坎地沙坦酯片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100685-201903对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数2000
标示量(mg)8供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.063738853738463741233737913735533738400.06
216.073725113721013723060.08
单位质量响应值RSD%判断
23277.7123167.770.34数据可信
供试品溶液-24122001批-pH4.5(内含1%Tween80)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min17421-74211.7941.889.071.791.889.11
28025-80251.9401.94
38437-84372.0402.04
46498-64981.5711.57
58095-80951.9571.96
68120-81201.9631.96
10min128835-288356.9707.288.846.977.288.82
229713-297137.1837.19
332209-322097.7867.79
425699-256996.2126.22
533046-330467.9887.99
631179-311797.5377.54
15min158163-5816314.06014.497.0414.0714.507.03
260300-6030014.57714.59
363400-6340015.32615.34
452343-5234312.65312.67
563263-6326315.29315.31
662159-6215915.02615.04
20min190471-9047121.87022.296.2421.9122.326.25
292680-9268022.40422.44
396417-9641723.30823.35
481572-8157219.71919.75
597116-9711623.47623.52
694875-9487522.93522.98
30min1146480-14648035.41035.533.6235.4835.613.63
2147047-14704735.54735.62
3150928-15092836.48536.57
4136902-13690233.09433.16
5151278-15127836.56936.65
6149241-14924136.07736.16
45min1209462-20946250.63550.442.3750.7750.572.38
2207936-20793650.26650.40
3211439-21143951.11351.25
4199255-19925548.16748.29
5213294-21329451.56151.70
6210500-21050050.88651.02
60min1253103-25310361.18460.691.7461.4060.901.75
2249642-24964260.34860.57
3254452-25445261.51061.74
4242859-24285958.70858.91
5253959-25395961.39161.62
6252216-25221660.97061.19
极限1279002-27900267.44566.701.3567.7667.021.36
2273878-27387866.20666.53
3278311-27831167.27867.61
4269549-26954965.16065.46
5278895-27889567.41967.75
6275852-27585266.68367.01
坎地沙坦酯片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100685-201903对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数2000
标示量(mg)8供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.063733553724553727053728713731053728980.10
216.073738633741143739880.05
单位质量响应值RSD%判断
23219.0523272.430.17数据可信
供试品溶液-24122401批-pH4.5(内含1%Tween80)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min111022-110222.6623.058.642.663.058.63
213742-137423.3193.32
313850-138503.3453.34
412151-121512.9342.93
512072-120722.9152.92
612921-129213.1203.12
10min143930-4393010.60911.015.0010.6111.015.02
247998-4799811.59111.60
348923-4892311.81511.82
444083-4408310.64610.65
543797-4379710.57710.58
644697-4469710.79410.80
15min183973-8397320.27920.045.1320.3020.065.13
287721-8772121.18421.21
388074-8807421.27021.29
479512-7951219.20219.22
578464-7846418.94918.97
680051-8005119.33219.36
20min1118740-11874028.67528.074.1828.7328.134.18
2121767-12176729.40629.47
3120818-12081829.17729.24
4112326-11232627.12627.18
5110006-11000626.56626.62
6113834-11383427.49027.55
30min1174184-17418442.06541.542.8942.1741.652.89
2179331-17933143.30843.42
3173951-17395142.00842.12
4171616-17161641.44541.54
5165966-16596640.08040.18
6167096-16709640.35340.45
45min1241024-24102458.20656.942.1258.3857.122.12
2239473-23947357.83258.01
3239968-23996857.95158.13
4232093-23209356.05056.22
5229061-22906155.31755.48
6233133-23313356.30156.47
60min1282612-28261268.25067.201.3868.5267.461.38
2281045-28104567.87168.15
3280621-28062167.76968.04
4275363-27536366.49966.76
5272687-27268765.85366.11
6277206-27720666.94467.21
极限1319649-31964977.19474.402.0777.5874.782.07
2308966-30896674.61475.00
3309331-30933174.70275.09
4304116-30411673.44373.82
5302247-30224772.99173.36
6304052-30405273.42773.80
坎地沙坦酯片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100685-201903对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数2000
标示量(mg)8供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.063725223731613725723728853727023727680.07
216.073724493726253725370.04
单位质量响应值RSD%判断
23210.9623182.140.09数据可信
供试品溶液-24122002批-pH4.5(内含1%Tween80)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min115436-154363.7364.0210.213.744.0210.19
219304-193044.6724.67
317430-174304.2184.22
416814-168144.0694.07
516156-161563.9103.91
614424-144243.4913.49
10min148859-4885911.82412.427.1111.8312.437.12
258143-5814314.07114.08
351814-5181412.53912.55
448044-4804411.62711.63
551479-5147912.45812.46
649601-4960112.00412.01
15min185901-8590120.78921.694.8820.8121.714.90
296792-9679223.42423.46
391963-9196322.25622.28
485358-8535820.65720.68
590483-9048321.89821.92
687191-8719121.10121.13
20min1120023-12002329.04729.933.1229.1130.003.12
2129803-12980331.41331.48
3122484-12248429.64229.71
4120156-12015629.07929.14
5126695-12669530.66130.72
6122924-12292429.74929.81
30min1176909-17690942.81344.702.6442.9244.822.65
2190469-19046946.09546.22
3183699-18369944.45744.57
4182936-18293644.27244.38
5189224-18922445.79445.91
6185110-18511044.79844.91
45min1242428-24242858.67059.451.1958.8559.641.19
2246416-24641659.63559.83
3244157-24415759.08859.28
4243877-24387759.02059.20
5250729-25072960.67860.87
6246233-24623359.59059.78
60min1283526-28352668.61669.241.0268.8969.531.02
2285346-28534669.05669.35
3284068-28406868.74769.03
4284682-28468268.89569.18
5291133-29113370.45770.75
6287924-28792469.68069.96
极限1307241-30724174.35574.711.0074.7575.111.00
2307123-30712374.32674.74
3306361-30636174.14274.54
4306353-30635374.14074.54
5313595-31359575.89376.30
6311516-31151675.38975.79
坎地沙坦酯片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100685-201903对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数2000
标示量(mg)8供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
116.063720373726353726513723873721483723720.08
216.073744763745433745100.02
单位质量响应值RSD%判断
23186.3023304.920.37数据可信
供试品溶液-24122402批-pH4.5(内含1%Tween80)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min115851-158513.8283.3710.263.833.3710.26
211941-119412.8842.88
313574-135743.2783.28
413705-137053.3103.31
513356-133563.2253.23
615383-153833.7153.71
10min150009-5000912.07710.856.9612.0810.866.93
240792-407929.8519.86
345530-4553010.99511.00
445329-4532910.94710.95
542654-4265410.30110.31
645366-4536610.95610.96
15min186647-8664720.92519.616.3820.9519.646.39
273885-7388517.84317.86
386386-8638620.86220.89
481307-8130719.63619.66
576497-7649718.47418.50
682577-8257719.94219.97
20min1119531-11953128.86727.324.2128.9327.384.20
2106397-10639725.69525.75
3113562-11356227.42527.48
4114312-11431227.60627.66
5108997-10899726.32326.38
6115969-11596928.00628.06
30min1173097-17309741.80340.432.2041.9140.532.20
2163127-16312739.39539.49
3166783-16678340.27840.38
4167706-16770640.50140.60
5164053-16405339.61939.72
6169656-16965640.97241.08
45min1231574-23157455.92554.751.6356.1054.921.63
2221432-22143253.47653.64
3226478-22647854.69454.87
4227651-22765154.97755.15
5223786-22378654.04454.21
6229368-22936855.39255.56
60min1270856-27085665.41164.361.5065.6864.621.51
2261808-26180863.22663.47
3266516-26651664.36364.63
4265059-26505964.01164.27
5263228-26322863.56963.82
6271565-27156565.58365.85
极限1292579-29257970.65770.071.3371.0470.441.33
2289140-28914069.82770.18
3290316-29031670.11170.48
4286540-28654069.19969.57
5286109-28610969.09569.45
6296293-29629371.55471.93
点击查看处理图标(人工保存)
　
原始图谱下载图谱(谢超君 于 2024-12-30 15:14:44 完成)
生成报告数据部分下载报告(谢超君 于 2024-12-30 15:15:03 完成)
Current page cost:102 ms