洛索洛芬钠细粒剂项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100638-202405对照品来源中检所对照品使用方法直接使用
对照品含量(%)87.5对照品水分(%)0对照品稀释倍数200
标示量(mg)60供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.761166486116545811667371166941116692211665090.06
213.741176327117660411764660.02
单位质量响应值RSD%判断
84775.3685623.440.71数据可信
供试品溶液-2025020621批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11288729-128872999.26798.541.6799.2798.541.67
21300333-1300333100.161100.16
31257221-125722196.84096.84
41272174-127217497.99297.99
51303154-1303154100.378100.38
61254079-125407996.59896.60
10min11310971-1310971100.980100.051.65101.15100.221.66
21317260-1317260101.465101.63
31284054-128405498.90799.07
41295870-129587099.81799.98
51320190-1320190101.690101.86
61265280-126528097.46197.62
15min11309462-1309462100.86499.991.56101.20100.321.56
21315549-1315549101.333101.67
31283635-128363598.87599.20
41295449-129544999.785100.11
51318325-1318325101.547101.88
61266628-126662897.56597.89
30min11311125-1311125100.992100.181.56101.49100.681.56
21317369-1317369101.473101.98
31285989-128598999.05699.55
41300220-1300220100.152100.65
51320687-1320687101.729102.23
61268244-126824497.68998.18
极限11310240-1310240100.924100.001.60101.59100.671.60
21315412-1315412101.322102.00
31283909-128390998.89699.55
41300114-1300114100.144100.81
51316127-1316127101.377102.05
61264031-126403197.36598.01
洛索洛芬钠细粒剂项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100638-202405对照品来源中检所对照品使用方法直接使用
对照品含量(%)87.5对照品水分(%)0对照品稀释倍数200
标示量(mg)60供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.761166782116661211672101166395116587911665760.05
213.741168848116688711678680.12
单位质量响应值RSD%判断
84780.2384997.670.19数据可信
供试品溶液-2025020621批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11305467-1305467100.92297.155.75100.9297.165.75
21111871-111187185.95585.96
31298053-1298053100.349100.35
41274014-127401498.49098.49
51271627-127162798.30698.31
61279411-127941198.90798.91
10min11325010-1325010102.433100.193.44102.60100.363.44
21209333-120933393.49093.63
31332686-1332686103.026103.19
41309112-1309112101.204101.37
51299919-1299919100.493100.66
61300301-1300301100.522100.69
15min11321989-1321989102.199100.572.33102.54100.902.34
21245635-124563596.29696.60
31332548-1332548103.015103.35
41309426-1309426101.228101.56
51298307-1298307100.368100.70
61297823-1297823100.331100.66
30min11325130-1325130102.442101.011.99102.95101.502.00
21261606-126160697.53197.99
31336966-1336966103.357103.87
41311892-1311892101.418101.92
51303080-1303080100.737101.24
61300619-1300619100.547101.05
极限11323278-1323278102.299100.811.97102.98101.471.98
21259581-125958197.37498.00
31333334-1333334103.076103.76
41308879-1308879101.186101.86
51300878-1300878100.567101.23
61297950-1297950100.341101.01
洛索洛芬钠细粒剂项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100638-202405对照品来源中检所对照品使用方法直接使用
对照品含量(%)87.5对照品水分(%)0对照品稀释倍数200
标示量(mg)60供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.761173113117351511744181173618117445311738230.06
213.741181330118125111812900.01
单位质量响应值RSD%判断
85306.9085974.530.56数据可信
供试品溶液-2025020721批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11332237-1332237102.08999.251.78102.0999.251.78
21269426-126942697.27597.28
31276921-127692197.85097.85
41309079-1309079100.314100.31
51297063-129706399.39399.39
61286430-128643098.57898.58
10min11340525-1340525102.724100.061.81102.89100.221.81
21278564-127856497.97698.14
31286275-128627598.56798.73
41322157-1322157101.316101.48
51312519-1312519100.578100.74
61294493-129449399.19699.36
15min11337327-1337327102.47999.891.78102.82100.221.79
21276005-127600597.78098.10
31281961-128196198.23698.56
41319297-1319297101.097101.43
51309527-1309527100.348100.68
61297083-129708399.39599.72
30min11335991-1335991102.37699.731.78102.89100.231.78
21274880-127488097.69398.18
31281282-128128298.18498.68
41318145-1318145101.009101.51
51305476-1305476100.038100.54
61292982-129298299.08099.58
极限11330919-1330919101.98899.451.73102.67100.111.73
21270892-127089297.38898.04
31278856-127885697.99898.65
41312580-1312580100.582101.26
51303463-130346399.884100.55
61289872-128987298.84299.50
洛索洛芬钠细粒剂项目信息
介质体积(ml)900取样体积(ml)1.5补液体积(ml)1.5
对照品批号100638-202405对照品来源中检所对照品使用方法直接使用
对照品含量(%)87.5对照品水分(%)0对照品稀释倍数200
标示量(mg)60供试品稀释倍数1系数1
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.761165799116579411665101166763116705011663830.05
213.741162996116433411636650.09
单位质量响应值RSD%判断
84766.2184691.780.07数据可信
供试品溶液-2025020721批-pH6.8
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min11278068-127806898.990100.322.5398.99100.322.53
21289385-128938599.86799.87
31249257-124925796.75996.76
41289409-128940999.86899.87
51326771-1326771102.762102.76
61338720-1338720103.688103.69
10min11303700-1303700100.975101.532.00101.14101.702.00
21296337-1296337100.405100.57
31272109-127210998.52898.69
41315688-1315688101.904102.07
51333354-1333354103.272103.44
61344342-1344342104.123104.30
15min11302318-1302318100.868101.491.89101.20101.821.89
21294977-1294977100.300100.63
31276331-127633198.85599.18
41312520-1312520101.658101.99
51332089-1332089103.174103.52
61343688-1343688104.072104.42
30min11297290-1297290100.479101.261.91100.98101.761.91
21292151-1292151100.081100.58
31273780-127378098.65899.15
41310635-1310635101.512102.02
51327903-1327903102.850103.37
61342291-1342291103.964104.48
极限11296462-1296462100.415100.991.89101.08101.661.89
21287461-128746199.718100.39
31270878-127087898.43399.09
41305110-1305110101.084101.76
51326551-1326551102.745103.43
61336781-1336781103.537104.23
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