佩玛贝特片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号DHX240702对照品来源ZZ对照品使用方法直接使用
对照品含量(%)99.74对照品水分(%)0对照品稀释倍数100000
标示量(mg)0.1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.682040120389203732024020354203510.32
29.492026520199202320.24
单位质量响应值RSD%判断
2102.382131.930.99数据可信
供试品溶液-25011301批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min117049-1704972.29064.1411.3372.2964.1411.33
216275-1627569.00869.01
314675-1467562.22462.22
416169-1616968.55968.56
512384-1238452.51052.51
614203-1420360.22360.22
10min120560-2056087.17784.354.9687.3084.454.97
220801-2080188.19988.31
320217-2021785.72385.83
420457-2045786.74186.85
518415-1841578.08278.17
618903-1890380.15280.25
15min121313-2131390.37090.321.8190.6490.571.82
221537-2153791.32091.58
321500-2150091.16391.41
421758-2175892.25792.52
520971-2097188.92089.14
620732-2073287.90788.14
20min121500-2150091.16392.622.1591.5893.022.15
221813-2181392.49092.90
322377-2237794.88295.28
422466-2246695.25995.67
521460-2146090.99491.36
621450-2145090.95191.33
30min121871-2187192.73693.992.1693.3094.542.16
221956-2195693.09793.67
322264-2226494.40394.96
423056-2305697.76198.33
521713-2171392.06692.58
622142-2214293.88594.42
45min122052-2205293.50495.633.0694.2396.343.05
222417-2241795.05195.77
323259-2325998.62299.34
423563-2356399.911100.64
521970-2197093.15693.83
622061-2206193.54294.23
60min122080-2208093.62296.133.7694.5097.003.75
222526-2252695.51496.40
323576-2357699.966100.84
423760-23760100.746101.65
521562-2156291.42692.25
622523-2252395.50196.35
极限122061-2206193.54296.683.6994.5897.713.68
222450-2245095.19196.23
323599-23599100.063101.11
424082-24082102.111103.18
522090-2209093.66594.64
622526-2252695.51496.52
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