辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号2306201对照品来源原料药对照品使用方法直接使用
对照品含量(%)99.5对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.042705172702262700802704552702372703030.07
210.092695462691332693400.11
单位质量响应值RSD%判断
26922.6126693.760.61数据可信
供试品溶液-25011003批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min193647-9364734.75837.019.0934.7637.019.10
291742-9174234.05134.05
391425-9142533.93333.93
4100379-10037937.25737.26
5112301-11230141.68241.68
6108807-10880740.38540.39
10min1119013-11901344.17345.606.4244.2845.726.42
2117235-11723543.51343.62
3114706-11470642.57542.68
4126357-12635746.89947.01
5136455-13645550.64750.77
6123436-12343645.81545.94
15min1138438-13843851.38352.645.5851.6252.895.59
2136913-13691350.81751.05
3132735-13273549.26649.50
4146126-14612654.23654.49
5155086-15508657.56257.84
6141666-14166652.58152.84
20min1151380-15138056.18757.554.8056.5857.954.81
2150812-15081255.97656.36
3147374-14737454.70055.08
4159192-15919259.08659.50
5167961-16796162.34162.79
6153524-15352456.98257.40
30min1172274-17227463.94264.573.7464.5065.153.75
2171301-17130163.58064.13
3166975-16697561.97562.52
4177773-17777365.98366.58
5185104-18510468.70469.34
6170338-17033863.22363.81
45min1193252-19325271.72870.952.8472.4871.722.85
2190861-19086170.84071.58
3185798-18579868.96169.69
4191907-19190771.22972.02
5199940-19994074.21075.05
6185130-18513068.71369.49
60min1206870-20687076.78274.932.8577.7575.922.84
2204440-20444075.88076.84
3198439-19843973.65374.59
4201268-20126874.70375.71
5207748-20774877.10878.17
6192548-19254871.46772.45
极限1231877-23187786.06486.782.2287.2687.992.24
2229813-22981385.29886.48
3227811-22781184.55585.71
4238442-23844288.50189.73
5241324-24132489.57090.87
6233533-23353386.67987.88
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号2306201对照品来源原料药对照品使用方法直接使用
对照品含量(%)99.5对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.042701362703842703742698982702432702070.08
210.092703742696682700210.19
单位质量响应值RSD%判断
26913.0526761.250.40数据可信
供试品溶液-25011004批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1126082-12608246.74652.5410.1346.7552.5410.12
2131479-13147948.74748.75
3129025-12902547.83747.84
4157361-15736158.34358.34
5155530-15553057.66457.66
6150827-15082755.92055.92
10min1152141-15214156.40762.788.6956.5562.948.70
2161978-16197860.05560.20
3155192-15519257.53957.68
4185933-18593368.93669.11
5182935-18293567.82568.00
6177842-17784265.93666.10
15min1172632-17263264.00570.307.8264.3170.647.83
2180898-18089867.06967.40
3175971-17597165.24365.56
4206682-20668276.62977.01
5202856-20285675.21075.59
6198577-19857773.62473.99
20min1185034-18503468.60375.027.2869.1075.577.29
2193370-19337071.69372.22
3189951-18995170.42670.94
4220420-22042081.72282.33
5214959-21495979.69880.30
6210270-21027077.95978.55
30min1203410-20341075.41680.835.7876.1281.615.81
2210605-21060578.08378.83
3207065-20706576.77177.49
4233923-23392386.72987.59
5228398-22839884.68085.52
6224616-22461683.27884.10
45min1214316-21431679.45984.514.7680.3985.534.80
2221853-22185382.25483.23
3219913-21991381.53482.49
4242075-24207589.75190.87
5236948-23694887.85088.95
6232453-23245386.18487.25
60min1219368-21936881.33285.844.2182.5087.124.26
2225678-22567883.67284.90
3224843-22484383.36284.56
4244839-24483990.77692.16
5238923-23892388.58389.94
6235549-23554987.33288.66
极限1265789-26578998.54399.971.9299.96101.511.96
2263199-26319997.58399.06
3270048-270048100.122101.57
4277574-277574102.913104.57
5273014-273014101.222102.85
6268226-26822699.447101.04
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