叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.062464432460442455992459552453772458840.17
210.102462432461752462090.02
单位质量响应值RSD%判断
24441.7524377.130.19数据可信
供试品溶液-24122401批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min170431-7043147.36746.582.7447.3746.582.74
271225-7122547.90147.90
367719-6771945.54345.54
471089-7108947.80947.81
566760-6676044.89844.90
668362-6836245.97545.98
10min1102096-10209668.66268.540.3069.1969.060.30
2102303-10230368.80269.33
3101705-10170568.39968.91
4101748-10174868.42868.96
5102109-10210968.67169.17
6101518-10151868.27468.78
15min1116093-11609378.07677.261.2179.3678.541.18
2113306-11330676.20177.50
3115613-11561377.75379.02
4113924-11392476.61777.91
5113763-11376376.50977.77
6116590-11659078.41079.68
20min1120465-12046581.01681.181.7883.1783.321.73
2118908-11890879.96982.11
3124388-12438883.65485.78
4119031-11903180.05282.19
5119466-11946680.34482.46
6122001-12200182.04984.19
30min1124136-12413683.48583.110.9586.5486.140.93
2122330-12233082.27085.30
3124081-12408183.44886.51
4121857-12185781.95284.98
5124393-12439383.65886.66
6124645-12464583.82786.88
45min1126136-12613684.83085.291.0488.8189.260.99
2124879-12487983.98587.93
3126922-12692285.35989.35
4126486-12648685.06589.01
5128379-12837986.33890.27
6128152-12815286.18690.17
60min1124903-12490384.00184.321.2988.9389.231.23
2122824-12282482.60387.48
3124761-12476183.90588.84
4127257-12725785.58490.47
5125599-12559984.46989.36
6126886-12688685.33490.28
90min1125636-12563684.49484.981.1990.3590.821.13
2123810-12381083.26689.06
3127747-12774785.91391.78
4127809-12780985.95591.79
5126727-12672785.22791.06
6126422-12642285.02290.91
极限1125308-12530884.27384.781.7891.0791.571.68
2122344-12234482.28089.00
3126102-12610284.80791.63
4129159-12915986.86393.66
5127043-12704385.44092.22
6126398-12639885.00691.84
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.062464012458732458712460392459762460320.09
210.102442022447202444610.15
单位质量响应值RSD%判断
24456.4624204.060.74数据可信
供试品溶液-24122402批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min173496-7349649.59046.804.6649.5946.804.66
271790-7179048.43948.44
369969-6996947.21047.21
468148-6814845.98245.98
564207-6420743.32343.32
668551-6855146.25446.25
10min1106433-10643371.81469.413.7272.3669.923.72
2103117-10311769.57670.11
3107077-10707772.24872.77
498901-9890166.73267.24
597785-9778565.97966.46
6103867-10386770.08370.60
15min1121256-12125681.81578.663.4783.1679.953.47
2115768-11576878.11379.42
3121306-12130681.84983.18
4111028-11102874.91476.17
5114250-11425077.08878.30
6115833-11583378.15679.45
20min1125653-12565384.78282.303.3487.0484.473.33
2120608-12060881.37883.56
3126929-12692985.64387.88
4115619-11561978.01280.10
5120501-12050181.30683.38
6122562-12256282.69784.86
30min1128436-12843686.66085.233.0089.8688.313.00
2126061-12606185.05888.14
3130925-13092588.33991.53
4119872-11987280.88283.83
5124881-12488184.26187.24
6127719-12771986.17689.26
45min1130814-13081488.26586.632.7392.4390.662.74
2127799-12779986.23090.26
3132525-13252589.41993.59
4122300-12230082.52086.37
5127843-12784386.26090.17
6129102-12910287.10991.15
60min1130035-13003587.73985.912.1392.8890.902.18
2126763-12676385.53190.52
3130504-13050488.05593.22
4123703-12370383.46788.23
5125021-12502184.35689.22
6127917-12791786.31091.32
90min1128602-12860286.77286.032.8592.8991.982.83
2127129-12712985.77891.72
3131726-13172688.88095.02
4120815-12081581.51887.21
5127955-12795586.33692.14
6128801-12880186.90692.87
极限1128515-12851586.71385.483.1893.8092.383.13
2125724-12572484.83091.72
3130502-13050288.05495.18
4119201-11920180.42987.03
5127114-12711485.76892.53
6129077-12907787.09394.02
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