叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.062467162468012464002460072455332462910.22
210.102476592476462476520.01
单位质量响应值RSD%判断
24482.2124520.000.11数据可信
供试品溶液-24122701批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min162310-6231041.74842.301.4341.7542.301.43
263064-6306442.25442.25
364420-6442043.16243.16
463985-6398542.87142.87
562891-6289142.13842.14
662173-6217341.65741.66
10min191691-9169161.43461.590.7561.9062.060.75
292196-9219661.77262.24
391937-9193761.59962.08
492145-9214561.73862.21
592816-9281662.18862.66
690754-9075460.80661.27
15min1104988-10498870.34370.591.1171.4971.751.11
2105942-10594270.98272.14
3105366-10536670.59671.76
4106960-10696071.66472.83
5105470-10547070.66671.83
6103413-10341369.28870.43
20min1111167-11116774.48375.301.0176.4177.241.00
2112400-11240075.30977.25
3111887-11188774.96676.91
4114520-11452076.73078.69
5112167-11216775.15377.10
6112207-11220775.18077.09
30min1114701-11470176.85179.091.9379.6181.861.88
2117356-11735678.63081.41
3117702-11770278.86281.64
4121728-12172881.55984.37
5118712-11871279.53882.32
6118025-11802579.07881.82
45min1116942-11694278.35280.052.0581.9683.702.00
2120217-12021780.54784.20
3117900-11790078.99482.65
4123923-12392383.03086.75
5118830-11883079.61783.28
6119016-11901679.74283.36
60min1118962-11896279.70681.222.3684.1985.772.30
2120507-12050780.74185.29
3120214-12021480.54585.08
4126888-12688885.01689.66
5120945-12094581.03485.58
6119835-11983580.29184.80
90min1117856-11785678.96581.712.9784.3387.162.87
2121837-12183781.63287.08
3121652-12165281.50886.94
4128599-12859986.16391.75
5121872-12187281.65687.10
6119898-11989880.33385.73
极限1120281-12028180.59083.013.3486.8389.363.22
2123832-12383282.96989.32
3122583-12258382.13288.47
4131933-13193388.39794.94
5123144-12314482.50888.86
6121569-12156981.45387.75
叶酸片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100074-202217对照品来源中检院对照品使用方法直接使用
对照品含量(%)91.2对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数2系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.062467642469292467972469332468122468470.04
210.102469462470762470110.04
单位质量响应值RSD%判断
24537.4824456.530.24数据可信
供试品溶液-24122703批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min171277-7127747.76445.682.8347.7645.682.83
268802-6880246.10646.11
365616-6561643.97143.97
468258-6825845.74145.74
568276-6827645.75345.75
666761-6676144.73844.74
10min1102839-10283968.91569.040.6569.4569.550.65
2103601-10360169.42669.94
3102915-10291568.96669.45
4103843-10384369.58870.10
5102989-10298969.01569.52
6101961-10196168.32768.82
15min1115842-11584277.62977.950.9278.9379.220.92
2117146-11714678.50279.79
3115523-11552377.41578.67
4117784-11778478.93080.21
5116670-11667078.18379.46
6114953-11495377.03378.29
20min1122743-12274382.25381.980.9284.4184.120.92
2122673-12267382.20684.36
3121335-12133581.31083.42
4124250-12425083.26385.42
5121523-12152381.43683.58
6121501-12150181.42183.53
30min1126465-12646584.74785.220.6887.8288.270.67
2126841-12684184.99988.07
3127704-12770485.57888.60
4128654-12865486.21489.30
5126423-12642384.71987.77
6126917-12691785.05088.07
45min1128515-12851586.12185.840.7990.1489.840.79
2128903-12890386.38190.39
3127272-12727285.28889.26
4129489-12948986.77490.82
5127084-12708485.16289.15
6127351-12735185.34189.30
60min1129257-12925786.61885.920.9791.5990.880.95
2128524-12852486.12791.10
3126616-12661684.84889.77
4129536-12953686.80591.81
5126785-12678584.96289.90
6128609-12860986.18491.09
90min1128284-12828485.96685.541.4891.9091.451.41
2126180-12618084.55690.49
3125695-12569584.23190.09
4130295-13029587.31493.28
5126268-12626884.61590.50
6129204-12920486.58392.45
极限1129136-12913686.53785.521.6393.4392.381.56
2126328-12632884.65591.53
3125032-12503283.78790.58
4130426-13042687.40294.34
5126214-12621484.57991.40
6128616-12861686.18993.02
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