美阿沙坦钾片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号D211-4R701-2402002对照品来源自制工作对照品对照品使用方法直接使用
对照品含量(%)99.5对照品水分(%)0对照品稀释倍数1000
标示量(mg)80供试品稀释倍数5系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
118.032084952075442084212074362079132079620.24
218.072075182071092073140.14
单位质量响应值RSD%判断
11534.2211472.830.38数据可信
供试品溶液-2025010221批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1815-8150.3970.448.350.400.458.46
2959-9590.4670.47
3913-9130.4440.44
4937-9370.4560.46
5838-8380.4080.41
61019-10190.4960.50
10min11879-18790.9140.892.570.920.902.53
21810-18100.8810.89
31874-18740.9120.92
41751-17510.8520.86
51819-18190.8850.89
61823-18230.8870.89
15min12287-22871.1131.114.291.131.124.42
22195-21951.0681.08
32448-24481.1911.21
42325-23251.1311.15
52211-22111.0761.09
62205-22051.0731.09
20min12558-25581.2451.272.311.271.302.22
22545-25451.2381.27
32619-26191.2741.30
42693-26931.3101.34
52664-26641.2961.32
62574-25741.2521.28
30min13404-34041.6561.622.711.701.662.78
23150-31501.5331.57
33388-33881.6481.69
43329-33291.6201.66
53326-33261.6181.66
63336-33361.6231.66
45min14395-43952.1382.242.522.202.302.39
24715-47152.2942.35
34686-46862.2802.34
44580-45802.2282.29
54603-46032.2402.30
64664-46642.2692.33
60min15993-59932.9162.991.733.003.071.69
26126-61262.9813.06
36320-63203.0753.16
46111-61112.9733.06
56159-61592.9973.08
66114-61142.9753.06
极限16798-67983.3073.412.043.423.522.00
26842-68423.3293.45
37096-70963.4523.57
47088-70883.4493.57
57098-70983.4533.57
67094-70943.4523.57
美阿沙坦钾片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号D211-4R701-2402002对照品来源自制工作对照品对照品使用方法直接使用
对照品含量(%)99.5对照品水分(%)0对照品稀释倍数1000
标示量(mg)80供试品稀释倍数5系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
118.032077702084102079402070872080242078460.24
218.072062282072992067640.37
单位质量响应值RSD%判断
11527.7911442.390.53数据可信
供试品溶液-2025010221批
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11092-10920.5320.5113.600.530.5113.74
21047-10470.5100.51
31188-11880.5790.58
41145-11450.5580.56
5782-7820.3810.38
61045-10450.5090.51
10min11910-19100.9310.943.210.940.953.40
21894-18940.9230.93
31948-19480.9490.96
41914-19140.9330.94
51888-18880.9200.92
62055-20551.0011.01
15min12416-24161.1771.184.171.191.204.09
22326-23261.1341.15
32595-25951.2651.28
42466-24661.2021.22
52324-23241.1331.15
62453-24531.1951.21
20min12742-27421.3361.373.691.371.403.68
22746-27461.3381.37
32934-29341.4301.46
42766-27661.3481.38
52724-27241.3271.35
62950-29501.4381.47
30min13440-34401.6761.673.351.721.723.39
23317-33171.6161.66
33576-35761.7431.79
43522-35221.7161.76
53283-32831.6001.64
63471-34711.6911.74
45min14753-47532.3162.322.562.382.392.59
24649-46492.2662.33
34863-48632.3702.44
44792-47922.3352.40
54623-46232.2532.31
64940-49402.4072.47
60min16258-62583.0503.082.953.143.172.96
26024-60242.9363.02
36535-65353.1853.28
46468-64683.1523.24
56224-62243.0333.12
66388-63883.1133.20
极限17102-71023.4613.491.023.583.611.05
27142-71423.4803.60
37176-71763.4973.63
47240-72403.5283.65
57056-70563.4393.56
67233-72333.5253.65
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