恩格列净片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号101566-202301对照品来源中检所对照品使用方法直接使用
对照品含量(%) 100对照品水分(%)0对照品稀释倍数400
标示量(mg)25供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.851341349133877013412701340903134088613406360.08
29.861344038134322313436300.05
单位质量响应值RSD%判断
136105.18136270.790.09数据可信
加速6月-供试品溶液-2024052411批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1921671-92167160.90956.628.8260.9156.618.82
2919233-91923360.74860.75
3935216-93521661.80461.80
4791151-79115152.28352.28
5781447-78144751.64251.64
6791475-79147552.30552.30
10min11246711-124671182.38980.193.1282.4980.283.13
21241143-124114382.02182.12
31254280-125428082.88982.99
41188565-118856578.54678.63
51176828-117682877.77177.86
61172881-117288177.51077.60
15min11333529-133352988.12686.651.8688.3786.881.87
21330695-133069587.93988.18
31333515-133351588.12688.37
41294568-129456885.55285.77
51278158-127815884.46784.68
61296669-129666985.69185.91
20min11356113-135611389.61988.841.1090.0089.211.11
21359233-135923389.82590.21
31354897-135489789.53989.93
41338789-133878988.47488.83
51322428-132242887.39387.75
61334118-133411888.16588.52
30min11372491-137249190.70190.400.9091.2490.920.91
21377453-137745391.02991.56
31374839-137483990.85691.39
41364163-136416390.15190.66
51344655-134465588.86289.36
61374208-137420890.81591.32
45min11379921-137992191.19291.430.4291.8892.100.42
21384739-138473991.51192.20
31390699-139069991.90592.59
41378982-137898291.13091.79
51377090-137709091.00591.66
61389410-138941091.81992.48
60min11379896-137989691.19191.610.4092.0392.430.40
21389651-138965191.83592.67
31391741-139174191.97392.82
41381361-138136191.28792.10
51382513-138251391.36492.17
61392020-139202091.99292.80
极限11528187-1528187100.99099.991.18101.98100.961.16
21493358-149335898.68999.68
31513901-1513901100.046101.04
41500468-150046899.159100.12
51539359-1539359101.729102.68
61502854-150285499.316100.28
恩格列净片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号101566-202301对照品来源中检所对照品使用方法直接使用
对照品含量(%) 100对照品水分(%)0对照品稀释倍数400
标示量(mg)25供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.851339835134189513426191340669134119113412420.09
29.861342157134160613418820.03
单位质量响应值RSD%判断
136166.70136093.510.04数据可信
加速6月-供试品溶液-2024052511批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1927858-92785861.34455.719.5461.3455.719.53
2891994-89199458.97358.97
3903660-90366059.74459.74
4833664-83366455.11655.12
5723389-72338947.82647.83
6775162-77516251.24851.25
10min11258457-125845783.20179.363.1883.3079.463.18
21189928-118992878.67078.77
31216044-121604480.39780.50
41213199-121319980.20980.30
51146660-114666075.80975.89
61178310-117831077.90277.99
15min11353106-135310689.45885.862.7589.7086.082.76
21264528-126452883.60283.83
31296370-129637085.70785.94
41326190-132619087.67987.90
51261097-126109783.37583.58
61290360-129036085.31085.53
20min11372955-137295590.77088.122.2491.1688.482.24
21305604-130560486.31886.69
31335208-133520888.27588.65
41360572-136057289.95290.32
51297596-129759685.78886.13
61324803-132480387.58787.94
30min11390892-139089291.95689.252.1892.5089.772.19
21320662-132066287.31387.83
31349609-134960989.22789.75
41376733-137673391.02091.54
51317616-131761687.11287.60
61344388-134438888.88289.39
45min11392618-139261892.07089.892.1292.7790.562.13
21326576-132657687.70488.36
31373718-137371890.82191.49
41386637-138663791.67592.35
51329292-132929287.88488.52
61349398-134939889.21389.86
60min11397949-139794992.42390.122.1293.2790.942.13
21328305-132830587.81988.62
31364431-136443190.20791.03
41391895-139189592.02392.85
51332975-133297588.12788.91
61363233-136323390.12890.93
极限11519096-1519096100.432100.230.72101.43101.200.73
21512936-1512936100.025100.98
31526162-1526162100.899101.87
41529093-1529093101.093102.07
51500394-150039499.196100.12
61508756-150875699.749100.70
恩格列净片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号101566-202301对照品来源中检所对照品使用方法直接使用
对照品含量(%) 100对照品水分(%)0对照品稀释倍数400
标示量(mg)25供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.851341058134092813403811339995134018613405100.04
29.861335747133690813363280.07
单位质量响应值RSD%判断
136092.39135530.220.30数据可信
加速6月-供试品溶液-2024052611批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1943829-94382962.54663.108.4462.5563.108.44
21067733-106773370.75770.76
3900722-90072259.69059.69
4936626-93662662.06962.07
5845125-84512556.00556.01
61019093-101909367.53467.53
10min11301701-130170186.26287.774.1586.3787.874.16
21384514-138451491.75091.87
31305002-130500286.48186.58
41319572-131957287.44687.55
51245527-124552782.53982.63
61390175-139017592.12592.24
15min11388750-138875092.03194.092.9092.2894.342.91
21461387-146138796.84497.12
31403605-140360593.01593.26
41410908-141090893.49993.75
51375378-137537891.14591.38
61478671-147867197.99098.26
20min11426340-142634094.52296.552.5294.9296.952.53
21489164-148916498.68599.12
31435320-143532095.11795.52
41445649-144564995.80196.21
51429501-142950194.73195.11
61515279-1515279100.416100.84
30min11454401-145440196.38198.692.4396.9499.262.44
21519857-1519857100.719101.32
31471396-147139697.50798.06
41479744-147974498.06198.63
51463530-146353096.98697.53
61546680-1546680102.496103.09
45min11476533-147653397.84899.822.1098.57100.552.11
21532109-1532109101.531102.30
31485221-148522198.42499.14
41507966-150796699.931100.66
51480888-148088898.13798.84
61554647-1554647103.024103.79
60min11473225-147322597.629100.342.2898.51101.242.28
21535859-1535859101.779102.71
31490313-149031398.76199.64
41535364-1535364101.747102.64
51489334-148933498.69699.56
61560509-1560509103.413104.35
极限11546333-1546333102.473102.231.20103.52103.291.21
21542900-1542900102.246103.35
31531018-1531018101.459102.51
41561124-1561124103.454104.52
51513286-1513286100.283101.31
61560963-1560963103.443104.55
点击查看处理图标(人工保存)
　
原始图谱下载图谱(姜进硙 于 2025-02-05 13:26:27 完成)
生成报告数据部分(等待生成报告)
Current page cost:84 ms