替米沙坦氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100374-202106对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.872710727094270862690226806269990.51
213.942671326751267320.11
单位质量响应值RSD%判断
1946.581917.651.06数据可信
供试品溶液-2024100621批-ph1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min122833-2283385.13785.004.6085.1485.004.60
223701-2370188.37388.37
321389-2138979.75279.75
423521-2352187.70287.70
521640-2164080.68880.69
623700-2370088.36988.37
10min123448-2344887.43089.893.8588.2890.743.82
223946-2394689.28790.17
322705-2270584.65985.46
424688-2468892.05392.93
525215-2521594.01894.83
624651-2465191.91592.80
15min123048-2304885.93890.142.8387.6691.892.81
224215-2421590.29092.07
323778-2377888.66090.30
424516-2451691.41293.21
524999-2499993.21394.96
624494-2449491.33093.13
20min123831-2383188.85888.845.2391.4491.495.07
224859-2485992.69195.37
324044-2404489.65292.18
424553-2455391.55094.26
524281-2428190.53693.21
621396-2139679.77882.49
30min122671-2267184.53386.163.6588.0189.703.54
222016-2201682.09085.70
322855-2285585.21988.65
424032-2403289.60793.23
524201-2420190.23793.82
622871-2287185.27888.79
45min123174-2317486.40886.633.3990.7391.033.23
224729-2472992.20696.63
323167-2316786.38290.66
423146-2314686.30490.83
522636-2263684.40288.89
622542-2254284.05288.42
60min122508-2250883.92586.173.9889.1191.443.85
223301-2330186.88292.23
322175-2217582.68387.83
423780-2378088.66894.05
524517-2451791.41696.75
622385-2238583.46688.67
极限123312-2331286.92386.122.6892.9492.252.52
224150-2415090.04796.27
322902-2290285.39491.36
422352-2235283.34389.62
523164-2316486.37192.62
622697-2269784.62990.67
替米沙坦氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100374-202106对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.872691426862264722689026940268160.73
213.94264882613257141.15
单位质量响应值RSD%判断
1933.38951.0048.17数据不可信!(响应值差异过大,请重新称样测定!)
供试品溶液-2024100621批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min124002-24002135.622129.635.66135.62129.635.66
221352-21352120.649120.65
321761-21761122.960122.96
424127-24127136.329136.33
522249-22249125.717125.72
624161-24161136.521136.52
10min124955-24955141.007136.023.17142.36137.323.16
223931-23931135.221136.43
324513-24513138.510139.74
424226-24226136.888138.25
522700-22700128.266129.52
624114-24114136.255137.62
15min124480-24480138.323114.6348.97141.09117.2947.91
224584-24584138.911141.47
324099-24099136.171138.79
423811-23811134.543137.28
521-210.1192.66
624730-24730139.736142.46
20min125103-25103141.844113.7449.02145.99117.5447.32
223886-23886134.967138.91
323729-23729134.080138.06
424428-24428138.030142.11
523610-23610133.408135.95
622-220.1244.25
30min123470-23470132.616134.532.32138.18139.472.02
223866-23866134.854140.15
323536-23536132.989138.31
423794-23794134.447139.91
524856-24856140.448144.32
623334-23334131.848135.97
45min124937-24937140.906135.393.09147.80141.683.31
224460-24460138.210144.86
323843-23843134.724141.37
423723-23723134.046140.85
522759-22759128.599133.88
624046-24046135.871141.32
60min122967-22967129.774132.642.45138.08140.282.03
222824-22824128.966136.99
323945-23945135.300143.29
423235-23235131.289139.43
523569-23569133.176139.74
624301-24301137.312144.12
极限124868-24868140.516134.813.26150.12143.783.44
224294-24294137.272146.59
323917-23917135.142144.49
423560-23560133.125142.58
522551-22551127.424135.32
623958-23958135.374143.55
替米沙坦氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100374-202106对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.872684626386265472649326641265830.66
213.942665626370265130.77
单位质量响应值RSD%判断
1916.581901.940.55数据可信
供试品溶液-2024100621批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min121529-2152981.23284.932.9581.2384.922.95
222346-2234684.31484.31
322004-2200483.02483.02
423224-2322487.62787.63
523039-2303986.92986.93
622906-2290686.42786.43
10min121988-2198882.96487.993.0083.7888.832.99
223268-2326887.79388.64
323544-2354488.83589.66
423937-2393790.31891.19
523790-2379089.76390.63
623386-2338688.23989.10
15min123438-2343888.43585.725.0490.0887.454.95
221281-2128180.29682.02
322017-2201783.07384.79
423512-2351288.71490.49
524182-2418291.24293.01
621881-2188182.56084.31
20min122322-2232284.22485.512.0186.7588.102.01
222156-2215683.59886.12
322728-2272885.75688.31
423473-2347388.56791.23
522624-2262485.36388.04
622675-2267585.55688.13
30min121781-2178182.18382.892.1285.5586.332.08
222386-2238684.46587.83
321348-2134880.54983.96
422323-2232384.22887.78
522410-2241084.55688.09
621559-2155981.34584.77
45min121591-2159181.46685.182.6185.6689.452.55
222374-2237484.42088.62
323164-2316487.40191.61
423160-2316087.38691.78
522719-2271985.72290.10
622444-2244484.68488.93
60min121718-2171881.94583.904.3086.9589.024.16
221708-2170881.90786.96
321013-2101379.28584.37
423293-2329387.88893.16
523418-2341888.35993.60
622268-2226884.02089.11
极限121207-2120780.01779.464.6985.8485.424.32
220429-2042977.08182.95
322310-2231084.17990.06
421768-2176882.13488.28
519519-1951973.64879.77
621120-2112079.68985.62
替米沙坦氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100374-202106对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)5供试品稀释倍数10系数0.7211
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.872641126568265042634626481264620.33
213.94267382613382141.15
单位质量响应值RSD%判断
1907.86959.9746.75数据不可信!(响应值差异过大,请重新称样测定!)
供试品溶液-2024100621批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min121623-21623121.954126.583.44121.95126.583.44
221884-21884123.426123.43
321740-21740122.614122.61
423171-23171130.685130.68
522964-22964129.517129.52
623273-23273131.260131.26
10min122344-22344126.020131.923.95127.24133.193.94
222799-22799128.587129.82
322986-22986129.641130.87
424828-24828140.030141.34
523250-23250131.130132.43
624138-24138136.139137.45
15min123493-23493132.501131.973.31134.98134.563.27
223015-23015129.805132.32
323551-23551132.828135.35
424773-24773139.720142.43
522499-22499126.895129.50
623065-23065130.087132.76
20min123321-23321131.531133.162.84135.34137.062.82
222731-22731128.203132.02
323068-23068130.104133.95
424294-24294137.018141.12
524336-24336137.255141.13
623909-23909134.847138.82
30min122974-22974129.574124.346.74134.69129.586.52
221784-21784122.862127.96
319349-19349109.129114.28
423648-23648133.375138.85
522544-22544127.148132.40
621978-21978123.956129.28
45min122045-22045124.334126.593.95130.75133.073.88
221193-21193119.529125.86
322436-22436126.539132.78
423914-23914134.875141.68
522437-22437126.545133.06
622646-22646127.724134.29
60min121740-21740122.614122.641.55130.27130.381.39
221606-21606121.858129.38
321809-21809123.003130.51
421173-21173119.416127.57
522025-22025124.221132.01
622114-22114124.723132.56
极限122029-22029124.244124.933.26133.13133.903.22
221424-21424120.832129.57
321517-21517121.356130.09
423421-23421132.095141.45
522365-22365126.139135.17
622150-22150124.926134.01
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