贝派度酸片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号BEMA-231010D对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.72对照品水分(%)0对照品稀释倍数50
标示量(mg)180供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.292989622994803019772995992995962999230.40
210.312988302987582987940.02
单位质量响应值RSD%判断
29147.0428980.990.41数据可信
供试品溶液-24031301批-pH6.6
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1128240-12824044.00035.4514.4344.0035.4514.43
299522-9952234.14734.15
3105131-10513136.07136.07
4101664-10166434.88234.88
581656-8165628.01728.02
6103719-10371935.58735.59
10min1251072-25107286.14582.912.5786.2282.972.57
2245297-24529784.16384.22
3243522-24352283.55483.61
4239367-23936782.12982.19
5234533-23453380.47080.52
6236125-23612581.01681.08
15min1273118-27311893.70993.681.8193.9393.881.81
2280610-28061096.27996.48
3272892-27289293.63193.83
4268715-26871592.19892.39
5266981-26698191.60391.78
6275940-27594094.67794.87
20min1278496-27849695.55496.392.1795.9396.752.16
2288724-28872499.06399.42
3286471-28647198.29098.65
4275182-27518294.41794.77
5273827-27382793.95294.29
6282898-28289897.06497.42
30min1281033-28103396.42596.811.9896.9697.321.98
2291800-291800100.119100.64
3280827-28082796.35496.87
4278596-27859695.58896.09
5275844-27584494.64495.13
6284876-28487697.74398.26
45min1282109-28210996.79496.942.1397.4997.622.13
2292744-292744100.443101.13
3280204-28020496.14096.82
4277854-27785495.33496.00
5276407-27640794.83795.49
6285906-28590698.09698.77
60min1281396-28139696.54996.842.1097.4097.682.10
2292205-292205100.258101.11
3280333-28033396.18497.02
4277092-27709295.07295.90
5276588-27658894.89995.71
6285824-28582498.06898.91
极限1280844-28084496.36096.662.2197.3797.662.21
2291915-291915100.158101.18
3278845-27884595.67496.67
4276757-27675794.95795.94
5275765-27576594.61795.58
6286175-28617598.18999.19
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