替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.072640326161262412614726059262020.50
214.072609326235261640.39
单位质量响应值RSD%判断
1862.261859.560.11数据可信
中间条件6月-供试品溶液-2024070321批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min126096-2609698.37894.494.2898.3894.494.28
224566-2456692.61092.61
325784-2578497.20297.20
425565-2556596.37696.38
523158-2315887.30287.30
625216-2521695.06095.06
10min126741-26741100.80997.063.41101.7998.013.40
226258-2625898.98899.91
324738-2473893.25894.23
426335-2633599.279100.24
524638-2463892.88193.75
625777-2577797.17598.13
15min127215-27215102.59699.212.51104.59101.122.53
226515-2651599.957101.87
326483-2648399.837101.74
426489-2648999.859101.82
525251-2525195.19296.99
625942-2594297.79799.72
20min127383-27383103.23099.342.72106.25102.252.72
226465-2646599.769102.68
326636-26636100.413103.32
426414-2641499.577102.53
525231-2523195.11797.87
625983-2598397.952100.85
30min126796-26796101.01797.152.64105.07101.052.64
225491-2549196.097100.01
325640-2564096.659100.57
426356-2635699.358103.31
524959-2495994.09197.80
625381-2538195.68299.56
极限126805-26805101.05197.882.39106.11102.752.40
226245-2624598.939103.81
326207-2620798.796103.67
425920-2592097.714102.66
524989-2498994.20598.85
625612-2561296.553101.39
替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.072604326225260372606426108260950.30
214.072619926062261300.38
单位质量响应值RSD%判断
1854.661857.140.10数据可信
中间条件6月-供试品溶液-ald批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min123765-2376589.83292.754.0189.8392.754.01
223639-2363989.35689.36
324736-2473693.50393.50
425103-2510394.89094.89
523841-2384190.11990.12
626144-2614498.82598.82
10min125785-2578597.46896.242.3698.3797.172.36
224625-2462593.08393.98
325193-2519395.23096.17
425453-2545396.21397.16
525297-2529795.62396.52
626408-2640899.823100.81
15min125945-2594598.07396.602.8499.9598.492.83
224801-2480193.74895.57
324740-2474093.51895.40
425571-2557196.65998.57
525606-2560696.79198.65
626668-26668100.806102.79
20min125867-2586797.77896.432.38100.6399.292.38
224807-2480793.77196.53
325413-2541396.06298.88
424931-2493194.24097.12
525607-2560796.79599.62
626440-2644099.944102.94
30min125371-2537195.90393.783.0199.7397.602.95
223325-2332588.16991.87
324875-2487594.02897.81
425094-2509494.85698.68
525154-2515495.08398.88
625041-2504194.65598.65
极限125204-2520495.27295.022.92100.0699.782.89
224063-2406390.95995.54
325003-2500394.51299.24
424933-2493394.24799.02
525286-2528695.582100.33
626337-2633799.554104.49
替米沙坦左氨氯地平片项目信息
介质体积(ml)500取样体积(ml)5补液体积(ml)5
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数10000
标示量(mg)2.5供试品稀释倍数5系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
114.072636526270259842632126033261950.67
214.072597925895259370.23
单位质量响应值RSD%判断
1861.761843.430.70数据可信
中间条件6月-供试品溶液-2024070421批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min124807-2480793.94093.921.0593.9493.921.05
224880-2488094.21794.22
324514-2451492.83192.83
424590-2459093.11993.12
524772-2477293.80893.81
625247-2524795.60795.61
10min125466-2546696.43696.941.2897.3897.881.27
226063-2606398.69799.64
325524-2552496.65697.58
425099-2509995.04695.98
525810-2581097.73998.68
625636-2563697.08098.04
15min125417-2541796.25096.271.7498.1598.181.71
224900-2490094.29396.22
324981-2498194.59996.49
425533-2553396.69098.57
526100-2610098.837100.75
625605-2560596.96298.89
20min125584-2558496.88395.903.3499.7598.773.23
226212-2621299.261102.13
325506-2550696.58799.43
425568-2556896.82299.67
525374-2537496.08898.99
623705-2370589.76792.66
30min124996-2499694.65695.992.0898.4999.822.00
225692-2569297.292101.16
324791-2479193.88097.69
424962-2496294.52798.34
525486-2548696.512100.38
626163-2616399.075102.87
极限125829-2582997.81196.111.92102.59100.901.85
225560-2556096.792101.63
324582-2458293.08897.83
425517-2551796.629101.39
525771-2577197.591102.42
625014-2501494.72499.51
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