诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.123950406395042039476213951106395166939502440.04
210.183952979396901039609940.29
单位质量响应值RSD%判断
390340.32389095.680.23数据可信
供试品溶液-24032201批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min13195931-319593173.51177.245.9773.5177.245.96
23059318-305931870.36870.37
33509114-350911480.71480.71
43351475-335147577.08877.09
53593870-359387082.66482.66
63437467-343746779.06679.07
10min14536609-4536609104.348102.831.85104.47102.961.85
24466586-4466586102.737102.85
34542962-4542962104.494104.63
44396547-4396547101.126101.25
54532599-4532599104.256104.39
64348186-4348186100.014100.15
15min14549618-4549618104.647103.221.94104.94103.521.94
24493041-4493041103.346103.63
34573359-4573359105.193105.50
44407371-4407371101.375101.67
54544253-4544253104.524104.84
64357423-4357423100.226100.52
20min14546909-4546909104.585102.991.90105.06103.461.90
24484474-4484474103.149103.61
34551774-4551774104.697105.18
44394835-4394835101.087101.55
54534278-4534278104.294104.78
64352137-4352137100.105100.57
30min14536491-4536491104.345102.851.86104.99103.491.86
24479381-4479381103.032103.66
34541919-4541919104.470105.13
44397393-4397393101.146101.78
54529200-4529200104.178104.84
64343271-434327199.901100.53
诺氟沙星胶囊项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号130450-201907对照品来源中检院对照品使用方法直接使用
对照品含量(%)99.60对照品水分(%)0对照品稀释倍数100
标示量(mg)100 供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.123953087395451939523073952655395200939529150.03
210.183944213394464539444290.01
单位质量响应值RSD%判断
390604.25387468.470.57数据可信
供试品溶液-24032202批-pH1.2
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min13482578-348257880.24582.4611.1080.2582.4611.10
23334973-333497376.84476.84
33041404-304140470.08070.08
43561872-356187282.07282.07
54150564-415056495.63795.64
63900795-390079589.88289.88
10min14464837-4464837102.878101.741.08103.01101.881.09
24392205-4392205101.205101.33
34336705-433670599.926100.04
44406485-4406485101.534101.67
54451178-4451178102.564102.72
64440974-4440974102.329102.48
15min14468169-4468169102.955101.880.81103.26102.190.82
24394896-4394896101.267101.56
34377499-4377499100.866101.15
44402494-4402494101.442101.75
54452698-4452698102.599102.93
64434235-4434235102.173102.49
20min14459389-4459389102.753101.870.75103.23102.340.76
24390240-4390240101.160101.63
34375180-4375180100.813101.26
44416451-4416451101.764102.24
54446153-4446153102.448102.95
64438378-4438378102.269102.76
30min14455744-4455744102.669101.630.76103.32102.280.77
24382393-4382393100.979101.61
34372056-4372056100.741101.36
44391957-4391957101.199101.84
54433858-4433858102.165102.84
64429017-4429017102.053102.71
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