非奈利酮片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D231201对照品来源自制对照品使用方法直接使用
对照品含量(%)99.92对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.05378423441437862037794137744730336955.09
211.123799093783243791160.30
单位质量响应值RSD%判断
27454.2134093.1715.26数据不可信!(响应值差异过大,请重新称样测定!)
供试品溶液-1批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min151612-5161215.26014.238.9115.2614.238.91
244978-4497813.29813.30
353618-5361815.85315.85
445737-4573713.52313.52
542663-4266312.61412.61
650112-5011214.81614.82
10min1136282-13628240.29439.427.1540.3239.457.16
2130426-13042638.56238.58
3146214-14621443.23043.26
4135362-13536240.02240.04
5117052-11705234.60834.63
6134715-13471539.83039.86
15min1221686-22168665.54564.366.1265.6464.456.12
2213547-21354763.13863.22
3233738-23373869.10869.21
4222270-22227065.71765.81
5193956-19395657.34657.42
6220874-22087465.30465.40
20min1294205-29420586.98685.213.8187.1985.413.82
2281270-28127083.16183.35
3299370-29937088.51388.73
4294554-29455487.08987.29
5269544-26954479.69479.87
6290318-29031885.83786.04
30min1339899-339899100.49699.811.17100.84100.141.18
2333103-33310398.48798.82
3343950-343950101.694102.05
4337787-33778799.871100.22
5334593-33459398.92799.23
6336083-33608399.36899.71
45min1362673-362673107.229106.771.09107.74107.281.09
2355955-355955105.243105.74
3367117-367117108.543109.07
4361968-361968107.021107.53
5361136-361136106.775107.25
6357871-357871105.810106.32
60min1374173-374173110.629109.911.04111.32110.601.04
2366925-366925108.486109.16
3377078-377078111.488112.20
4372352-372352110.091110.78
5372135-372135110.027110.68
6367834-367834108.755109.44
极限1381500-381500112.796112.180.92113.67113.040.93
2374720-374720110.791111.64
3384017-384017113.540114.44
4379904-379904112.324113.20
5380348-380348112.455113.29
6375927-375927111.148112.01
非奈利酮片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D231201对照品来源自制对照品使用方法直接使用
对照品含量(%)99.92对照品水分(%)0对照品稀释倍数500
标示量(mg)20供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
111.053811813817473806613808763804543809840.14
211.123801283800063800670.03
单位质量响应值RSD%判断
34478.1934178.690.62数据可信
供试品溶液-2批-pH4.5
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min124262-242626.3566.8044.786.366.8044.76
218195-181954.7674.77
325402-254026.6556.65
420237-202375.3015.30
518793-187934.9234.92
648948-4894812.82312.82
10min198116-9811625.70321.3338.0125.7121.3438.01
248866-4886612.80112.81
388391-8839123.15623.17
458152-5815215.23415.24
563281-6328116.57816.59
6131710-13171034.50434.53
15min1181820-18182047.63141.0829.5147.6841.1229.52
299510-9951026.06826.10
3170492-17049244.66444.71
4124338-12433832.57332.61
5136201-13620135.68035.72
6228427-22842759.84159.92
20min1269525-26952570.60761.9220.5470.7462.0320.56
2163495-16349542.83142.90
3266890-26689069.91770.04
4212398-21239855.64255.73
5212162-21216255.58055.68
6293612-29361276.91777.10
30min1322252-32225284.42078.3310.3084.6778.5510.34
2255021-25502166.80766.95
3323929-32392984.85985.10
4278416-27841672.93673.12
5284007-28400774.40174.59
6330480-33048086.57586.88
45min1349414-34941491.53587.596.0791.9387.946.12
2306568-30656880.31180.57
3349709-34970991.61391.99
4317259-31725983.11283.41
5327042-32704285.67585.99
6356103-35610393.28893.74
60min1360040-36004094.31991.174.5794.8691.664.63
2326924-32692485.64486.03
3362506-36250694.96595.50
4334720-33472087.68688.13
5340591-34059189.22489.68
6363242-36324295.15895.76
极限1368819-36881996.61994.882.7497.3295.522.81
2350734-35073491.88192.41
3372747-37274797.64898.34
4351106-35110691.97992.57
5358982-35898294.04294.65
6370649-37064997.09897.86
点击查看处理图标(自动生成)
　
原始图谱下载图谱(谢超君 于 2025-02-21 13:18:02 完成)
生成报告数据部分(等待生成报告)
Current page cost:39 ms