玛巴洛沙韦片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号115240801对照品来源原料对照品使用方法直接使用
对照品含量(%)100.6对照品水分(%)0对照品稀释倍数250
标示量(mg)40供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.879653379660679653289655379652159654970.04
210.859679049676089677560.03
单位质量响应值RSD%判断
88822.1789194.100.30数据可信
供试品溶液-24122501批-pH6.8(内含0.16%CTAB)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1408740-40874041.57838.9614.2841.5838.9614.28
2389659-38965939.63739.64
3306712-30671231.19931.20
4329318-32931833.49933.50
5411792-41179241.88841.89
6451641-45164145.94245.94
10min1656903-65690366.82164.089.1866.8964.149.19
2654702-65470266.59766.66
3560284-56028456.99357.04
4555011-55501156.45756.51
5659218-65921867.05767.13
6693459-69345970.54070.62
15min1750114-75011476.30374.485.2476.4874.655.25
2745227-74522775.80675.98
3686293-68629369.81169.96
4683173-68317369.49369.64
5752067-75206776.50176.68
6776346-77634678.97179.17
20min1791739-79173980.53779.473.5180.8479.773.53
2789431-78943180.30280.61
3748165-74816576.10476.37
4748445-74844576.13376.40
5793223-79322380.68881.00
6816782-81678283.08483.41
30min1830145-83014584.44484.172.0084.8984.602.02
2829746-82974684.40384.84
3808383-80838382.23082.62
4810523-81052382.44882.84
5832958-83295884.73085.17
6853225-85322586.79187.26
45min1856875-85687587.16387.091.4887.7587.661.51
2855327-85532787.00587.58
3841013-84101385.54986.08
4845612-84561286.01786.55
5861541-86154187.63788.22
6876870-87687089.19789.81
60min1865163-86516388.00687.911.4288.7388.621.45
2861361-86136187.61988.34
3848190-84819086.27986.95
4859045-85904587.38388.06
5866052-86605288.09688.83
6885531-88553190.07890.84
极限1923961-92396193.98793.091.4594.8693.951.47
2913594-91359492.93293.80
3897058-89705891.25092.06
4902103-90210391.76392.58
5929545-92954594.55595.43
6924552-92455294.04794.95
玛巴洛沙韦片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号115240801对照品来源原料对照品使用方法直接使用
对照品含量(%)100.6对照品水分(%)0对照品稀释倍数250
标示量(mg)40供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.879709929705329705909719459711039710320.06
210.859736139723959730040.09
单位质量响应值RSD%判断
89331.3789677.790.28数据可信
供试品溶液-24122502批-pH6.8(内含0.16%CTAB)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1368729-36872937.30027.0623.5737.3027.0623.57
2313448-31344831.70831.71
3256273-25627325.92425.92
4202251-20225120.45920.46
5214534-21453421.70221.70
6249747-24974725.26425.26
10min1665073-66507367.27755.1911.8867.3455.2411.89
2569863-56986357.64657.70
3522958-52295852.90152.94
4491382-49138249.70749.74
5497118-49711850.28750.32
6527239-52723953.33453.38
15min1766585-76658577.54668.626.8177.7268.766.82
2688428-68842869.63969.79
3661296-66129666.89567.03
4638591-63859164.59864.72
5654326-65432666.19066.31
6660616-66061666.82666.96
20min1813862-81386282.32875.764.5182.6376.014.53
2754847-75484776.35876.62
3727821-72782173.62473.87
4722402-72240273.07673.30
5739598-73959874.81675.05
6735048-73504874.35574.60
30min1858874-85887486.88182.233.1187.3282.613.13
2809164-80916481.85382.25
3790772-79077279.99280.36
4797584-79758480.68181.03
5823462-82346283.29983.65
6797706-79770680.69481.06
45min1893308-89330890.36586.402.6990.9586.922.70
2842776-84277685.25385.78
3831701-83170184.13384.63
4846759-84675985.65686.14
5869236-86923687.92988.42
6841070-84107085.08085.58
60min1906069-90606991.65588.062.6592.3988.722.66
2858523-85852386.84687.52
3845467-84546785.52586.16
4873258-87325888.33688.96
5887396-88739689.76790.41
6852283-85228386.21586.86
极限1946672-94667295.76393.282.1396.6594.082.15
2929781-92978194.05494.87
3895229-89522990.55991.34
4909014-90901491.95392.72
5939008-93900894.98795.78
6912833-91283392.34093.13
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