诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.123974767397613739792673975379397519039761480.05
210.183970191397035239702720.01
单位质量响应值RSD%判断
392900.00390007.070.53数据可信
供试品溶液-24032106批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1741369-74136916.97716.8511.7316.9816.8511.72
2781943-78194317.90617.91
3879089-87908920.13120.13
4637907-63790714.60814.61
5693192-69319215.87415.87
6680188-68018815.57615.58
10min11884639-188463943.15741.306.3543.1941.336.36
21861375-186137542.62542.65
31959580-195958044.87444.91
41732664-173266439.67739.70
51714749-171474939.26739.29
61668202-166820238.20138.23
15min12691774-269177461.64059.875.4361.7459.965.44
22658823-265882360.88660.99
32836055-283605564.94465.05
42552594-255259458.45358.54
52472197-247219756.61256.70
62474920-247492056.67556.76
20min13220320-322032073.74473.094.4273.9573.294.42
23247918-324791874.37674.58
33425502-342550278.44378.66
43135909-313590971.81172.00
53020642-302064269.17169.36
63100873-310087371.00971.19
30min13800804-380080487.03787.093.6687.3687.413.67
23859623-385962388.38488.71
34028616-402861692.25492.60
43702309-370230984.78185.09
53622573-362257382.95583.26
63805943-380594387.15587.46
45min14092249-409224993.71194.533.7494.1895.003.74
24250806-425080697.34297.82
34327672-432767299.10299.60
43954073-395407390.54791.00
53957757-395775790.63191.07
64185669-418566995.85096.30
60min14264801-426480197.66297.563.1598.2998.183.15
24343804-434380499.471100.11
34398354-4398354100.720101.39
44044913-404491392.62793.23
54162408-416240895.31795.91
64347732-434773299.561100.17
极限14419493-4419493101.205100.431.48101.99101.211.50
24422667-4422667101.277102.08
34446582-4446582101.825102.66
44265257-426525797.67398.43
54368519-4368519100.037100.79
64391085-4391085100.554101.33
诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.123964014396365039710323964072396589039657320.08
210.183970352395933839648450.20
单位质量响应值RSD%判断
391870.75389473.970.44数据可信
供试品溶液-B001批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1414935-4149359.5219.289.029.529.289.02
2461094-46109410.58010.58
3425667-4256679.7679.77
4382949-3829498.7878.79
5361775-3617758.3018.30
6380102-3801028.7228.72
10min11128344-112834425.89026.105.1625.9126.125.17
21248684-124868428.65128.67
31151826-115182626.42926.45
41093786-109378625.09725.11
51094089-109408925.10425.12
61109527-110952725.45825.47
15min11899230-189923043.57843.852.3743.6443.912.37
21984696-198469645.53945.60
31929903-192990344.28244.34
41858679-185867942.64842.70
51920879-192087944.07544.13
61872789-187278942.97243.03
20min12534878-253487858.16358.641.8058.3058.781.79
22623335-262333560.19360.33
32575079-257507959.08659.22
42501216-250121657.39157.52
52582455-258245559.25559.38
62518040-251804057.77757.91
30min13403150-340315078.08678.221.2278.3178.441.23
23443225-344322579.00679.25
33432046-343204678.74978.98
43375860-337586077.46077.68
53452287-345228779.21479.44
63346549-334654976.78777.01
45min14050791-405079192.94793.401.1893.3193.761.18
24103522-410352294.15694.53
34104010-410401094.16894.53
44018986-401898692.21792.57
54128567-412856794.73195.09
64017164-401716492.17592.53
60min14305279-430527998.78698.861.3499.3099.381.34
24325363-432536399.24799.78
34364697-4364697100.149100.67
44220537-422053796.84197.35
54368601-4368601100.239100.76
64266395-426639597.89498.40
极限14348270-434827099.772100.211.13100.45100.891.12
24343640-434364099.666100.36
34403372-4403372101.037101.72
44344002-434400299.674100.34
54448646-4448646102.075102.76
64315837-431583799.02899.70
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