辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.962687642691442680192681302689962686110.19
29.942682582687682685130.14
单位质量响应值RSD%判断
26968.9827013.380.12数据可信
供试品溶液-25021902-yd1批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1159405-15940558.94058.251.4158.9458.251.40
2158363-15836358.55558.55
3160382-16038259.30159.30
4155244-15524457.40257.40
5155024-15502457.32057.32
6156830-15683057.98857.99
10min1189969-18996970.24171.791.1970.4271.961.19
2196569-19656972.68272.86
3194263-19426371.82972.01
4195673-19567372.35072.52
5193532-19353271.55971.73
6194908-19490872.06772.24
15min1208216-20821676.98878.420.9477.3878.810.94
2213060-21306078.77979.17
3212207-21220778.46478.86
4213223-21322378.83979.23
5212160-21216078.44678.83
6213672-21367279.00579.40
20min1218144-21814480.65982.161.1781.2882.781.17
2224600-22460083.04683.68
3220055-22005581.36581.99
4223743-22374382.72983.35
5222393-22239382.23082.85
6224290-22429082.93183.56
30min1225972-22597283.55385.631.5184.4186.501.50
2232886-23288686.11086.99
3228967-22896784.66185.53
4235237-23523786.97987.85
5232400-23240085.93086.80
6234104-23410486.56087.44
45min1231779-23177985.70087.491.3486.8188.621.33
2238117-23811788.04489.18
3233526-23352686.34687.47
4238651-23865188.24189.38
5238147-23814788.05589.18
6239447-23944788.53689.67
60min1234622-23462286.75288.441.4488.1289.841.43
2240291-24029188.84890.25
3235484-23548487.07088.46
4241160-24116089.16990.57
5240160-24016088.79990.19
6243463-24346390.02191.42
极限1264522-26452297.80797.861.1999.4499.521.18
2268707-26870799.355101.02
3259971-25997196.12497.77
4263232-26323297.33099.00
5264022-26402297.62299.28
6267515-26751598.914100.59
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.962693502686192689982689052692762690300.11
29.942685382680812683100.13
单位质量响应值RSD%判断
27011.0426992.960.05数据可信
供试品溶液-25021902yd2批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1180331-18033166.65161.394.4166.6561.394.41
2163584-16358460.46160.46
3165965-16596561.34161.34
4161423-16142359.66259.66
5165236-16523661.07261.07
6160112-16011259.17859.18
10min1213467-21346778.89874.403.2379.1074.583.24
2199452-19945273.71873.90
3203520-20352075.22175.41
4196734-19673472.71372.89
5198273-19827373.28273.47
6196315-19631572.55872.74
15min1227285-22728584.00580.482.3284.4480.882.32
2216634-21663480.06880.47
3218522-21852280.76681.18
4214779-21477979.38379.78
5216243-21624379.92480.33
6212963-21296378.71279.11
20min1233879-23387986.44283.761.8687.1384.411.87
2223247-22324782.51383.16
3229498-22949884.82385.47
4225346-22534683.28883.92
5223987-22398782.78683.43
6223849-22384982.73583.37
30min1236908-23690887.56286.421.0588.5187.321.07
2232887-23288786.07686.97
3236691-23669187.48288.39
4232409-23240985.89986.78
5233121-23312186.16287.05
6230834-23083485.31786.20
45min1240433-24043388.86588.270.8790.0889.430.88
2237161-23716187.65588.80
3242155-24215589.50190.67
4238277-23827788.06889.21
5238022-23802287.97389.12
6236883-23688387.55288.69
60min1240224-24022488.78788.630.8990.2690.050.89
2236094-23609487.26188.67
3242491-24249189.62591.06
4239081-23908188.36589.77
5240585-24058588.92190.33
6240329-24032988.82690.22
极限1271569-271569100.37399.671.57102.12101.361.56
2274756-274756101.550103.22
3272213-272213100.611102.32
4270169-27016999.855101.53
5265812-26581298.24599.93
6263491-26349197.38799.05
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