苯磺酸左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数8000
标示量(mg)2.5供试品稀释倍数2系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.754204942154421404216141921420850.25
213.754202142189421050.29
单位质量响应值RSD%判断
3060.733062.180.04数据可信
加速5月-供试品溶液-24092401批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min146809-4680996.53798.942.5496.5498.942.54
248971-48971100.995101.00
348241-4824199.49099.49
447648-4764898.26798.27
546523-4652395.94795.95
649643-49643102.381102.38
10min148771-48771100.583101.151.77101.66102.261.77
249024-49024101.105102.23
349459-49459102.002103.11
447809-4780998.59999.69
548799-48799100.641101.71
650423-50423103.990105.13
15min149037-49037101.132100.271.29103.32102.491.29
248535-48535100.096102.34
348843-48843100.731102.97
448264-4826499.537101.72
547638-4763898.246100.43
649405-49405101.891104.18
20min148184-4818499.37298.501.45102.69101.841.45
247871-4787198.727102.08
347633-4763398.236101.59
447066-4706697.067100.36
546999-4699996.928100.20
648820-48820100.684104.11
30min147633-4763398.23697.851.21102.65102.281.22
247711-4771198.397102.85
347194-4719497.331101.78
446733-4673396.380100.75
547056-4705697.046101.40
648345-4834599.704104.25
45min146261-4626195.40696.241.94100.92101.761.90
246787-4678796.491102.04
346647-4664796.203101.73
445475-4547593.78599.23
546586-4658696.077101.51
648237-4823799.482105.13
60min145619-4561994.08295.331.69100.65101.921.67
246327-4632795.543102.16
346267-4626795.419102.02
445581-4558194.004100.49
545882-4588294.625101.12
647680-4768098.333105.09
极限145582-4558294.00695.261.46101.62102.911.46
246760-4676096.436104.12
346237-4623795.357103.02
445440-4544093.713101.24
545964-4596494.794102.34
647170-4717097.281105.13
苯磺酸左氨氯地平片项目信息
介质体积(ml)900取样体积(ml)10补液体积(ml)10
对照品批号100546-202105对照品来源中检院对照品使用方法直接使用
对照品含量(%)97.3对照品水分(%)0对照品稀释倍数8000
标示量(mg)2.5供试品稀释倍数2系数0.7210
对照品溶液
序号称样量(mg)A1A2A3A4A5A平均RSD%
113.754201541853420284208942178420330.29
213.754219142128421600.11
单位质量响应值RSD%判断
3056.953066.180.22数据可信
加速5月-供试品溶液-24092401-2批-pH2.0
时间
(分钟)		样品A1A2A平均溶出量(%)平均(%)RSD%累计溶
出量(%)		平均(%)RSD%
5min147557-4755798.07696.911.3898.0896.911.38
246222-4622295.32395.32
346738-4673896.38796.39
446843-4684396.60496.60
547965-4796598.91798.92
646629-4662996.16296.16
10min146929-4692996.78197.021.0697.8798.101.06
246625-4662596.15497.21
346718-4671896.34697.42
447571-4757198.10599.18
547763-4776398.50199.60
646666-4666696.23997.31
15min147025-4702596.97997.290.7599.1499.440.75
246739-4673996.38998.52
347308-4730897.56299.70
447467-4746797.890100.05
547633-4763398.233100.43
646877-4687796.67498.81
20min145922-4592294.70494.700.5097.9597.940.50
245978-4597894.82098.02
345521-4552193.87797.10
446226-4622695.33198.58
545987-4598794.83898.12
645891-4589194.64097.85
30min145553-4555393.94394.750.6798.2499.040.63
246126-4612695.12599.38
345674-4567494.19398.46
445905-4590594.66998.98
546036-4603694.93999.28
646381-4638195.65199.91
45min145958-4595894.77894.220.52100.1299.560.52
245290-4529093.40198.71
345561-4556193.96099.27
445714-4571494.27599.64
545864-4586494.58599.98
645732-4573294.31299.64
60min145012-4501292.82792.231.0999.2298.621.05
243947-4394790.63196.98
344461-4446191.69198.05
444877-4487792.54998.96
545355-4535593.53599.98
644694-4469492.17298.55
极限144544-4454491.86291.410.7299.2998.820.71
243894-4389490.52297.88
344020-4402090.78298.16
444672-4467292.12699.56
544560-4456091.89599.38
644251-4425191.25898.66
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