273094-273094102.043102.48
4264645-26464598.88699.30
5267310-26731099.882100.31
6270515-270515101.080101.48
30min1267281-26728199.87199.891.24100.47100.471.25
2263619-26361998.50399.06
3272511-272511101.825102.42
4264251-26425198.73999.30
5266918-26691899.735100.31
6269458-269458100.685101.24
45min1266692-26669299.65199.671.22100.40100.391.23
2263202-26320298.34799.05
3271835-271835101.573102.32
4263828-26382898.58199.29
5265894-26589499.353100.08
6269012-269012100.518101.22
维格列汀片项目信息
介质体积(ml)1000取样体积(ml)1.5补液体积(ml)1.5
对照品批号101002-200701对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.052673432671302671282671482671662671830.04
29.982669662670122669890.02
单位质量响应值RSD%判断
26585.3726752.400.45数据可信
稳定性考察-中间条件36月-供试品溶液-S210102批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1234894-23489487.72693.084.5687.7393.084.56
2245813-24581391.80491.80
3242424-24242490.53990.54
4258926-25892696.70296.70
5247265-24726592.34792.35
6266062-26606299.36799.37
10min1263822-26382298.53096.833.3498.6696.973.34
2264261-26426198.69498.83
3244758-24475891.41091.55
4262598-26259898.07398.22
5252791-25279194.41094.55
6267368-26736899.855100.00
15min1263701-26370198.48596.773.3598.7697.063.34
2263935-26393598.57298.86
3244396-24439691.27591.55
4262342-26234297.97898.27
5253044-25304494.50594.79
6267266-26726699.817100.12
20min1262578-26257898.06696.623.3398.4997.053.32
2263342-26334298.35198.78
3244103-24410391.16691.58
4261991-26199197.84698.29
5252829-25282994.42594.85
6267323-26732399.838100.29
30min1263060-26306098.24696.463.3298.8297.033.31
2262811-26281198.15398.73
3243615-24361590.98491.53
4261432-26143297.63898.22
5252497-25249794.30194.86
6266258-26625899.440100.04
45min1263975-26397598.58796.453.3899.3197.173.38
2262454-26245498.01998.75
3243222-24322290.83791.52
4261253-26125397.57198.30
5252506-25250694.30495.01
6266164-26616499.405100.15
维格列汀片项目信息
介质体积(ml)1000取样体积(ml)1.5补液体积(ml)1.5
对照品批号101002-200701对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数200
标示量(mg)50供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.052438142442062436002434872432082436630.16
29.982431362428882430120.08
单位质量响应值RSD%判断
24245.0724349.900.31数据可信
稳定性考察-中间条件36月-供试品溶液-S210103批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1202289-20228982.92289.165.2282.9289.165.22
2230234-23023494.37894.38
3226317-22631792.77292.77
4219743-21974390.07790.08
5221269-22126990.70390.70
6205165-20516584.10184.10
10min1238349-23834997.70497.701.9297.8397.841.91
2243053-24305399.63299.77
3229853-22985394.22294.36
4240477-24047798.57798.71
5237818-23781897.48797.62
6240519-24051998.59498.72
15min1238838-23883897.90597.951.8798.1898.231.87
2241741-24174199.09599.39
3230208-23020894.36794.65
4242142-24214299.25999.54
5239737-23973798.27398.56
6241033-24103398.80499.08
20min1240232-24023298.47697.931.9998.8998.351.99
2241895-24189599.15899.60
3229396-22939694.03494.46
4239947-23994798.35998.79
5239834-23983498.31398.74
6242040-24204099.21799.64
30min1238822-23882297.89897.931.7898.4698.501.78
2241002-24100298.79299.38
3230525-23052594.49795.06
4240360-24036098.52999.11
5242170-24217099.27199.85
6240457-24045798.56899.14
45min1239644-23964498.23597.512.0798.9598.232.07
2241925-24192599.17099.91
3228166-22816693.53094.23
4238423-23842397.73598.46
5238798-23879897.88898.61
6240336-24033698.51999.24
点击查看处理图标(自动生成)
　
原始图谱下载图谱(谢超君 于 2024-03-14 16:12:54 完成)
生成报告数据部分(等待生成报告)
Current page cost:49 ms