替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.072628626265262892616226182262370.23
214.072620126136261680.18
单位质量响应值RSD%判断
1864.751859.840.19数据可信
加速6月-供试品溶液-2024070321批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min123857-2385789.87093.953.0889.8793.943.08
224725-2472593.14093.14
325949-2594997.75197.75
424707-2470793.07293.07
525705-2570596.83296.83
624691-2469193.01293.01
10min125060-2506094.40297.233.6095.3098.173.59
226157-2615798.53499.47
327317-27317102.904103.88
425560-2556096.28697.22
526069-2606998.20399.17
624706-2470693.06894.00
15min125114-2511494.60597.093.0196.4599.003.01
226377-2637799.363101.28
326696-26696100.565102.57
425339-2533995.45397.35
526291-2629199.039100.99
624826-2482693.52195.38
20min125232-2523295.05096.123.1597.8499.013.12
226679-26679100.501103.41
326099-2609998.316101.33
425305-2530595.32598.17
525455-2545595.89098.83
624334-2433491.66794.46
30min124000-2400090.40993.452.2794.1597.292.29
225051-2505194.36898.28
325618-2561896.504100.50
424622-2462292.75296.55
525071-2507194.44398.34
624475-2447592.19895.91
极限123873-2387389.93193.803.5694.5798.583.52
225875-2587597.472102.33
325916-2591697.627102.59
424490-2449092.25596.98
525152-2515294.74999.59
624095-2409590.76795.40
替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.072614526002260732609526095260820.20
214.072600926054260320.13
单位质量响应值RSD%判断
1853.731850.180.14数据可信
加速6月-供试品溶液-ald批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min123333-2333388.38790.253.9488.3990.243.93
223928-2392890.64190.64
322425-2242584.94884.95
423590-2359089.36189.36
525040-2504094.85394.85
624625-2462593.28193.28
10min124551-2455193.00194.072.0693.8894.972.07
224570-2457093.07393.98
324359-2435992.27493.12
424594-2459493.16494.06
525261-2526195.69096.64
625660-2566097.20298.13
15min124913-2491394.37294.062.2896.1995.902.27
224840-2484094.09695.93
324640-2464093.33895.11
423964-2396490.77792.60
525722-2572297.43799.34
624905-2490594.34296.25
20min125310-2531095.87694.921.7098.6397.701.70
224598-2459893.17995.96
324793-2479393.91896.62
424674-2467493.46796.20
525315-2531595.89598.77
625648-2564897.156100.00
30min124288-2428892.00592.661.3695.7296.391.36
224159-2415991.51695.23
324504-2450492.82396.47
424156-2415691.50595.17
524649-2464993.37297.21
625005-2500594.72198.54
极限124690-2469093.52792.632.1798.1697.292.09
224050-2405091.10395.73
323655-2365589.60794.18
425137-2513795.22199.80
524444-2444492.59697.37
624743-2474393.72898.50
替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.072629225994261272626126017261380.53
214.072590926011259600.28
单位质量响应值RSD%判断
1857.711845.060.49数据可信
加速6月-供试品溶液-2024070421批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min124857-2485794.19092.761.2294.1992.761.22
224353-2435392.28092.28
324420-2442092.53492.53
423996-2399690.92790.93
524581-2458193.14493.14
624672-2467293.48993.49
10min125507-2550796.65396.621.2697.5997.551.25
225450-2545096.43797.36
324963-2496394.59295.52
425948-2594898.32499.23
525652-2565297.20398.13
625470-2547096.51397.45
15min125387-2538796.19896.501.1598.1198.401.12
225495-2549596.60898.49
325843-2584397.92699.80
425753-2575397.58599.48
525078-2507895.02796.93
625251-2525195.68397.58
20min125515-2551596.68396.361.3599.5599.221.31
225628-2562897.11299.96
325014-2501494.78597.64
425945-2594598.313101.18
525125-2512595.20698.06
625347-2534796.04798.90
30min124393-2439392.43294.551.7196.2798.381.65
225251-2525195.68399.51
324443-2444392.62196.42
425341-2534196.02499.88
525250-2525095.67999.49
625039-2503994.88098.70
极限124662-2466293.45194.041.1298.2198.801.07
224498-2449892.83097.61
324960-2496094.58099.30
425284-2528495.808100.62
524686-2468693.54298.30
624811-2481194.01698.78
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