XXYYYY片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.123980570398281739820973978787397622839801000.07
210.183986624398148539840540.10
单位质量响应值RSD%判断
393290.51391360.900.35数据可信
供试品溶液-24032106批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min13824858-382485887.39290.635.8187.3990.635.81
24264903-426490397.44797.45
34122395-412239594.19194.19
43606910-360691082.41282.41
54014834-401483491.73391.73
63965884-396588490.61590.61
10min14501885-4501885102.861102.541.37103.01102.691.36
24571774-4571774104.458104.62
34443910-4443910101.537101.69
44513767-4513767103.133103.27
54499593-4499593102.809102.96
64394793-4394793100.414100.57
15min14552558-4552558104.019103.361.44104.34103.681.43
24585227-4585227104.766105.10
34461000-4461000101.927102.25
44541777-4541777103.773104.08
54574761-4574761104.526104.85
64426479-4426479101.138101.46
20min14555888-4555888104.095103.361.61104.59103.851.61
24600286-4600286105.110105.62
34455687-4455687101.806102.30
44530690-4530690103.519104.00
54581427-4581427104.679105.18
64417064-4417064100.923101.41
30min14558906-4558906104.164103.331.71104.83104.001.71
24610025-4610025105.332106.02
34446542-4446542101.597102.26
44526219-4526219103.417104.07
54578917-4578917104.621105.29
64413652-4413652100.845101.50
XXYYYY片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.123985030398600439858693983312398534039851110.03
210.183984869397604439804560.16
单位质量响应值RSD%判断
393785.67391007.470.51数据可信
供试品溶液-B001批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min14023508-402350891.91572.0714.2191.9272.0714.22
22990247-299024768.31168.31
32946890-294689067.32067.32
43003288-300328868.60968.61
52761780-276178063.09263.09
63203919-320391973.19273.19
10min14483123-4483123102.415102.171.16102.57102.291.16
24532408-4532408103.541103.65
34521223-4521223103.285103.40
44392977-4392977100.355100.47
54442187-4442187101.480101.58
64462406-4462406101.942102.06
15min14493014-4493014102.641102.510.97102.96102.800.97
24544191-4544191103.810104.10
34517274-4517274103.195103.48
44416527-4416527100.893101.18
54477718-4477718102.291102.57
64474860-4474860102.226102.52
20min14473917-4473917102.204102.510.88102.70102.970.88
24538384-4538384103.677104.14
34518808-4518808103.230103.69
44424469-4424469101.075101.52
54484320-4484320102.442102.89
64482891-4482891102.410102.87
30min14481911-4481911102.387102.430.93103.05103.060.93
24535190-4535190103.604104.24
34505639-4505639102.929103.56
44410599-4410599100.758101.38
54491028-4491028102.595103.21
64478350-4478350102.306102.94
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