达格列净片项目信息
介质体积(ml)1000取样体积(ml)1.5补液体积(ml)1.5
对照品批号D5551-23-012对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)19.2对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
112.461970341974171974361972641973431972990.09
212.451990511986921988720.13
单位质量响应值RSD%判断
15834.5915973.650.62数据可信
供试品溶液-25012101-1批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1130470-13047066.15366.415.8766.1566.415.86
2121186-12118661.44661.45
3124488-12448863.12063.12
4131112-13111266.47966.48
5136274-13627469.09669.10
6142305-14230572.15472.15
10min1145036-14503673.53975.984.6673.6476.084.66
2143844-14384472.93473.03
3147732-14773274.90675.00
4145112-14511273.57773.68
5159176-15917680.70880.81
6158249-15824980.23880.35
15min1148731-14873175.41277.754.0275.6277.964.02
2151082-15108276.60476.81
3150929-15092976.52776.73
4147170-14717074.62174.83
5161472-16147281.87282.10
6160649-16064981.45581.68
20min1150325-15032576.22078.254.0976.5478.584.09
2150026-15002676.06976.39
3152177-15217777.16077.48
4148767-14876775.43175.75
5162499-16249982.39382.74
6162222-16222282.25382.60
30min1153111-15311177.63379.643.8178.0780.093.81
2153787-15378777.97678.41
3154618-15461878.39778.83
4151555-15155576.84477.28
5164713-16471383.51683.99
6164619-16461983.46883.94
45min1155926-15592679.06081.293.4279.6181.863.43
2158621-15862180.42780.97
3157174-15717479.69380.25
4155737-15573778.96579.52
5166605-16660584.47585.07
6167906-16790685.13585.73
60min1159337-15933780.79082.803.1581.4683.493.16
2162031-16203182.15682.82
3161380-16138081.82682.50
4157884-15788480.05380.72
5168553-16855385.46386.19
6170645-17064586.52387.25
极限1192778-19277897.74698.121.1398.5498.931.15
2193820-19382098.27499.07
3193006-19300697.86198.66
4190276-19027696.47797.27
5194178-19417898.45699.31
6196982-19698299.877100.73
达格列净片项目信息
介质体积(ml)1000取样体积(ml)1.5补液体积(ml)1.5
对照品批号D5551-23-012对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)19.2对照品稀释倍数1000
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
112.469849898694989789878999580989080.42
212.459835999006986820.47
单位质量响应值RSD%判断
7938.047926.270.11数据可信
供试品溶液-25012101-2批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min172711-7271173.91871.393.5573.9271.393.55
271639-7163972.82872.83
372631-7263173.83773.84
469497-6949770.65170.65
566741-6674167.84967.85
668142-6814269.27369.27
10min183765-8376585.15683.332.3985.2783.442.38
279695-7969581.01881.13
383477-8347784.86384.97
480019-8001981.34781.45
580992-8099282.33782.44
683878-8387885.27185.37
15min185553-8555386.97385.382.8487.2185.612.83
281739-8173983.09683.33
384246-8424685.64585.88
482003-8200383.36483.59
582558-8255883.92984.15
687830-8783089.28889.52
20min186222-8622287.65385.642.4388.0286.002.42
283690-8369085.07985.43
384065-8406585.46185.83
482300-8230083.66684.02
582063-8206383.42583.78
687080-8708088.52688.89
30min187252-8725288.70187.261.5589.2087.741.55
284370-8437085.77186.25
385540-8554086.96087.45
486970-8697088.41488.89
584220-8422085.61886.09
686634-8663488.07288.57
45min190643-9064392.14890.973.1792.7891.593.16
286733-8673388.17388.78
389685-8968591.17491.80
488031-8803189.49390.10
587366-8736688.81689.42
694437-9443796.00596.64
60min1100513-100513102.18295.484.27102.9596.234.25
291644-9164493.16593.91
390848-9084892.35693.12
495454-9545497.03997.78
589696-8969691.18591.92
695345-9534596.92897.70
极限199113-99113100.75899.670.79101.68100.560.79
297421-9742199.03899.92
397138-9713898.75199.65
497600-9760099.220100.11
598636-98636100.274101.15
698326-9832699.958100.88
点击查看处理图标(人工保存)
　
原始图谱下载图谱(谢超君 于 2025-02-05 14:42:18 完成)
生成报告数据部分下载报告(谢超君 于 2025-02-05 14:42:36 完成)
Current page cost:72 ms