苯磺酸氨氯地平片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数4000
标示量(mg)5供试品稀释倍数1系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
115.341691516900168721689016915168980.11
215.231680716901168540.40
单位质量响应值RSD%判断
1101.561106.630.33数据可信
供试品溶液-8167603批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min122911-2291165.50968.554.8165.5168.554.81
223843-2384368.17468.17
323504-2350467.20467.20
425315-2531572.38272.38
525443-2544372.74872.75
622834-2283465.28965.29
10min130027-3002785.85587.462.5085.9687.582.51
231059-3105988.80688.92
329925-2992585.56485.68
430924-3092488.42088.54
531730-3173090.72590.85
629864-2986485.38985.50
15min132295-3229592.34094.832.3392.5995.092.33
233830-3383096.72996.99
332748-3274893.63593.89
433390-3339095.47195.74
534220-3422097.84498.12
632510-3251092.95593.21
20min133352-3335295.36298.152.1095.7798.572.10
235151-35151100.506100.93
333848-3384896.78197.19
434556-3455698.80599.23
535073-35073100.283100.72
633980-3398097.15897.56
30min133989-3398997.184100.662.3597.75101.242.36
235987-35987102.897103.49
334719-3471999.27199.84
435615-35615101.833102.42
536088-36088103.185103.79
634823-3482399.568100.14
45min134264-3426497.970101.252.2498.70102.002.25
236042-36042103.054103.82
334996-34996100.063100.80
435859-35859102.531103.29
536336-36336103.894104.67
634962-3496299.966100.70
60min134000-3400097.215101.132.5898.11102.052.58
236041-36041103.051103.98
334991-34991100.049100.95
436035-36035103.034103.97
536332-36332103.883104.83
634816-3481699.548100.45
极限134071-3407197.418100.592.6798.47101.672.67
236037-36037103.040104.14
334741-3474199.334100.40
435725-35725102.147103.25
536237-36237103.611104.73
634270-3427097.98799.05
苯磺酸氨氯地平片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数4000
标示量(mg)5供试品稀释倍数1系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
115.341693116844168791690216782168680.35
215.231685716930168940.31
单位质量响应值RSD%判断
1099.611109.260.62数据可信
供试品溶液-8167603批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min124485-2448569.98967.783.7169.9967.783.71
223639-2363967.57167.57
322725-2272564.95864.96
424317-2431769.50969.51
524515-2451570.07570.07
622586-2258664.56164.56
10min132397-3239792.60588.302.6892.7288.412.68
230969-3096988.52388.64
330220-3022086.38286.49
430354-3035486.76586.88
531116-3111688.94389.06
630289-3028986.57986.69
15min134661-3466199.07695.322.1199.3595.582.12
233278-3327895.12395.38
332964-3296494.22694.48
433348-3334895.32395.58
533252-3325295.04995.31
632580-3258093.12893.38
20min135162-35162100.50998.151.40100.9498.571.40
234003-3400397.19697.61
334149-3414997.61398.02
434574-3457498.82899.25
534313-3431398.08298.51
633829-3382996.69897.11
30min135761-35761102.221100.161.80102.82100.741.80
234609-3460998.92899.51
335252-35252100.766101.34
435737-35737102.152102.74
534337-3433798.15098.74
634535-3453598.71699.28
45min135665-35665101.946100.421.53102.72101.171.53
234632-3463298.99499.74
335382-35382101.137101.88
435728-35728102.126102.88
534470-3447098.53099.28
634906-3490699.777100.51
60min135613-35613101.798100.201.74102.74101.121.73
234651-3465199.04899.96
335377-35377101.123102.03
435671-35671101.963102.89
534125-3412597.54498.46
634887-3488799.722100.62
极限135375-35375101.11799.721.83102.23100.801.82
234485-3448598.57399.65
335146-35146100.463101.54
435736-35736102.149103.24
534047-3404797.32198.40
634524-3452498.68599.75
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