叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.062391402403542406872405832401322401790.26
210.102393962411562402760.52
单位质量响应值RSD%判断
23874.6523789.700.26数据可信
供试品溶液-AM222092批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min144681-4468130.77730.612.1430.7830.612.15
245250-4525031.16931.17
343399-4339929.89429.89
10min171763-7176349.43247.613.6849.7747.953.66
268879-6887947.44547.79
366704-6670445.94746.28
15min191510-9151063.03462.721.0263.9363.591.05
291659-9165963.13664.01
389982-8998261.98162.82
20min1108556-10855674.77573.871.0776.3775.431.08
2106523-10652373.37574.95
3106632-10663273.45074.98
30min1127435-12743587.78086.741.1190.2089.121.12
2125652-12565286.55188.94
3124688-12468885.88788.23
45min1138486-13848695.39293.702.3698.7997.052.28
2132407-13240791.20494.56
3137176-13717694.48997.79
60min1138470-13847095.38196.250.7999.84100.650.70
2140474-14047496.761101.13
3140268-14026896.619100.97
90min1142329-14232998.03998.570.50103.56104.030.43
2143716-14371698.994104.43
3143263-14326398.682104.11
极限1140283-14028396.63096.911.19103.24103.471.12
2142532-14253298.179104.72
3139272-13927295.933102.45
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.062393572406062408802407442403792403930.26
210.102388762402262395510.40
单位质量响应值RSD%判断
23895.9223717.920.53数据可信
供试品溶液-AM222092批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min133012-3301222.76422.682.0122.7622.682.01
232187-3218722.19522.19
333492-3349223.09523.09
10min154415-5441537.52236.362.7837.7836.612.77
251847-5184735.75136.00
351918-5191835.80036.06
15min176012-7601252.41550.263.7553.0850.913.72
271599-7159949.37250.02
371032-7103248.98149.63
20min188571-8857161.07559.682.0562.3360.892.07
285299-8529958.81960.01
385774-8577459.14660.34
30min1109007-10900775.16773.961.6977.1075.841.69
2107368-10736874.03675.88
3105406-10540672.68374.54
45min1126076-12607686.93784.552.4589.7087.252.44
2120911-12091183.37586.04
3120871-12087183.34786.01
60min1130090-13009089.70491.085.2593.4494.725.03
2139779-13977996.38699.98
3126371-12637187.14090.73
90min1135936-13593693.73692.021.7198.4696.671.67
2131476-13147690.66095.33
3132913-13291391.65196.21
极限1133260-13326091.89090.961.3097.6696.641.24
2130002-13000289.64495.32
3132488-13248891.35896.93
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