诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.23949421394859939481833948642394899939487690.02
210.23937995393710339375490.02
单位质量响应值RSD%判断
387134.22386034.220.21数据可信
供试品溶液-24022901批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min15514-55140.1280.1626.450.130.1625.07
27605-76050.1760.18
36708-67080.1560.16
46652-66520.1540.15
55527-55270.1280.13
610557-105570.2450.24
10min11912448-191244844.34549.1618.4844.3549.1618.48
22213058-221305851.31651.32
32337069-233706954.19154.19
42751144-275114463.79363.79
51769046-176904641.02041.02
61736914-173691440.27540.28
15min12581072-258107259.84973.2917.0359.9273.3717.03
23315642-331564276.88276.97
33121942-312194272.39172.48
44134017-413401795.85995.97
52972528-297252868.92668.99
62838928-283892865.82865.90
20min12950546-295054668.41785.6412.2968.5985.8512.29
23813877-381387788.43588.65
34009637-400963792.97493.19
44161836-416183696.50496.77
53867763-386776389.68589.87
63356481-335648177.82978.01
30min13520820-352082081.64094.407.5881.9394.757.59
24321791-4321791100.213100.57
34186212-418621297.06997.44
44184595-418459597.03197.46
54308828-430882899.912100.24
63904602-390460290.53990.85
诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.23941735394076739413493943379393934239413140.04
210.23942910393956439412370.07
单位质量响应值RSD%判断
386403.33386395.780.01数据可信
供试品溶液-24022901批-pH4.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11136-11360.0260.0333.820.030.0336.92
2890-8900.0210.02
3962-9620.0220.02
41527-15270.0350.04
52091-20910.0490.05
61500-15000.0350.03
10min11252399-125239929.05428.9019.4829.0528.9019.48
21038434-103843424.09024.09
31049232-104923224.34124.34
41078112-107811225.01125.01
51414782-141478232.82132.82
61640530-164053038.05838.06
15min12627920-262792060.96546.3817.9561.0146.4317.93
21611113-161111337.37637.42
31784117-178411741.38941.43
41844709-184470942.79542.84
51966099-196609945.61145.67
62161424-216142450.14250.21
20min13141124-314112472.87056.0916.4273.0256.2116.42
21964972-196497245.58545.69
32226711-222671151.65751.77
42308695-230869553.55953.67
52359208-235920854.73154.86
62505436-250543658.12358.27
30min13757781-375778187.17667.7115.1787.4567.9415.16
22500912-250091258.01858.20
32667373-266737361.88062.08
42977098-297709869.06569.27
52741254-274125463.59463.82
62868457-286845766.54566.79
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