贝派度酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号BEMA-231010D对照品来源自制对照品使用方法直接使用
对照品含量(%)99.72对照品水分(%)0对照品稀释倍数50
标示量(mg)180供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.193045873047893048323044523043783046080.07
210.213074933051073063000.56
单位质量响应值RSD%判断
29892.8430000.000.26数据可信
供试品溶液-24121801批-pH4.5(内含0.45%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min140014-4001426.64926.415.1226.6526.415.12
240712-4071227.11427.11
337601-3760125.04225.04
437051-3705124.67624.68
540058-4005826.67826.68
642520-4252028.31828.32
10min176225-7622550.76551.954.3351.0652.244.33
278816-7881652.49152.79
379125-7912552.69752.97
472147-7214748.04948.32
580053-8005353.31553.61
681654-8165454.38154.70
15min196216-9621664.07964.632.8364.9465.502.84
299248-9924866.09866.98
397728-9772865.08665.95
491887-9188761.19662.00
598574-9857465.64966.54
698651-9865165.70166.62
20min1103166-10316668.70871.743.1270.2873.333.11
2110451-11045173.55975.18
3108820-10882072.47374.06
4103925-10392569.21370.70
5111038-11103873.95075.57
6108892-10889272.52174.17
30min1121598-12159880.98381.221.8883.3283.601.90
2122233-12223381.40683.84
3122377-12237781.50283.89
4118176-11817678.70480.96
5122019-12201981.26483.70
6125329-12532983.46885.92
45min1127768-12776885.09287.741.6488.3391.031.60
2131689-13168987.70491.04
3131211-13121187.38590.68
4133134-13313488.66691.80
5133238-13323888.73592.08
6133416-13341688.85492.24
60min1135206-13520690.04691.011.9494.2395.271.86
2136028-13602890.59494.91
3139236-13923692.73097.00
4135818-13581890.45494.57
5140356-14035693.47697.80
6133275-13327588.76093.13
极限1144929-14492996.52295.591.76101.70100.861.68
2142174-14217494.687100.01
3145408-14540896.841102.14
4141949-14194994.53799.66
5146662-14666297.676103.04
6140031-14003193.25998.62
贝派度酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号BEMA-231010D对照品来源自制对照品使用方法直接使用
对照品含量(%)99.72对照品水分(%)0对照品稀释倍数50
标示量(mg)180供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.193049323045783046173044553046903046540.06
210.213059183042573050880.39
单位质量响应值RSD%判断
29897.3529881.290.04数据可信
供试品溶液-24121802批-pH4.5(内含0.45%SDS)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min137730-3773025.17627.946.0325.1827.946.03
243277-4327728.87728.88
340074-4007426.74026.74
442689-4268928.48528.48
542803-4280328.56128.56
644697-4469729.82529.82
10min176452-7645251.01354.913.8051.2955.223.80
282628-8262855.13555.46
384586-8458656.44156.74
481479-8147954.36854.68
583875-8387555.96756.28
684765-8476556.56056.89
15min198420-9842065.67268.222.4166.5269.142.42
2104604-10460469.79870.73
3103038-10303868.75369.68
4100014-10001466.73667.66
5104037-10403769.42070.36
6103311-10331168.93569.90
20min1108170-10817072.17877.393.7173.7579.073.69
2117072-11707278.11879.83
3118159-11815978.84380.53
4115035-11503576.75878.42
5120885-12088580.66282.37
6116579-11657977.78979.51
30min1128274-12827485.59286.491.0387.9789.021.07
2130006-13000686.74889.33
3130707-13070787.21689.78
4127787-12778785.26787.78
5131136-13113687.50290.11
6129774-12977486.59389.18
45min1136127-13612790.83293.171.6194.1696.671.64
2139331-13933192.97096.51
3140335-14033593.64097.17
4138606-13860692.48695.95
5142871-14287195.33298.91
6140538-14053893.77697.33
60min1142434-14243495.04196.001.0699.38100.531.07
2143892-14389296.014100.59
3146673-14667397.869102.44
4142658-14265895.19099.68
5143872-14387296.000100.64
6143674-14367495.868100.46
极限1143461-14346195.72696.401.39101.12102.001.35
2141394-14139494.34799.99
3143601-14360195.819101.48
4145918-14591897.366102.91
5146796-14679697.951103.66
6145614-14561497.163102.82
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