多替诺雷片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号241101对照品来源原料对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数5000
标示量(mg)2供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.124847948494487264860648433485480.25
210.164936849039492040.48
单位质量响应值RSD%判断
4797.234842.910.68数据可信
供试品溶液-25021401批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min121213-2121339.57040.3012.6239.5740.3012.62
224744-2474446.15746.16
323032-2303242.96342.96
422760-2276042.45642.46
521103-2110339.36539.36
616759-1675931.26231.26
10min132408-3240860.45359.666.7760.5259.736.76
233280-3328062.07962.16
327716-2771651.70051.77
433597-3359762.67162.74
532831-3283161.24261.31
632061-3206159.80659.86
15min136654-3665468.37368.354.0468.5468.524.04
237809-3780970.52870.71
333919-3391963.27163.43
438107-3810771.08471.26
536646-3664668.35868.53
636714-3671468.48568.64
20min139373-3937373.44573.132.7773.7373.412.78
239841-3984174.31874.62
337149-3714969.29669.56
440279-4027975.13575.43
539139-3913973.00973.29
639446-3944673.58173.85
30min142154-4215478.63378.621.5379.0479.021.54
242451-4245179.18779.61
341319-4131977.07577.45
443171-4317180.53080.95
541660-4166077.71178.11
642131-4213178.59078.98
45min144006-4400682.08782.370.8082.6282.910.80
244221-4422182.48883.04
344276-4427682.59183.10
444653-4465383.29483.85
543589-4358981.30981.84
644212-4421282.47282.99
60min144353-4435382.73583.711.0483.4184.381.03
244878-4487883.71484.41
345588-4558885.03885.68
445155-4515584.23184.92
544399-4439982.82083.49
644889-4488983.73484.39
极限146931-4693187.54487.390.8888.3588.200.87
246831-4683187.35788.19
346997-4699787.66788.45
447439-4743988.49189.32
546193-4619386.16786.97
646695-4669587.10387.90
多替诺雷片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号241101对照品来源原料对照品使用方法直接使用
对照品含量(%)99.9对照品水分(%)0对照品稀释倍数5000
标示量(mg)2供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.124925148811490564923848866490440.42
210.165021149984500980.33
单位质量响应值RSD%判断
4846.254930.911.23数据可信
供试品溶液-25021801批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min125693-2569347.25842.2912.0247.2642.2912.02
217886-1788632.89832.90
324100-2410044.32844.33
423898-2389843.95643.96
524346-2434644.78044.78
622029-2202940.51840.52
10min135237-3523764.81262.275.8264.8962.345.83
230033-3003355.24055.30
334988-3498864.35464.43
434648-3464863.72963.80
534760-3476063.93564.01
633476-3347661.57361.64
15min139831-3983173.26270.014.3373.4570.194.34
235869-3586965.97566.12
339170-3917072.04672.23
438724-3872471.22671.41
538637-3863771.06671.25
636161-3616166.51266.68
20min142050-4205077.34474.353.2677.6574.643.27
238742-3874271.25971.52
341004-4100475.42075.72
441031-4103175.46975.77
540815-4081575.07275.37
638895-3889571.54171.82
30min143893-4389380.73378.912.6781.1779.332.68
241478-4147876.29176.67
343479-4347979.97280.40
443760-4376080.48980.91
543387-4338779.80380.23
641415-4141576.17676.58
45min145903-4590384.43082.461.9985.0083.002.00
244562-4456281.96482.47
344979-4497982.73183.29
445477-4547783.64784.21
544747-4474782.30482.86
643313-4331379.66780.19
60min146561-4656185.64183.971.8586.3584.661.86
245746-4574684.14284.78
345685-4568584.03084.73
446322-4632285.20185.90
545454-4545483.60584.30
644159-4415981.22381.88
极限148155-4815588.57387.701.3389.4388.531.34
247667-4766787.67588.45
347758-4775887.84288.68
448378-4837888.98389.82
547581-4758187.51788.35
646559-4655985.63786.43
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