乌帕替尼缓释片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D240501对照品来源自制对照品使用方法直接使用
对照品含量(%)97.44对照品水分(%)0对照品稀释倍数1000
标示量(mg)15供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
115.231716021719051716821720461716181717710.12
215.221717421712401714910.21
单位质量响应值RSD%判断
11278.4611267.480.07数据可信
供试品溶液-25022001-2-2批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
30min127570-2757014.29814.047.5814.3014.047.58
226164-2616413.56913.57
325598-2559813.27613.28
427001-2700114.00314.00
525205-2520513.07213.07
630849-3084915.99916.00
60min150035-5003525.94924.813.1225.9724.843.11
248219-4821925.00725.03
346356-4635624.04124.06
448816-4881625.31725.34
546153-4615323.93623.96
647477-4747724.62324.65
120min181379-8137942.20540.782.1242.2740.852.12
278498-7849840.71140.78
376803-7680339.83239.89
479738-7973841.35441.42
577630-7763040.26140.32
677785-7778540.34140.41
240min1120516-12051662.50261.581.5062.6461.711.50
2117201-11720160.78360.92
3117347-11734760.85960.99
4121282-12128262.89963.03
5117369-11736960.87061.00
6118657-11865761.53861.67
360min1149338-14933877.45074.962.1577.6975.202.14
2140440-14044072.83573.07
3144588-14458874.98675.22
4142213-14221373.75573.99
5146157-14615775.80076.03
6144517-14451774.95075.19
480min1165290-16529085.72385.321.8086.0985.681.79
2159870-15987082.91283.27
3165729-16572985.95186.31
4168436-16843687.35487.72
5162555-16255584.30484.66
6165240-16524085.69786.06
600min1175257-17525790.89290.301.7491.4190.801.73
2169393-16939387.85188.34
3174894-17489490.70491.20
4178288-17828892.46492.97
5172232-17223289.32389.82
6174577-17457790.53991.04
720min1181822-18182294.29793.911.7794.9694.561.76
2174876-17487690.69491.33
3181773-18177394.27194.92
4184096-18409695.47696.14
5181348-18134894.05194.70
6182540-18254094.66995.33
960min1187654-18765497.32196.761.7798.1497.571.76
2180922-18092293.83094.62
3187867-18786797.43298.24
4190836-19083698.97299.79
5185498-18549896.20397.01
6186677-18667796.81597.63
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
1200min1190390-19039098.74098.391.7499.7299.361.73
2183730-18373095.28696.23
3191551-19155199.342100.31
4193227-193227100.212101.20
5188673-18867397.85098.81
6190667-19066798.88499.86
1440min1192427-19242799.79799.101.70100.95100.241.70
2186232-18623296.58497.69
3193225-193225100.211101.35
4195046-195046101.155102.31
5188416-18841697.71798.84
6191187-19118799.154100.29
极限1194120-194120100.67599.732.94101.99101.032.92
2184576-18457695.72596.99
3193408-193408100.305101.61
4201090-201090104.290105.61
5188145-18814597.57698.86
6192481-19248199.825101.13
乌帕替尼缓释片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D240501对照品来源自制对照品使用方法直接使用
对照品含量(%)97.44对照品水分(%)0对照品稀释倍数1000
标示量(mg)15供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
115.231716241722191717321717441719331718500.14
215.221722991716091719540.29
单位质量响应值RSD%判断
11283.6511297.900.09数据可信
供试品溶液-25022001-2-3批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
30min126073-2607313.50113.143.5013.5013.143.49
223880-2388012.36512.37
325546-2554613.22813.23
425034-2503412.96312.96
525277-2527713.08913.09
626399-2639913.66913.67
60min147518-4751824.60523.954.3124.6323.974.31
242663-4266322.09122.11
346568-4656824.11324.14
445346-4534623.48023.50
547336-4733624.51124.53
648049-4804924.88024.90
120min179311-7931141.06839.723.9141.1339.783.90
271589-7158937.06937.13
377016-7701639.87939.94
474914-7491438.79138.85
579227-7922741.02441.09
678174-7817440.47940.54
240min1118894-11889461.56460.153.1561.7060.273.15
2109817-10981756.86456.98
3117489-11748960.83660.96
4113875-11387558.96559.09
5119356-11935661.80361.93
6117508-11750860.84660.98
360min1145477-14547775.32873.673.1375.5673.903.13
2136206-13620670.52870.74
3141684-14168473.36473.59
4139367-13936772.16572.39
5148830-14883077.06577.30
6142085-14208573.57273.81
480min1164940-16494085.40784.051.7685.7784.401.76
2159700-15970082.69383.02
3160185-16018582.94483.30
4160341-16034183.02583.37
5166594-16659486.26386.63
6162184-16218483.97984.34
600min1173148-17314889.65788.951.6490.1689.441.65
2167837-16783786.90787.38
3170565-17056588.31988.81
4170203-17020388.13288.61
5175860-17586091.06191.57
6173047-17304789.60490.10
720min1181512-18151293.98892.411.7394.6493.051.74
2174665-17466590.44291.06
3176685-17668591.48892.13
4177241-17724191.77692.41
5182810-18281094.66095.32
6177884-17788492.10992.75
960min1185933-18593396.27795.831.5397.0996.621.54
2182210-18221094.34995.11
3183192-18319294.85795.65
4183680-18368095.11095.89
5190117-19011798.44399.26
6185279-18527995.93896.74
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
1200min1189342-18934298.04297.831.4599.0198.781.45
2186559-18655996.60197.52
3186540-18654096.59197.54
4187337-18733797.00497.94
5193565-193565100.229101.21
6190232-19023298.50399.46
1440min1189547-18954798.14898.401.4499.2899.521.44
2187255-18725596.96198.04
3188070-18807097.38398.49
4189174-18917497.95599.06
5194817-194817100.877102.02
6191337-19133799.075100.20
极限1189806-18980698.28298.981.4299.58100.261.41
2194130-194130100.521101.77
3188311-18831197.50898.78
4188948-18894897.83899.10
5194739-194739100.837102.15
6191032-19103298.917100.20
点击查看处理图标(人工保存)
　
原始图谱下载图谱(谢超君 于 2025-02-27 16:09:13 完成)
生成报告数据部分下载报告(谢超君 于 2025-02-27 16:09:30 完成)
Current page cost:105 ms