褪黑素颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号520023-202203对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.066505264144647426523065018648370.66
210.006513865083651100.06
单位质量响应值RSD%判断
6445.036511.000.73数据可信
供试品溶液-25020601批-pH1.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min170225-7022597.47099.311.2397.4799.311.23
272094-72094100.064100.06
372215-72215100.232100.23
470941-7094198.46398.46
572520-72520100.655100.65
671330-7133099.00399.00
10min173312-73312101.754101.220.46101.92101.390.46
272367-72367100.443100.61
372934-72934101.230101.40
472801-72801101.045101.21
573178-73178101.568101.74
672967-72967101.275101.44
15min173116-73116101.482100.630.87101.81100.960.87
271966-7196699.886100.22
372931-72931101.225101.56
472594-72594100.758101.09
571511-7151199.25499.59
672881-72881101.156101.49
20min173200-73200101.599100.661.01102.10101.161.01
272321-72321100.379100.88
372921-72921101.212101.72
471230-7123098.86499.36
573086-73086101.441101.94
672371-72371100.448100.95
30min173022-73022101.352100.440.73102.02101.110.72
271990-7199099.919100.59
372672-72672100.866101.54
471572-7157299.339100.00
572610-72610100.780101.45
672327-72327100.387101.06
45min172357-72357100.42999.581.49101.27100.421.47
272339-72339100.404101.24
372049-72049100.001100.84
471874-7187499.758100.59
569612-6961296.61997.46
672252-72252100.283101.12
60min172344-72344100.41199.081.81101.42100.091.79
272009-7200999.946100.95
372272-72272100.311101.32
470265-7026597.52598.52
572138-72138100.125101.13
669302-6930296.18897.19
极限172862-72862101.13099.730.96102.30100.900.95
272222-72222100.241101.41
371274-7127498.926100.10
471564-7156499.328100.49
572168-72168100.166101.33
671034-7103498.59299.76
褪黑素颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号520023-202203对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.066443864897651546482064854648330.40
210.006000060118600590.14
单位质量响应值RSD%判断
6444.636005.904.99数据不可信!(响应值差异过大,请重新称样测定!)
供试品溶液-25020601批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min168838-6883899.545103.642.0899.54103.642.08
272691-72691105.116105.12
372730-72730105.173105.17
471667-71667103.636103.64
571532-71532103.440103.44
672583-72583104.960104.96
10min172269-72269104.506104.890.45104.67105.060.45
272271-72271104.509104.68
372613-72613105.004105.18
472508-72508104.852105.02
572418-72418104.722104.89
673130-73130105.751105.93
15min172182-72182104.380105.170.45104.72105.520.45
272713-72713105.148105.50
372939-72939105.475105.83
472725-72725105.166105.51
572666-72666105.080105.43
673142-73142105.769106.12
20min172433-72433104.743105.500.64105.26106.020.63
272356-72356104.632105.16
373401-73401106.143106.67
473202-73202105.855106.38
572985-72985105.542106.06
673362-73362106.087106.61
30min172584-72584104.962105.290.47105.65105.980.47
273034-73034105.612106.31
372799-72799105.273105.98
473138-73138105.763106.46
573041-73041105.622106.32
672251-72251104.480105.18
45min172091-72091104.249104.820.37105.11105.700.37
272579-72579104.954105.83
372842-72842105.335106.21
472454-72454104.774105.65
572319-72319104.578105.45
672642-72642105.046105.92
60min171660-71660103.625104.560.63104.66105.600.63
272148-72148104.331105.38
372061-72061104.205105.26
472703-72703105.134106.18
572330-72330104.594105.64
672918-72918105.445106.50
极限171645-71645103.604104.440.66104.81105.660.66
271724-71724103.718104.94
372706-72706105.138106.37
472378-72378104.664105.89
572743-72743105.192106.41
672150-72150104.334105.56
褪黑素颗粒项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号520023-202203对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数10000
标示量(mg)1供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.066491664912650696511064921649860.15
210.006482164746647840.09
单位质量响应值RSD%判断
6459.846478.400.21数据可信
供试品溶液-25020601批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min167858-6785894.31298.602.7994.3198.602.79
272516-72516100.785100.79
371510-7151099.38799.39
469125-6912596.07296.07
572228-72228100.385100.39
672424-72424100.658100.66
10min171883-7188399.906101.741.14100.06101.911.15
274433-74433103.450103.62
373278-73278101.844102.01
473537-73537102.204102.36
573226-73226101.772101.94
672880-72880101.291101.46
15min172915-72915101.340102.290.75101.66102.620.75
274157-74157103.066103.41
373770-73770102.528102.86
474242-74242103.184103.51
573383-73383101.990102.33
673130-73130101.639101.98
20min172410-72410100.638101.950.81101.13102.450.81
274116-74116103.009103.52
373235-73235101.785102.29
473827-73827102.607103.11
573272-73272101.836102.34
673261-73261101.821102.33
30min172510-72510100.777101.590.51101.44102.270.51
273487-73487102.135102.82
372957-72957101.398102.07
473433-73433102.060102.73
572945-72945101.382102.06
673246-73246101.800102.48
45min172745-72745101.104101.670.63101.93102.510.63
273695-73695102.424103.28
372902-72902101.322102.17
473757-73757102.510103.35
573052-73052101.530102.38
672758-72758101.122101.97
60min172322-72322100.516101.470.59101.51102.480.59
273432-73432102.058103.08
373145-73145101.660102.67
473363-73363101.963102.98
573078-73078101.566102.58
672695-72695101.034102.05
极限171819-7181999.817101.260.79100.98102.440.79
273416-73416102.036103.23
372913-72913101.337102.52
473312-73312101.892103.08
572970-72970101.416102.60
672721-72721101.070102.25
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