依折麦布阿托伐他汀钙片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DSMF-387-240606对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.75对照品水分(%)0对照品稀释倍数5000
标示量(mg)10供试品稀释倍数5系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.391794041796791795311795201796351795540.06
210.431821131826831823980.23
单位质量响应值RSD%判断
17281.4217487.820.84数据可信
供试品溶液-25012201批-依折麦布-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min17232-72323.7353.8216.153.733.8216.14
27020-70203.6253.63
38382-83824.3294.33
49175-91754.7384.74
55922-59223.0583.06
66601-66013.4093.41
10min114561-145617.5207.673.447.547.693.46
215000-150007.7467.77
315212-152127.8567.88
415541-155418.0268.05
514097-140977.2807.30
614701-147017.5927.61
15min115062-150627.7788.032.147.848.092.10
216008-160088.2678.33
315479-154797.9948.06
415482-154827.9958.07
515815-158158.1678.22
615402-154027.9548.02
20min115290-152907.8967.921.678.008.021.62
215790-157908.1548.26
315033-150337.7637.88
415378-153787.9428.06
515195-151957.8477.95
615282-152827.8928.00
30min114813-148137.6507.781.557.807.931.55
215464-154647.9868.14
314901-149017.6957.85
415173-151737.8368.00
514972-149727.7327.88
615062-150627.7787.93
45min114274-142747.3717.783.737.567.983.69
215862-158628.1918.39
315154-151547.8268.02
415316-153167.9108.11
514603-146037.5417.73
615232-152327.8668.06
60min114540-145407.5097.643.317.747.883.30
215437-154377.9728.22
314852-148527.6707.91
415121-151217.8098.06
514014-140147.2377.47
614821-148217.6547.89
极限114657-146577.5697.753.867.848.033.84
215765-157658.1418.43
315198-151987.8498.13
415350-153507.9278.22
514098-140987.2817.55
614970-149707.7318.01
依折麦布阿托伐他汀钙片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100590-202005对照品来源中检院对照品使用方法直接使用
对照品含量(%)94.9对照品水分(%)0对照品稀释倍数5000
标示量(mg)10供试品稀释倍数5系数0.9671
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.211576251578051574911577631576521576670.08
211.221576191578561577380.11
单位质量响应值RSD%判断
14064.8514058.650.04数据可信
供试品溶液-25012201批-阿托伐他汀钙-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min135582-3558220.90119.5112.5120.9019.5112.51
234008-3400819.97719.98
334905-3490520.50420.50
435078-3507820.60520.61
524805-2480514.57114.57
634940-3494020.52420.52
10min169629-6962940.90136.8311.9641.0236.9411.96
265127-6512738.25638.37
362094-6209436.47536.59
464290-6429037.76537.88
548301-4830128.37228.45
666769-6676939.22139.33
15min180532-8053247.30543.749.0847.6544.069.10
276125-7612544.71745.04
371476-7147641.98642.30
478644-7864446.19646.52
562179-6217936.52536.76
677863-7786345.73746.07
20min189152-8915252.36947.5810.2252.9748.1310.22
282438-8243848.42549.00
377335-7733545.42745.98
487584-8758451.44852.03
566413-6641339.01239.45
683030-8303048.77349.36
30min187797-8779751.57347.967.9552.4748.787.99
282106-8210648.23049.07
379466-7946646.67947.48
486730-8673050.94651.81
569938-6993841.08241.74
683843-8384349.25050.11
45min187778-8777851.56250.127.4052.7551.217.44
288037-8803751.71452.82
384736-8473649.77550.84
490004-9000452.86954.02
572928-7292842.83943.73
688488-8848851.97953.11
60min190705-9070553.28149.728.6054.7551.088.61
286319-8631950.70552.10
383875-8387549.26950.61
488568-8856852.02653.47
570538-7053841.43542.56
687800-8780051.57552.99
极限196948-9694856.94853.917.4058.7155.557.45
292308-9230854.22355.90
391545-9154553.77455.39
496866-9686656.90058.63
578695-7869546.22647.58
694267-9426755.37357.08
依折麦布阿托伐他汀钙片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号DSMF-387-240606对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.75对照品水分(%)0对照品稀释倍数5000
标示量(mg)10供试品稀释倍数5系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.391799311798291799621799671796131798600.09
210.431817241820541818890.13
单位质量响应值RSD%判断
17310.8817439.020.53数据可信
供试品溶液-25012202批-依折麦布-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min18856-88564.5764.276.364.584.286.39
28546-85464.4164.42
38352-83524.3154.32
47565-75653.9093.91
57689-76893.9733.97
68616-86164.4524.45
10min115527-155278.0237.872.868.057.902.88
215149-151497.8277.85
315258-152587.8847.91
414417-144177.4497.47
515607-156078.0648.09
615451-154517.9848.01
15min115794-157948.1618.281.328.238.341.31
216285-162858.4148.48
315907-159078.2198.29
415813-158138.1718.23
516203-162038.3728.44
616133-161338.3368.40
20min115326-153267.9198.282.738.038.392.72
216268-162688.4068.52
315739-157398.1328.25
415943-159438.2388.35
516340-163408.4438.56
616491-164918.5218.64
30min115311-153117.9118.112.498.078.272.48
215916-159168.2248.39
315300-153007.9058.06
415655-156558.0898.24
515633-156338.0788.24
616326-163268.4368.60
45min115259-152597.8848.142.608.098.342.54
215654-156548.0888.30
315485-154858.0018.20
415779-157798.1538.35
515855-158558.1928.40
616460-164608.5058.71
60min116013-160138.2747.942.538.528.192.45
215606-156068.0648.32
314906-149067.7027.95
415180-151807.8438.09
515223-152237.8668.12
615276-152767.8938.15
极限115614-156148.0688.011.688.368.301.69
215695-156958.1108.41
315239-152397.8748.16
415104-151047.8048.09
515609-156098.0658.36
615721-157218.1238.42
依折麦布阿托伐他汀钙片项目信息
介质体积(ml)900取样体积(ml)5补液体积(ml)5
对照品批号100590-202005对照品来源中检院对照品使用方法直接使用
对照品含量(%)94.9对照品水分(%)0对照品稀释倍数5000
标示量(mg)10供试品稀释倍数5系数0.9671
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.213132793133223133603137383130383133470.09
211.223164443169493166960.12
单位质量响应值RSD%判断
27952.4528226.020.69数据可信
供试品溶液-25012202批-阿托伐他汀钙-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min143722-4372212.85714.096.4912.8614.096.47
248760-4876014.33914.34
347832-4783214.06614.07
445329-4532913.33013.33
549219-4921914.47414.47
652553-5255315.45415.45
10min193086-9308627.37428.656.6227.4528.726.61
2103701-10370130.49530.57
392150-9215027.09927.18
491628-9162826.94527.02
597105-9710528.55628.64
6106806-10680631.40831.49
15min1114672-11467233.72234.986.1333.9535.226.12
2123606-12360636.34936.60
3114488-11448833.66733.90
4109471-10947132.19232.42
5122250-12225035.95036.19
6129198-12919837.99338.25
20min1126189-12618937.10839.667.4637.5240.107.44
2136437-13643740.12240.57
3131030-13103038.53238.95
4122962-12296236.15936.56
5144275-14427542.42742.87
6148373-14837343.63244.10
30min1132432-13243238.94440.605.9739.5641.255.97
2137921-13792140.55841.23
3134209-13420939.46740.10
4128308-12830837.73238.33
5145677-14567742.83943.51
6149862-14986244.07044.78
45min1139775-13977541.10442.165.2641.9443.045.26
2140847-14084741.41942.32
3140971-14097141.45542.30
4133710-13371039.32040.13
5153130-15313045.03145.94
6151745-15174544.62445.58
60min1144425-14442542.47141.534.4143.5342.644.41
2140056-14005641.18642.32
3139193-13919340.93242.01
4130509-13050938.37939.41
5148209-14820943.58444.75
6144967-14496742.63043.84
极限1152094-15209444.72645.555.2746.0246.895.27
2155044-15504445.59446.95
3151470-15147044.54345.85
4142916-14291642.02743.27
5165733-16573348.73750.14
6162138-16213847.68049.12
点击查看处理图标(自动生成)
　
原始图谱下载图谱(谢超君 于 2025-02-08 16:56:48 完成)
生成报告数据部分下载报告(谢超君 于 2025-02-08 16:57:05 完成)
Current page cost:78 ms