辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.892647372644222643552648522647822646300.09
29.922644892644642644760.01
单位质量响应值RSD%判断
26757.3326660.890.26数据可信
供试品溶液-24122301批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1141126-14112652.73347.925.4852.7347.925.48
2127733-12773347.72847.73
3126582-12658247.29847.30
4128807-12880748.13048.13
5120021-12002144.84744.85
6125142-12514246.76046.76
10min1163049-16304960.92458.913.1261.0859.053.12
2159241-15924159.50159.64
3158707-15870759.30259.44
4159732-15973259.68559.83
5148565-14856555.51255.65
6156679-15667958.54458.68
15min1181520-18152067.82665.483.2368.1765.803.23
2177615-17761566.36766.69
3175912-17591265.73166.05
4177133-17713366.18766.51
5164741-16474161.55761.86
6174465-17446565.19065.51
20min1192425-19242571.90169.733.1372.4570.253.13
2188978-18897870.61371.13
3187963-18796370.23470.75
4189110-18911070.66271.18
5175572-17557265.60466.09
6185715-18571569.39469.91
30min1206844-20684477.28975.493.3378.0576.223.33
2202773-20277375.76776.50
3202984-20298475.84676.57
4203338-20333875.97976.71
5188936-18893670.59771.28
6207299-20729977.45978.18
45min1217640-21764081.32379.203.0682.3180.163.06
2213619-21361979.82080.78
3214690-21469080.22081.18
4214847-21484780.27981.24
5199373-19937374.49775.39
6211621-21162179.07480.03
60min1222200-22220083.02681.013.0284.2682.203.03
2217894-21789481.41882.62
3220214-22021482.28483.48
4220373-22037382.34483.55
5204215-20421576.30677.42
6215894-21589480.67081.86
极限1246230-24623092.00591.081.6993.4992.511.71
2244815-24481591.47792.92
3245540-24554091.74893.19
4246242-24624292.01093.46
5235515-23551588.00289.35
6244170-24417091.23692.67
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.892671632671562672352665562665992669420.13
29.922646512648152647330.05
单位质量响应值RSD%判断
26991.1026686.790.81数据可信
供试品溶液-24122302批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min196730-9673035.97036.451.2135.9736.451.21
299777-9977737.10337.10
397241-9724136.16036.16
497203-9720336.14636.15
599009-9900936.81736.82
698139-9813936.49436.49
10min1123118-12311845.78345.981.1545.8946.091.15
2124763-12476346.39446.51
3124128-12412846.15846.27
4123686-12368645.99446.10
5125028-12502846.49346.60
6121126-12112645.04245.15
15min1139481-13948151.86752.211.6552.1152.461.65
2144345-14434553.67653.93
3138682-13868251.57051.82
4140165-14016552.12252.37
5141699-14169952.69252.94
6138014-13801451.32251.57
20min1149820-14982055.71256.080.7456.1156.480.74
2151747-15174756.42956.84
3149751-14975155.68656.09
4151342-15134256.27856.68
5152251-15225156.61657.02
6149954-14995455.76256.16
30min1165849-16584961.67361.740.6062.2462.310.59
2166347-16634761.85862.44
3164710-16471061.24961.82
4167513-16751362.29162.86
5166448-16644861.89562.47
6165269-16526961.45762.02
45min1179351-17935166.69367.382.2367.4568.142.20
2179626-17962666.79667.56
3177344-17734465.94766.70
4188956-18895670.26571.02
5180666-18066667.18267.95
6181272-18127267.40868.16
60min1186398-18639869.31469.420.7870.2770.380.78
2186347-18634769.29570.26
3184428-18442868.58169.53
4188557-18855770.11771.09
5186376-18637669.30670.27
6187984-18798469.90470.86
极限1224811-22481183.59883.760.8484.7684.920.83
2225753-22575383.94885.12
3224872-22487283.62184.78
4227907-22790784.74985.93
5222184-22218482.62183.79
6225915-22591584.00985.17
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.892642862640872637772636512631332637870.17
29.922644522643582644050.03
单位质量响应值RSD%判断
26672.0926653.730.05数据可信
供试品溶液-24122303批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1113650-11365042.54041.783.9242.5441.783.92
2118183-11818344.23644.24
3112594-11259442.14442.14
4111093-11109341.58241.58
5105322-10532239.42239.42
6108931-10893140.77340.77
10min1138967-13896752.01652.394.0952.1452.524.08
2146040-14604054.66354.80
3136116-13611650.94951.08
4136548-13654851.11051.24
5148005-14800555.39955.52
6134072-13407250.18450.31
15min1158875-15887559.46758.474.2759.7558.754.26
2166197-16619762.20862.50
3156345-15634558.52058.80
4157005-15700558.76759.05
5146082-14608254.67954.96
6152779-15277957.18657.46
20min1168273-16827362.98562.933.0163.4563.383.01
2175421-17542165.66166.14
3168348-16834863.01363.47
4171063-17106364.02964.48
5160653-16065360.13360.58
6164962-16496261.74662.19
30min1183410-18341068.65169.063.9469.3069.713.93
2195357-19535773.12373.80
3185776-18577669.53670.18
4188303-18830370.48271.13
5173991-17399165.12565.75
6180264-18026467.47368.10
45min1201696-20169675.49574.853.7276.3575.703.70
2208209-20820977.93378.83
3199761-19976174.77175.62
4206566-20656677.31878.18
5188089-18808970.40271.23
6195538-19553873.19074.02
60min1210080-21008078.63477.762.8579.7278.842.85
2215487-21548780.65781.79
3205935-20593577.08278.16
4212219-21221979.43480.52
5199758-19975874.77075.81
6202994-20299475.98177.03
极限1232769-23276987.12688.332.0788.4589.642.08
2243372-24337291.09592.47
3232793-23279387.13588.44
4239518-23951889.65290.98
5230467-23046786.26487.52
6237044-23704488.72690.01
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