辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.882649292644942641812643072641582644140.13
29.842647322645522646420.05
单位质量响应值RSD%判断
26762.5526894.510.35数据可信
供试品溶液-24121601批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min190620-9062033.71039.397.7133.7139.397.72
2102846-10284638.25838.26
3109950-10995040.90140.90
4109561-10956140.75640.76
5109569-10956940.75940.76
6112762-11276241.94741.95
10min1143337-14333753.32153.982.8353.4254.102.83
2139255-13925551.80251.92
3145754-14575454.22054.34
4144120-14412053.61253.73
5146552-14655254.51754.64
6151691-15169156.42856.55
15min1176568-17656865.68263.003.3865.9463.283.37
2161061-16106159.91460.18
3169106-16910662.90663.19
4165778-16577861.66861.95
5168820-16882062.80063.09
6174798-17479865.02465.32
20min1179027-17902766.59767.592.7167.0668.052.71
2174783-17478365.01865.47
3183762-18376268.35868.83
4180472-18047267.13567.60
5182693-18269367.96168.43
6189369-18936970.44470.93
30min1196955-19695573.26674.951.7973.9275.631.79
2203207-20320775.59276.24
3202805-20280575.44276.12
4198361-19836173.78974.46
5200741-20074174.67575.35
6206898-20689876.96577.67
45min1212505-21250579.05179.872.2079.9380.762.20
2207737-20773777.27778.15
3219180-21918081.53482.44
4213685-21368579.49080.38
5214318-21431879.72580.63
6220772-22077282.12683.06
60min1218304-21830481.20882.151.9782.3283.281.98
2213824-21382479.54180.64
3225085-22508583.73084.88
4220429-22042981.99883.13
5222183-22218382.65183.79
6225160-22516083.75884.94
极限1250335-25033593.12393.401.6794.4894.781.67
2243165-24316590.45691.80
3255188-25518894.92896.33
4251926-25192693.71595.09
5253082-25308294.14595.53
6252787-25278794.03595.47
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.882656002655392657132657422657322656650.04
29.842663042660142661590.08
单位质量响应值RSD%判断
26889.1727048.680.42数据可信
供试品溶液-24121601批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1196041-19604172.54773.721.7572.5573.721.75
2199526-19952673.83673.84
3200268-20026874.11174.11
4195063-19506372.18572.18
5204850-20485075.80775.81
6199439-19943973.80473.80
10min1228688-22868884.62884.951.2384.8585.171.23
2229999-22999985.11385.33
3231910-23191085.82086.04
4225552-22555283.46783.68
5233301-23330186.33586.56
6227878-22787884.32884.55
15min1238698-23869888.33288.851.2388.8089.321.23
2241731-24173189.45589.93
3242055-24205589.57590.05
4235906-23590687.29987.77
5243841-24384190.23690.72
6238355-23835588.20588.68
20min1242586-24258689.77190.611.2890.5191.351.28
2246803-24680391.33292.08
3247580-24758091.61992.37
4240661-24066189.05989.79
5248304-24830491.88792.64
6243137-24313789.97590.71
30min1245118-24511890.70891.441.0891.7192.451.08
2250975-25097592.87693.89
3246894-24689491.36592.39
4245063-24506390.68891.68
5249713-24971392.40893.44
6244833-24483390.60391.61
45min1253033-25303393.63792.262.5994.9293.552.57
2258249-25824995.56796.87
3250089-25008992.54893.85
4245126-24512690.71191.98
5249883-24988392.47193.78
6239512-23951288.63489.91
60min1247314-24731491.52193.842.9593.0895.402.92
2254116-25411694.03895.62
3259260-25926095.94197.52
4248567-24856791.98493.52
5265323-26532398.18599.77
6246879-24687991.36092.91
极限1258039-25803995.49096.491.0997.3298.331.09
2265457-26545798.235100.10
3260357-26035796.34798.21
4259045-25904595.86297.68
5262649-26264997.19699.08
6258845-25884595.78897.61
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.882681462682572680402677462673592679100.14
29.842676592671992674290.13
单位质量响应值RSD%判断
27116.4027177.740.16数据可信
供试品溶液-24121601批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1193419-19341971.10673.253.7471.1173.253.74
2188897-18889769.44469.44
3206390-20639075.87575.87
4197754-19775472.70072.70
5200813-20081373.82473.82
6208193-20819376.53776.54
10min1204180-20418075.06275.315.1075.2875.545.09
2202452-20245274.42774.64
3221319-22131981.36381.59
4192895-19289570.91471.13
5196320-19632072.17372.39
6212026-21202677.94778.18
15min1225560-22556082.92281.542.8583.3681.982.84
2216528-21652879.60280.03
3227813-22781383.75084.22
4213292-21329278.41278.84
5228250-22825083.91184.35
6219283-21928380.61481.08
20min1221078-22107881.27483.782.9381.9684.472.90
2227208-22720883.52884.20
3221158-22115881.30482.03
4229707-22970784.44785.11
5229148-22914884.24184.93
6239041-23904187.87888.58
30min1236988-23698887.12387.311.9788.0588.251.97
2231318-23131885.03985.96
3237301-23730187.23888.21
4234874-23487486.34687.27
5239148-23914887.91788.86
6245318-24531890.18691.15
45min1243619-24361989.56188.333.0590.7589.543.02
2226946-22694683.43284.61
3238429-23842987.65388.88
4240167-24016788.29289.47
5244950-24495090.05091.26
6247541-24754191.00392.24
60min1243017-24301789.34088.322.9690.8089.802.94
2226969-22696983.44084.87
3238880-23888087.81989.31
4240731-24073188.49989.94
5245328-24532890.18991.67
6246617-24661790.66392.18
极限1253256-25325693.10492.163.0694.8393.903.03
2236576-23657686.97288.65
3248448-24844891.33693.09
4253130-25313093.05894.77
5254079-25407993.40695.15
6258716-25871695.11196.90
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