多替诺雷片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D241101对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.69对照品水分(%)0对照品稀释倍数5000
标示量(mg)2供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.004742746996473064705447071471710.40
29.994774347687477150.09
单位质量响应值RSD%判断
4717.104776.280.89数据可信
供试品溶液-25030601批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min119006-1900635.92633.9110.7835.9333.9110.79
218570-1857035.10235.10
320134-2013438.05838.06
416066-1606630.36930.37
515084-1508428.51328.51
618766-1876635.47335.47
10min128223-2822353.34952.524.9753.4152.574.98
228376-2837653.63853.70
329393-2939355.56055.62
426573-2657350.23050.28
525669-2566948.52148.57
628459-2845953.79553.85
15min133278-3327862.90462.362.6663.0562.502.67
232996-3299662.37162.52
333957-3395764.18764.34
432230-3223060.92361.06
531706-3170659.93260.06
633762-3376263.81963.97
20min135935-3593567.92668.201.7068.1868.451.71
235919-3591967.89668.15
336689-3668969.35269.61
436043-3604368.13068.37
535112-3511266.37166.60
636794-3679469.55069.81
30min138839-3883973.41674.481.4773.7874.841.48
239052-3905273.81874.18
340148-4014875.89076.27
439367-3936774.41474.76
538937-3893773.60173.94
640076-4007675.75476.12
45min141319-4131978.10379.301.0878.5979.781.07
241719-4171978.86079.35
342044-4204479.47479.98
441781-4178178.97779.45
542228-4222879.82280.28
642615-4261580.55381.05
60min141965-4196579.32581.071.2579.9481.691.24
242778-4277880.86181.48
343144-4314481.55382.19
442966-4296681.21781.82
543589-4358982.39482.99
642901-4290181.09481.73
极限144363-4436383.85785.401.3184.6186.161.30
244753-4475384.59585.35
346098-4609887.13787.91
445220-4522085.47786.22
545293-4529385.61586.35
645352-4535285.72786.49
多替诺雷片项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号D241101对照品来源工作对照品对照品使用方法直接使用
对照品含量(%)99.69对照品水分(%)0对照品稀释倍数5000
标示量(mg)2供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
110.004758047244471784732547146472950.37
29.994748347454474680.05
单位质量响应值RSD%判断
4729.504751.550.33数据可信
供试品溶液-25030602批-水
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min116696-1669631.60039.9818.7731.6039.9818.78
215673-1567329.66329.66
323183-2318343.87743.88
422028-2202841.69141.69
524973-2497347.26547.27
624189-2418945.78145.78
10min128972-2897254.83459.318.4654.8959.388.47
227564-2756452.16952.22
332504-3250461.51961.59
431237-3123759.12159.19
534586-3458665.45965.54
633160-3316062.76062.84
15min135281-3528166.77568.193.8566.9268.353.87
233793-3379363.95864.09
336150-3615068.41968.59
436065-3606568.25868.43
537575-3757571.11671.30
637299-3729970.59470.77
20min139356-3935674.48772.952.6274.7473.232.62
236791-3679169.63269.88
338243-3824372.38172.67
438319-3831972.52472.81
539524-3952474.80575.11
639023-3902373.85774.16
30min142652-4265280.72577.972.2581.1078.372.24
240181-4018176.04976.41
340365-4036576.39776.81
440868-4086877.34977.75
541726-4172678.97379.40
641378-4137878.31478.74
45min145182-4518285.51481.092.9786.0381.622.96
242130-4213079.73780.22
341796-4179679.10579.64
441948-4194879.39379.92
543285-4328581.92382.49
642742-4274280.89681.45
60min146377-4637787.77582.363.5288.4383.023.49
243347-4334782.04182.66
342471-4247180.38381.05
441974-4197479.44280.11
543448-4344882.23282.93
643464-4346482.26282.95
极限147248-4724889.42485.552.4090.2386.352.38
245289-4528985.71686.47
344719-4471984.63785.44
444051-4405183.37384.17
544935-4493585.04685.88
644967-4496785.10785.93
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