辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.962672722665662670692660812666362667250.18
29.942671202667352669280.11
单位质量响应值RSD%判断
26779.6226853.920.20数据可信
供试品溶液-236B11S批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1219931-21993181.84983.251.6781.8583.251.67
2221945-22194582.59882.60
3229451-22945185.39285.39
4224811-22481183.66583.66
5225931-22593184.08284.08
6220131-22013181.92381.92
10min1243547-24354790.63790.681.7590.8890.931.75
2239758-23975889.22789.48
3250263-25026393.13793.39
4245743-24574391.45591.71
5244213-24421390.88591.14
6238456-23845688.74388.99
15min1251850-25185093.72793.061.2694.2493.581.26
2246529-24652991.74792.26
3253894-25389494.48895.02
4252536-25253693.98394.51
5248902-24890292.63093.16
6246690-24669091.80792.32
20min1253360-25336094.28993.801.4195.0994.601.41
2248890-24889092.62693.42
3256504-25650495.45996.28
4254003-25400394.52995.34
5252673-25267394.03494.84
6246845-24684591.86592.65
30min1253674-25367494.40694.131.3695.4995.211.36
2250529-25052993.23694.30
3257456-25745695.81496.92
4255566-25556695.11096.20
5252349-25234993.91395.00
6247968-24796892.28393.35
45min1251961-25196193.76993.661.4895.1395.031.48
2248914-24891492.63593.98
3255695-25569595.15896.55
4255314-25531495.01796.39
5252166-25216693.84595.21
6246031-24603191.56292.90
60min1251640-25164093.64993.191.5795.3094.841.57
2249172-24917292.73194.36
3255123-25512394.94696.62
4252928-25292894.12995.79
5249958-24995893.02394.67
6243673-24367390.68492.30
极限1260768-26076897.04696.841.2498.9798.761.24
2258352-25835296.14798.05
3263810-26381098.178100.14
4264161-26416198.309100.25
5257510-25751095.83497.76
6256705-25670595.53497.42
辅酶Q10片项目信息
介质体积(ml)500取样体积(ml)1.5补液体积(ml)1.5
对照品批号140611-202107对照品来源中检所对照品使用方法直接使用
对照品含量(%)99.8对照品水分(%)0对照品稀释倍数500
标示量(mg)10供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
19.962665172660512667752667132669102665930.13
29.942675612669132672370.18
单位质量响应值RSD%判断
26766.3726885.010.32数据可信
供试品溶液-243B62S批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min1201331-20133174.90276.382.4174.9076.382.42
2212747-21274779.14979.15
3207235-20723577.09877.10
4206775-20677576.92776.93
5198590-19859073.88273.88
6205099-20509976.30476.30
10min1226383-22638384.22285.881.6184.4586.111.62
2236720-23672088.06888.31
3230882-23088285.89686.13
4232861-23286186.63286.86
5227644-22764484.69184.91
6230508-23050885.75785.99
15min1238069-23806988.57089.081.0089.0589.561.00
2243644-24364490.64491.15
3239519-23951989.10989.60
4239716-23971689.18289.67
5236552-23655288.00588.48
6239106-23910688.95589.44
20min1241955-24195590.01590.290.9990.7691.041.00
2246632-24663291.75592.53
3240718-24071889.55590.31
4243234-24323490.49191.25
5239931-23993189.26290.00
6243632-24363290.63991.39
30min1242315-24231590.14990.620.9291.1691.650.92
2246839-24683991.83292.88
3242928-24292890.37791.40
4243977-24397790.76891.80
5240453-24045389.45790.46
6245023-24502391.15792.18
45min1241943-24194390.01190.420.8291.2991.720.83
2244892-24489291.10892.43
3241126-24112689.70791.00
4244155-24415590.83492.14
5240823-24082389.59490.87
6245348-24534891.27892.58
60min1241499-24149989.84690.451.0891.4092.011.08
2246766-24676691.80593.40
3240457-24045789.45891.02
4243441-24344190.56892.14
5240938-24093889.63791.18
6245582-24558291.36592.94
极限1256488-25648895.42295.040.7797.2596.880.78
2257375-25737595.75297.63
3253909-25390994.46396.30
4255421-25542195.02596.87
5252394-25239493.89995.71
6257107-25710795.65297.50
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