诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.184101571410029241037014103132410050841018410.04
210.144090238410444240973400.25
单位质量响应值RSD%判断
402931.34404076.920.21数据可信
供试品溶液-25010201批-pH4.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min13275347-327534772.76372.806.6072.7672.806.60
23565585-356558579.21179.21
33477007-347700777.24377.24
42970600-297060065.99365.99
53176379-317637970.56570.56
63197042-319704271.02471.02
10min14320308-432030895.97894.342.3896.1094.462.37
24247365-424736594.35794.49
34310369-431036995.75795.89
44206319-420631993.44593.56
54329305-432930596.17796.29
64065567-406556790.31890.44
15min14422315-442231598.24496.342.8398.5296.622.83
24310585-431058595.76296.05
34333147-433314796.26396.55
44376767-437676797.23297.50
54463726-446372699.16499.44
64114452-411445291.40491.67
20min14415904-441590498.10196.842.8498.5597.282.84
24333570-433357096.27296.72
34395014-439501497.63798.09
44389879-438987997.52397.95
54491828-449182899.788100.23
64129262-412926291.73392.15
30min14416934-441693498.12497.692.2098.7398.292.20
24405938-440593897.88098.49
34385827-438582797.43398.04
44429027-442902798.39398.98
54521999-4521999100.458101.07
64225452-422545293.87094.44
诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.184097979409652341055714097664409760340990680.09
210.144076558407822440773910.03
单位质量响应值RSD%判断
402658.94402109.570.10数据可信
供试品溶液-25010202批-pH4.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min13515485-351548578.31573.915.0578.3273.915.05
23467539-346753977.24777.25
33177055-317705570.77670.78
43130910-313091069.74869.75
53199100-319910071.26771.27
63415565-341556576.08976.09
10min14417416-441741698.40896.502.0498.5496.632.05
24307952-430795295.96996.10
34253462-425346294.75594.87
44230908-423090894.25394.37
54328875-432887596.43596.55
64453279-445327999.20799.33
15min14472428-447242899.63397.821.9099.9398.111.90
24349252-434925296.88997.18
34326077-432607796.37396.65
44318354-431835496.20196.47
54363320-436332097.20397.48
64517407-4517407100.635100.93
20min14451855-445185599.17598.551.4399.6499.001.43
24367888-436788897.30497.75
34394944-439494497.90798.34
44361130-436113097.15497.59
54437663-443766398.85999.30
64528934-4528934100.892101.35
30min14484271-448427199.89798.431.10100.5299.041.10
24399766-439976698.01598.63
34374044-437404497.44298.04
44371345-437134597.38197.98
54471655-447165599.616100.22
64409272-440927298.22698.85
诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.6对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.184103052410192141033564101521410167141023040.03
210.144092973409486840939200.04
单位质量响应值RSD%判断
402976.82403739.640.14数据可信
供试品溶液-25010203批-pH4.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min13486389-348638977.48073.805.2777.4873.805.27
23483889-348388977.42477.42
33105937-310593769.02569.02
43370140-337014074.89674.90
53376207-337620775.03175.03
63103360-310336068.96768.97
10min14312755-431275595.84495.162.7895.9795.282.78
24348697-434869796.64396.77
34128930-412893091.75991.87
44414576-441457698.10798.23
54347593-434759396.61896.74
64140403-414040392.01492.13
15min14378810-437881097.31296.871.5597.6097.161.55
24358328-435832896.85797.15
34323586-432358696.08596.35
44461409-446140999.14899.44
54374420-437442097.21597.50
64257921-425792194.62694.89
20min14411611-441161198.04197.232.6098.4997.682.59
24425734-442573498.35598.81
34167258-416725892.61193.04
44480392-448039299.570100.02
54437889-443788998.62599.07
64329040-432904096.20696.63
30min14469659-446965999.33198.471.0299.9599.081.03
24440830-444083098.69199.31
34380366-438036697.34797.93
44475809-447580999.468100.09
54447915-444791598.84899.46
64370663-437066397.13197.72
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