玛巴洛沙韦片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号115240801对照品来源原料对照品使用方法直接使用
对照品含量(%)100.6对照品水分(%)0对照品稀释倍数2500
标示量(mg)20供试品稀释倍数5系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.571015341015271015681015361016141015560.04
211.571016961017641017300.05
单位质量响应值RSD%判断
8777.538792.570.13数据可信
供试品溶液-25011701批-pH6.8(内含0.16%CTAB)
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min125282-2528226.05622.0631.5526.0622.0631.55
220689-2068921.32221.32
316576-1657617.08317.08
418408-1840818.97218.97
532931-3293133.93933.94
614533-1453314.97814.98
10min161227-6122763.10162.3613.2963.3962.6113.35
261670-6167063.55863.79
356962-5696258.70658.90
459109-5910960.91961.13
574340-7434076.61676.99
649765-4976551.28951.46
15min178834-7883481.24880.806.5882.2481.746.70
279248-7924881.67482.62
378074-7807480.46481.31
476477-7647778.81879.71
586863-8686389.52290.75
670880-7088073.05073.79
20min183073-8307385.61688.153.9787.5189.984.09
285910-8591088.54090.39
387189-8718989.85891.59
484247-8424786.82688.59
591149-9114993.94096.16
681616-8161684.11585.66
30min187923-8792390.61594.182.6793.4697.002.74
291384-9138494.18297.02
393624-9362496.49099.22
491947-9194794.76297.49
594176-9417697.059100.33
689233-8923391.96594.45
45min188531-8853191.24195.382.8995.0999.242.89
291920-9192094.73498.62
396005-9600598.944102.75
492985-9298595.83299.61
594748-9474897.649101.99
691099-9109993.88897.39
60min189397-8939792.13496.703.0497.00101.622.84
292141-9214194.96299.90
395225-9522598.140103.05
493972-9397296.849101.69
594463-9446397.355102.79
697780-97780100.774105.32
极限189726-8972692.47398.243.1498.36104.242.94
295213-9521398.128104.12
397305-97305100.284106.28
497502-97502100.487106.41
594789-9478997.691104.20
697423-97423100.406106.07
玛巴洛沙韦片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号115240801对照品来源原料对照品使用方法直接使用
对照品含量(%)100.6对照品水分(%)0对照品稀释倍数2500
标示量(mg)20供试品稀释倍数5系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.571018551019511019951016361013111017500.28
211.571018971016841017900.15
单位质量响应值RSD%判断
8794.308797.750.03数据可信
供试品溶液-25011701批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min111446-1144611.78210.5240.4311.7810.5240.44
26782-67826.9816.98
317931-1793118.45718.46
48028-80288.2638.26
57496-74967.7167.72
69637-96379.9209.92
10min128892-2889229.73929.388.3729.8729.498.49
225816-2581626.57326.65
332728-3272833.68833.89
427161-2716127.95828.05
527481-2748128.28728.37
629150-2915030.00530.12
15min135475-3547536.51537.533.4436.9837.983.55
234928-3492835.95236.33
338409-3840939.53540.11
436225-3622537.28737.69
536438-3643837.50737.91
637291-3729138.38538.83
20min138304-3830439.42741.002.7540.2941.862.70
238944-3894440.08640.86
339598-3959840.75941.78
440165-4016541.34342.16
540824-4082442.02142.84
641140-4114042.34743.22
30min141361-4136142.57444.212.1943.8845.532.10
243270-4327044.53945.76
342978-4297844.23845.71
443410-4341044.68345.96
544133-4413345.42746.71
642561-4256143.80945.15
45min142626-4262643.87646.553.2745.6548.363.17
244845-4484546.16047.87
345422-4542246.75448.72
446911-4691148.28750.06
546267-4626747.62449.41
645292-4529246.62048.45
60min145926-4592647.27347.940.9249.5450.271.01
246184-4618447.53949.76
346907-4690748.28350.77
446911-4691148.28750.60
546629-4662947.99750.31
646910-4691048.28650.63
极限144548-4454845.85547.894.0848.6550.743.98
244136-4413645.43048.18
348155-4815549.56752.59
447390-4739048.78051.63
548716-4871650.14553.00
646188-4618847.54350.42
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