叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.062421802435552434762431782428452430470.24
210.102422692435822429260.39
单位质量响应值RSD%判断
24159.7424052.080.32数据可信
供试品溶液-24121901批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min173078-7307849.76650.431.8349.7750.431.83
276479-7647952.08252.08
372736-7273649.53349.53
474497-7449750.73250.73
573428-7342850.00450.00
674113-7411350.47150.47
10min188688-8868860.39660.361.9860.9560.921.97
291506-9150662.31562.89
386239-8623958.72959.28
487575-8757559.63860.20
588983-8898360.59761.15
688774-8877460.45561.02
15min192256-9225662.82663.301.7064.0564.531.69
295116-9511664.77466.04
391153-9115362.07563.28
491636-9163662.40463.63
594436-9443664.31165.54
693136-9313663.42564.66
20min192652-9265263.09664.442.5965.0266.372.56
298637-9863767.17269.16
392273-9227362.83864.73
493020-9302063.34665.27
595466-9546665.01266.96
695689-9568965.16467.10
30min194538-9453864.38064.932.2467.0067.582.23
298904-9890467.35370.09
393063-9306363.37665.97
493576-9357663.72566.35
596384-9638465.63768.30
695614-9561465.11367.77
45min195362-9536264.94165.532.0168.2868.902.01
299207-9920767.56071.05
393822-9382263.89367.19
494885-9488564.61767.95
597140-9714066.15269.55
696924-9692466.00569.39
60min193384-9338463.59464.872.5067.6568.972.46
297800-9780066.60270.84
392819-9281963.21067.21
493215-9321563.47967.53
597832-9783266.62370.75
696524-9652465.73369.85
90min194528-9452864.37365.752.7469.1470.572.69
299563-9956367.80272.78
393139-9313963.42768.13
495158-9515864.80269.56
599171-9917167.53572.41
697721-9772166.54871.40
极限194957-9495764.66665.912.5870.1571.472.54
2100240-10024068.26373.99
393476-9347663.65769.07
495922-9592265.32370.80
598686-9868667.20572.83
697461-9746166.37171.96
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.062410772424242422862423132424332421070.24
210.102404892417602411240.38
单位质量响应值RSD%判断
24066.3023873.660.57数据可信
供试品溶液-24121902批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min174793-7479351.22355.003.5851.2255.003.58
281228-8122855.63055.63
381174-8117455.59355.59
479934-7993454.74454.74
581768-8176856.00056.00
682937-8293756.80156.80
10min191790-9179062.86465.362.0363.4365.972.04
296994-9699466.42867.05
394848-9484864.95865.58
496602-9660266.16066.77
596422-9642266.03666.66
695964-9596465.72366.35
15min197206-9720666.57369.042.2267.8470.382.23
2103261-10326170.72072.08
3100210-10021068.63169.97
4100265-10026568.66870.01
5103123-10312370.62671.98
6100796-10079669.03270.39
20min198658-9865867.56870.192.1169.5872.292.11
2105242-10524272.07774.22
3101995-10199569.85371.96
4102989-10298970.53472.64
5102992-10299270.53672.68
6103007-10300770.54672.67
30min1100272-10027268.67371.562.3771.4374.442.36
2107629-10762973.71276.65
3103773-10377371.07173.95
4104292-10429271.42674.32
5105880-10588072.51475.44
6105057-10505771.95074.86
45min1101076-10107669.22472.362.3372.7476.042.33
2107596-10759673.68977.45
3104684-10468471.69575.36
4107150-10715073.38477.07
5106702-10670273.07776.81
6106750-10675073.11076.82
60min1103007-10300770.54672.801.9774.8477.291.98
2109351-10935174.89179.47
3105411-10541172.19376.66
4106670-10667073.05577.55
5107185-10718573.40877.95
6106192-10619272.72777.25
90min1104136-10413671.31973.752.3176.3979.042.29
2111270-11127076.20581.62
3106125-10612572.68277.95
4108621-10862174.39179.70
5108949-10894974.61679.97
6106973-10697373.26278.59
极限1103826-10382671.10774.272.5476.9780.382.51
2111900-11190076.63782.90
3107764-10776473.80479.88
4109594-10959475.05781.19
5109894-10989475.26381.45
6107718-10771873.77379.92
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.062407122418582417792416552420042416020.22
210.102395302405002400150.29
单位质量响应值RSD%判断
24016.1023763.860.75数据可信
供试品溶液-24121903批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min181942-8194256.30854.043.3056.3154.043.30
279145-7914554.38654.39
378784-7878454.13854.14
479787-7978754.82754.83
574090-7409050.91250.91
678108-7810853.67353.67
10min198498-9849867.68564.884.2168.3165.484.20
297009-9700966.66267.27
394787-9478765.13565.74
496403-9640366.24566.85
587623-8762360.21260.78
692139-9213963.31563.91
15min1103142-10314270.87668.235.2072.2569.545.17
2103994-10399471.46172.81
3100744-10074469.22870.55
4100557-10055769.10070.44
589853-8985361.74462.98
697421-9742166.94568.24
20min1105980-10598072.82669.665.4574.9971.745.41
2105975-10597572.82374.96
3102350-10235070.33272.43
4102566-10256670.48072.59
591047-9104762.56564.49
6100297-10029768.92170.96
30min1108891-10889174.82771.145.9377.8073.995.88
2107586-10758673.93076.88
3105888-10588872.76375.64
4105134-10513472.24575.14
592079-9207963.27465.89
6101565-10156569.79272.60
45min1109450-10945075.21171.476.3479.0275.126.26
2109143-10914375.00078.77
3105946-10594672.80376.49
4105951-10595172.80676.51
591838-9183863.10866.43
6101742-10174269.91473.50
60min1108161-10816174.32571.195.9778.9775.635.91
2108331-10833174.44279.04
3105475-10547572.47976.97
4104615-10461571.88876.40
591642-9164262.97466.99
6103394-10339471.04975.41
90min1112209-11220977.10771.696.8982.5776.926.78
2109720-10972075.39680.83
3105800-10580072.70278.00
4104993-10499372.14877.45
591855-9185563.12067.84
6101360-10136069.65174.80
极限1110764-11076476.11472.076.1582.4478.106.10
2110683-11068376.05882.33
3106416-10641673.12679.23
4105566-10556672.54278.65
593447-9344764.21469.64
6102416-10241670.37776.30
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